Detection of 2,4-dinitrotoluene using microcantilever sensors

2004 ◽  
Vol 99 (2-3) ◽  
pp. 223-229 ◽  
Author(s):  
L.A Pinnaduwage ◽  
T Thundat ◽  
J.E Hawk ◽  
D.L Hedden ◽  
P.F Britt ◽  
...  
Author(s):  
Andrew W. McFarland ◽  
Jonathan S. Colton ◽  
Daniel Cox ◽  
Steven Y. Liang

Mechanical micro machining is an emerging technology with many potential benefits and equally great challenges. The push to develop processes and tools capable of micro scale fabrication is a result of the widespread drive to reduce part and feature size. One important factor that contributes to the ability to machine at the microscale level is the overall size of the machine tool due to the effects of thermal, static, and dynamic stabilities. This paper explores the technical feasibility of miniaturized machine tools capable of fabricating features and parts on the micro scale in terms of depth of cut and part form accuracy. It develops a machine tool and examines its capabilities through benchmarking tests and the making of precision dies for the injection molding of microcantilever parts. The design and configuration of a miniaturized vertical machining center of overall dimension less than 300 mm on a side is presented and the component specifications discussed. The six axis machine has linear positioning resolution of 4 nm by 10 nm by 10 nm, with accuracy on the order of 0.3 μm, in the height, feed, and cross feed directions. The work volume as defined by the ranges of axes travel are 4 mm by 25 mm by 25 mm in the height, feed, and cross feed and 20 degrees in the rotational space. To quantify the performance capability of the miniaturized machine tool as a system, a series of evaluation tests were implemented based on linear and arch trajectories over a range of feed speed and depth of cut conditions. Test results suggest that micro level form accuracy and sub-micron level finish are generally achievable for parts with moderate curvature and gradient in the geometry under selected machining parameters and conditions. An injection mold was made of steel with this machine and plastic microcantilevers fabricated. Plastic microcantilevers are appropriate for sensing applications such as surface probe microscopy. The microcantilevers, made from polystyrene, were 464 to 755 μm long, 130 μm wide and only 6–9 μm thick. They showed very good uniformity, reproducibility, and appropriate mechanical response for use as sensors in surface force microscopy.


2008 ◽  
Vol 19 (38) ◽  
pp. 384007 ◽  
Author(s):  
Tuomas P J Knowles ◽  
Wenmiao Shu ◽  
François Huber ◽  
Hans Peter Lang ◽  
Christoph Gerber ◽  
...  

2011 ◽  
Vol 415-417 ◽  
pp. 455-459
Author(s):  
Xiao Ming Wang ◽  
Fei Wang ◽  
Xue Zeng Zhao ◽  
Da Lei Jing

The modified static bending model of microcantilever with monolayer molecules has been established based on energy method, in which the change in neutral layer position caused by adsorption-induced stress has been considered. On this basis, we have analyzed the relationship between the bending curvature radius of a microcantilever with its thickness, Young’s modulus and molecule-molecule distance of adsorbed molecules when it is adsorbed with monolayer water molecules. Additionally, we have investigated the effect of change in neutral layer position on the static behavior of microcantilever sensors and have found that: 1) the bending curvature radius of microcantilever is affected by its Young’s modulus, thickness and distance of adsorbed molecules respectively; 2)the predicted error of bending curvature radius caused by the change in neutral layer position slightly increases with decreasing Young’s modulus and thickness, whereas the effect of distance between adsorbed molecules on the error is significant.


AIChE Journal ◽  
2007 ◽  
Vol 53 (10) ◽  
pp. 2726-2731 ◽  
Author(s):  
Eunhyea Chung ◽  
Nickolay Lavrik ◽  
Panos Datskos ◽  
Joanna Mcfarlane ◽  
Sheng Dai ◽  
...  

2010 ◽  
Vol 518 (15) ◽  
pp. 4345-4350 ◽  
Author(s):  
Fu-Zhen Xuan ◽  
Shan-Shan Shao ◽  
Zhengdong Wang ◽  
Shan-Tung Tu

Author(s):  
Paris E. Georghiou ◽  
Shofiur Rahman ◽  
Yousif Assiri ◽  
Gopi Kishore Valluru ◽  
Melita Menelaou ◽  
...  

The development of a microcantilever (MCL) sensing device capable of simultaneously detecting several metal ionic species in aqueous media with low limits of detection requires a variety of sensing layers which are ion-specific. Calix[4]arenes are robust molecules which can be easily modified and have been extensively studied for their ion binding properties. They are also capable of forming self-assembled monolayers (SAMs) onto the gold layers of MCLs and are capable of detecting various metal ions with different anionic counterions in aqueous solutions. In this paper we report on the effect of the alkoxy group in the narrow rim [O-(alkoxycarbonyl)methoxy] substituents of bimodal calix[4]arenes which have been used as metal ion MCL sensing layers, using classical solution state experimental studies. A DFT computational study to compare the experimental results with several metal ions is also reported herein.


Sensors ◽  
2019 ◽  
Vol 19 (21) ◽  
pp. 4758 ◽  
Author(s):  
Wilson Ombati Nyang’au ◽  
Andi Setiono ◽  
Maik Bertke ◽  
Harald Bosse ◽  
Erwin Peiner

Cantilever-based sensors have attracted considerable attention in the recent past due to their enormous and endless potential and possibilities coupled with their dynamic and unprecedented sensitivity in sensing applications. In this paper, we present a technique that involves depositing and vaporizing (at ambient conditions) a particle-laden water droplet onto a defined sensing area on in-house fabricated and commercial-based silicon microcantilever sensors. This process entailed the optimization of dispensing pressure and time to generate and realize a small water droplet volume (Vd = 49.7 ± 1.9 pL). Moreover, we monitored the water evaporation trends on the sensing surface and observed total evaporation time per droplet of 39.0 ± 1.8 s against a theoretically determined value of about 37.14 s. By using monodispersed particles in water, i.e., magnetic polystyrene particles (MPS) and polymethyl methacrylate (PMMA), and adsorbing them on a dynamic cantilever sensor, the mass and number of these particles were measured and determined comparatively using resonant frequency response measurements and SEM particle count analysis, respectively. As a result, we observed and reported monolayer particles assembled on the sensor with the lowest MPS particles count of about 19 ± 2.


2007 ◽  
Vol 29 (10) ◽  
pp. 1084-1088 ◽  
Author(s):  
R. Stewart ◽  
J. Reed ◽  
J. Zhong ◽  
K. Morton ◽  
T.L. Porter

Author(s):  
Jungchul Lee ◽  
Hanif Hunter ◽  
Fabian Goericke ◽  
Nisarga Naik ◽  
Mark Allen ◽  
...  

This paper reports novel microcantilever metrology tools to investigate free microjets emanating from a micromachined nozzle having 10 μm diameter. Microcantilever sensors are well-suited to interrogate these flows due to their high spatial and temporal resolution. In this work, microcantilevers with integrated piezoresistors have been used to detect the breakup distance of free microjets, and microcantilevers with integrated resistive heaters have been applied to study microjet cooling and phase change characteristics. Measured microjet thrusts were in the range of 10 – 60 μN and heat fluxes were measured in the range of 25 – 350 °C. The convective heat fluxes by microjet impingement boiling were estimated at 2.9 – 7.6 kW/cm2. The techniques reported herein are promising to characterize microscale flows.


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