Impact of Sn on the Ti/Ge solid-state reaction: Phase formation sequence, morphological and electrical properties

2022 ◽  
Vol 252 ◽  
pp. 111667
Author(s):  
Andrea Quintero ◽  
Patrice Gergaud ◽  
Jean-Michel Hartmann ◽  
Vincent Reboud ◽  
Eric Cassan ◽  
...  
2018 ◽  
Vol 124 (8) ◽  
pp. 085305 ◽  
Author(s):  
A. Quintero ◽  
P. Gergaud ◽  
J. Aubin ◽  
J. M. Hartmann ◽  
N. Chevalier ◽  
...  

JOM ◽  
2021 ◽  
Author(s):  
Evgeny T. Moiseenko ◽  
Sergey M. Zharkov ◽  
Roman R. Altunin ◽  
Oleg V. Belousov ◽  
Leonid A. Solovyov ◽  
...  

2016 ◽  
Vol 675-676 ◽  
pp. 527-530
Author(s):  
Thanatep Phatungthane ◽  
Kachaporn Sanjoom ◽  
Denis Russell Sweatman ◽  
Buagun Samran ◽  
Chamnan Randorn ◽  
...  

In the present work, strontium iron niobate SrFe0.5Nb0.5O3 ceramics doped with aluminum were synthesized by a solid-state reaction technique. Phase formation investigation by X-ray diffraction technique (XRD) revealed that all ceramics exhibited pure perovskite phase with orthorhombic symmetry. Grain size observed by electron microscopy (SEM) was found to increase with increasing sintering temperature. The electrical properties and related parameters of the ceramics were also measured. The ceramics exhibit very good dielectric behavior and have a significant potential for dielectric applications.


2018 ◽  
Vol 70 (3) ◽  
pp. 560-567 ◽  
Author(s):  
Jian Feng Li ◽  
Qin Shi ◽  
HeJun Zhu ◽  
ChenYu Huang ◽  
Shuai Zhang ◽  
...  

Purpose This paper aims to clarify the size and morphology of transition metal dichalcogenides has an impact on lubrication performance of Cu-based composites. This study is intended to show that Cu-based electrical contact materials containing Nb0.91Ti0.09Se2 have better electrical and tribological properties than those containing NbSe2. The tribological properties of Cu-based with different Ti-dopped NbSe2 content were also discussed. Design/methodology/approach The NbSe2 and Nb0.91Ti0.09Se2 particles were fabricated by thermal solid state reaction method. The powder metallurgy technique was used to fabricate composites with varying Nb0.91Ti0.09Se2 mass fraction. The phase composition of Cu-based composites was identified by X-ray diffraction, and the morphology of NbSe2/Nb0.91Ti0.09Se2 and the worn surface of composites were characterized by scanning electron microscopy and transmission electron microscopy. In addition, the tribological properties of composites were appraised using a ball-on-disk multi-functional tribometer. The data of friction coefficient and resistivity were analyzed and the corresponding conclusion was drawn. Findings In comparison with the pure copper, Cu-based composites containing Nb0.91Ti0.09Se2/NbSe2 had a lower friction coefficient, illustrating the Nb0.91Ti0.09Se2 with nano-size particles prepared in this work is a perfect choice for the fabrication of excellent electrical contact composites. Compared to composites with NbSe2, composites containing Nb0.91Ti0.09Se2 have better tribological and electrical properties. Research limitations/implications Because of the use of thermal solid state reaction method, the size of NbSe2 and Nb0.91Ti0.09Se2 is relatively large. Therefore, the fabrication of finer particles of Nb0.91Ti0.09Se2 is encouraged. Originality/value In this paper, the authors discuss the tribological and electrical properties of Cu-based composites, and the value of optimum obtained as Nb0.91Ti0.09Se2 content is 15 Wt.%.


2008 ◽  
Vol 368-372 ◽  
pp. 265-267 ◽  
Author(s):  
Hui Zhu Zhou ◽  
Lei Dai ◽  
Yue Hua Li ◽  
Yin Lin Wu ◽  
Ling Wang ◽  
...  

Mg ion conductors, MgAl2O4 and MgZr4(PO4)6, were prepared by solid state reaction. Their electrical properties were measured and their application in electrochemical sensors for on-line determination of Mg in molten Al in the refining process and alloying process was examined. The activation energies for Mg ion conduction in MgAl2O4 and MgZr4(PO4)6 are 2.08 eV and 1.7 eV, respectively. The sensors have been found to respond rapidly to the change of Mg content in molten aluminium around 1000 K.


RSC Advances ◽  
2018 ◽  
Vol 8 (28) ◽  
pp. 15613-15620 ◽  
Author(s):  
Xiaochun He ◽  
Ruiqing Chu ◽  
Zhijun Xu ◽  
Zhongran Yao ◽  
Jigong Hao

Lead-free ceramics, SrBi2Nb2O9–xBi2O3 (SBN–xBi), with different Bi contents of which the molar ratio, n(Sr) : n(Bi) : n(Nb), is 1 : 2(1 + x/2) : 2 (x = −0.05, 0.0, 0.05, 0.10), were prepared by conventional solid-state reaction method.


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