Properties enhancement of graphene and chemical reduction silver nanoparticles conductive inks printed on polyvinyl alcohol (PVA) substrate

2019 ◽  
Vol 256 ◽  
pp. 116120 ◽  
Author(s):  
Y.Z.N. Htwe ◽  
W.S. Chow ◽  
G. Suriati ◽  
A.A. Thant ◽  
M. Mariatti
2015 ◽  
Vol 2015 ◽  
pp. 1-10 ◽  
Author(s):  
Vinod Vellora Thekkae Padil ◽  
Nhung H. A. Nguyen ◽  
Alena Ševců ◽  
Miroslav Černík

Gum karaya (GK), a natural hydrocolloid, was mixed with polyvinyl alcohol (PVA) at different weight ratios and electrospun to produce PVA/GK nanofibers. An 80 : 20 PVA/GK ratio produced the most suitable nanofiber for further testing. Silver nanoparticles (Ag-NPs) were synthesised through chemical reduction of AgNO3(at different concentrations) in the PVA/GK solution, the GK hydroxyl groups being oxidised to carbonyl groups, and Ag+cations reduced to metallic Ag-NPs. These PVA/GK/Ag solutions were then electrospun to produce nanofiber membranes containing Ag-NPs (Ag-MEMs). Membrane morphology and other characteristics were analysed using scanning electron microscopy coupled with energy dispersive X-ray analysis, transmission electron microscopy, and UV-Vis and ATR-FTIR spectroscopy. The antibacterial activity of the Ag-NP solution and Ag-MEM was then investigated against Gram-negativeEscherichia coliandPseudomonas aeruginosaand Gram-positiveStaphylococcus aureus. Our results show that electrospun nanofiber membranes based on natural hydrocolloid, synthetic polymer, and Ag-NPs have many potential uses in medical applications, food packaging, and water treatment.


2021 ◽  
Vol 2075 (1) ◽  
pp. 012004
Author(s):  
N N M Rashid ◽  
M Q Lokman ◽  
N A Nordin ◽  
H Yahaya ◽  
F Ahmad

Abstract Silver nanoparticles (AgNP), a novel candidate of noble metal nanoparticles, which has great potential for pulsed laser applications due to strong saturation absorption behaviour. This study demonstrated the passively Q-switched laser operating within an Erbium-doped fibre laser cavity using AgNP saturable absorber (SA). The AgNP was synthesized via the chemical reduction method and the average size of nanoparticles was around 52.39 nm. The AgNP was incorporated with polyvinyl alcohol (PVA) polymer to form an AgNP-PVA composite SA. The proposed experimental works generated single pulse energy and peak power of about 66.14 nJ and 18.71 mW corresponds to the repetition rate and pulse width of 62.89 kHz and 3.32 µs.


Author(s):  
Umadevi M ◽  
Rani T ◽  
Balakrishnan T ◽  
Ramanibai R

Nanotechnology has great promise for improving the therapeutic potential of medicinal molecules and related agents. In this study, silver nanoparticles of different sizes were synthesized in an ultrasonic field using the chemical reduction method with sodium borohydride as a reducing agent. The size effect of silver nanoparticles on antimicrobial activity were tested against the microorganisms Staphylococcus aureus (MTCC No. 96), Bacillus subtilis (MTCC No. 441), Streptococcus mutans (MTCC No. 497), Escherichia coli (MTCC No. 739) and Pseudomonas aeruginosa (MTCC No. 1934). The results shows that B. subtilis, and E. coli were more sensitive to silver nanoparticles and its size, indicating the superior antimicrobial efficacy of silver nanoparticles. 


Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2326
Author(s):  
Entesar Ali Ganash ◽  
Reem Mohammad Altuwirqi

In this work, silver nanoparticles (Ag NPs) were synthesized using a chemical reduction approach and a pulsed laser fragmentation in liquid (PLFL) technique, simultaneously. A laser wavelength of 532 nm was focused on the as produced Ag NPs, suspended in an Origanum majorana extract solution, with the aim of controlling their size. The effect of liquid medium concentration and irradiation time on the properties of the fabricated NPs was studied. While the X-ray diffraction (XRD) pattern confirmed the existence of Ag NPs, the UV–Vis spectrophotometry showed a significant absorption peak at about 420 nm, which is attributed to the characteristic surface plasmon resonance (SPR) peak of the obtained Ag NPs. By increasing the irradiation time and the Origanum majora extract concentration, the SPR peak shifted toward a shorter wavelength. This shift indicates a reduction in the NPs’ size. The effect of PLFL on size reduction was clearly revealed from the transmission electron microscopy images. The PLFL technique, depending on experimental parameters, reduced the size of the obtained Ag NPs to less than 10 nm. The mean zeta potential of the fabricated Ag NPs was found to be greater than −30 mV, signifying their stability. The Ag NPs were also found to effectively inhibit bacterial activity. The PLFL technique has proved to be a powerful method for controlling the size of NPs when it is simultaneously associated with a chemical reduction process.


DYNA ◽  
2018 ◽  
Vol 85 (206) ◽  
pp. 69-78 ◽  
Author(s):  
Wilson Agudelo ◽  
Yuliet Montoya ◽  
John Bustamante

El uso de compuestos químicos más biocompatibles y renovables para la obtención de nanopartículas metálicas con propiedades y características deseadas, se convierte en una ruta alternativa para la reducción de riesgos ambientales y del grado de incompatibilidad de estas estructuras al interactuar con modelos biológicos para su posible aplicación en el área de la salud. El propósito de este trabajo se centró en el uso de sacarosa, como agente reductor de nanopartículas de oro y plata al emplear diferentes volúmenes de hidróxido de sodio. Las nanopartículas obtenidas fueron caracterizadas mediante espectrometría UV-visible, microscopía electrónica de transmisión TEM y espectroscopia infrarroja por transformada de Fourier FTIR, la cual permitió determinar los plasmones de resonancia superficial, tamaños de partícula experimentales y teóricos, morfología y cambios estructurales en el agente reductor, así como la influencia del hidróxido de sodio en el proceso de síntesis. Los resultados obtenidos confirman la formación de nanopartículas de oro y plata mediante la previa formación de azúcares reductores. Así mismo, la oxidación del grupo funcional de la glucosa a sales de ácido carboxílico.


2014 ◽  
Vol 32 (1) ◽  
pp. 107-111 ◽  
Author(s):  
M. K. Alqadi ◽  
O. A. Abo Noqtah ◽  
F. Y. Alzoubi ◽  
J. Alzouby ◽  
K. Aljarrah

2020 ◽  
Vol 19 (04) ◽  
pp. 1950029
Author(s):  
A. G. Demchenko ◽  
V. S. Sadykova ◽  
A. V. Lyundup ◽  
N. E. Sedyakina ◽  
T. I. Gromovykh ◽  
...  

Silver nanoparticles were synthesized by chemical reduction of silver nitrate using arabinogalactan polysaccharide as a reducing agent and a stabilizer. The average size of nanoparticles, obtained by analyzing TEM-images, was 10.8[Formula: see text]nm; zeta potential [Formula: see text][Formula: see text]mV. A study of the sol by electron diffraction showed that silver in the sample is in metallic form. The resulting preparation of silver nanoparticles showed both antibacterial and antifungal activity. A pronounced antibacterial activity of silver nanoparticles was demonstrated both in relation to conditionally pathogenic gram-positive (Bacillus subtilis and B. coagulans) and gram-negative (Escherichia coli) bacteria. Silver nanoparticles also possess antifungal activity against macromycete Fomitopsis sp., as well as two strains of micromycetes Trichoderma citrinoviride and Fusarium sporotrichioides. Using the methods of light and fluorescence microscopy, MTT-analysis and Real-time cell analysis, the cytotoxic activity of silver nanoparticles was investigated on HepG2 human hepatocellular carcinoma cells. It was demonstrated that nanoparticles cause a suppression of cell metabolic and proliferative activity, as well as dose-dependent induction of cell death (average relative EC[Formula: see text] value was [Formula: see text]g/ml). The preparation of silver nanoparticles stabilized by arabinogalactan can be used in medicine, as a potential antimicrobial and antitumor agent.


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