Microtensile bond strength of new self-adhesive luting agents and conventional multistep systems

2009 ◽  
Vol 102 (5) ◽  
pp. 306-312 ◽  
Author(s):  
Ronaldo G. Viotti ◽  
Alline Kasaz ◽  
Carlos E. Pena ◽  
Rodrigo S. Alexandre ◽  
Cesar A. Arrais ◽  
...  
2016 ◽  
Vol 41 (2) ◽  
pp. 189-199 ◽  
Author(s):  
VB Santana ◽  
RS de Alexandre ◽  
JA Rodrigues ◽  
C Ely ◽  
AF Reis

SUMMARY Objective: The object of this study was to evaluate the simulated pulpal pressure (SPP) and immediate dentin sealing technique (IDS) effects on the microtensile bond strength (μTBS) and nanoleakage of interfaces produced by different luting agents. Methods and Materials: Two self-adhesive luting agents (RelyX Unicem [UC] and Clearfil SA Luting [SA]) and two conventional luting agents (Rely X ARC [RX] and Panavia F [PF]) were evaluated. Eighty human molars were divided in four groups according to luting agents. Each group was subdivided according to SPP (with or without) and dentin sealing (immediate or delayed) using Clearfil SE Bond (n=5). After IDS was performed, specimens were stored in water for seven days before luting procedures. Composite blocks were luted according to the manufacturers' instructions. One half of the specimens were subjected to 15 cm H2O of hydrostatic pressure for 24 hours before cementation procedures and continued for 24 hours afterward. Then, restored teeth were sectioned into beams and tested in tension. Two additional teeth per group were prepared for nanoleakage evaluation with scanning electron microscopy. Bond strength data were statistically analyzed by three-way analysis of variance and Tukey test. Results: μTBS of RX decreased when it was subjected to SPP without IDS. However, in the same conditions, μTBS of UC increased. The IDS prevented negative influence of SPP on μTBS of RX and PF; however, a decrease in μTBS of SA and UC was observed. Except for RX, IDS increased μTBS for all resin cements. Conclusion: Independent of SPP, the IDS technique obtained higher μTBS for PF, SA, and UC and did not influence RX μTBS.


2009 ◽  
Vol 34 (3) ◽  
pp. 328-336 ◽  
Author(s):  
C. D'Arcangelo ◽  
F. De Angelis ◽  
M. D'Amario ◽  
S. Zazzeroni ◽  
C. Ciampoli ◽  
...  

Clinical Relevance Compared to self-etch and self-adhesive luting systems, the two etch-and-rinse luting agents evaluated in the current study provided more reliable bonding when used to bond indirect resin-based composite restorations to sound dentin. On the contrary, the self-adhesive luting system showed the highest mean bond strength for the cementation of glass ceramic restorations.


2001 ◽  
Vol 28 (12) ◽  
pp. 1122-1128 ◽  
Author(s):  
K. Soeno ◽  
Y. Taira ◽  
H. Matsumura ◽  
M. Atsuta

2014 ◽  
Vol 39 (5) ◽  
pp. 508-520 ◽  
Author(s):  
RS de Alexandre ◽  
VB Santana ◽  
AC Kasaz ◽  
CAG Arrais ◽  
JA Rodrigues ◽  
...  

SUMMARY This study evaluated the effects of simulated hydrostatic pulpal pressure (SPP) on the microtensile bond strength (μTBS) to dentin and nanoleakage patterns produced by self-adhesive luting agents after 12 months. Three self-adhesive luting agents (RelyX Unicem [UN], RelyX U100 [UC], and Clearfil SA Luting [SA]) and three conventional luting agents (Rely X ARC [RX], Panavia F [PF], and a two-step self-etching adhesive system [Clearfil SE Bond] associated with Panavia F [PS]) were evaluated. One hundred twenty-three human molars were abraded to expose occlusal surfaces. Resin cements were used to lute cylindrical composite blocks to the teeth either subjected or not to SPP. Sixty specimens were subjected to 15 cm H2O of SPP for 24 hours before and 24 hours or 12 months after cementation procedures. Afterward, restored teeth were serially sectioned into beams with a cross-sectional area of 1 mm2 at the bonded interface and were tested in tension (cross-head speed of 1 mm/min). Failure mode was determined using scanning electron microscopy (SEM). Data were statistically analyzed by three-way analysis of variance and post hoc Tukey test (p=0.05). Two additional teeth in each group were serially sectioned into 0.9-mm-thick slabs, which were submitted to a nanoleakage protocol with AgNO3 and analyzed with scanning and transmission electron microscopes. The μTBS values of the etch-and-rinse group (RX) were negatively influenced by SPP and long-term water storage with SPP. After 12 months, UC and SA presented premature failures in all specimens when submitted to SPP. SPP increased silver deposition in most groups in both evaluation times. The hydrostatic pulpal pressure effect was material dependent. The storage time without SPP did not affect bond strength. However, long-term SPP influenced the performance of the etch-and-rinse and self-adhesive cements regarding μTBS and nanoleakage pattern, except to UN.


2011 ◽  
Vol 36 (6) ◽  
pp. 626-634 ◽  
Author(s):  
F De Angelis ◽  
A Minnoni ◽  
LM Vitalone ◽  
F Carluccio ◽  
M Vadini ◽  
...  

Clinical Relevance Although all self-adhesive systems give improved handling and ease of use compared to traditional multi-step adhesive cements, clinicians should still consider self-adhesive cements as a heterogeneous category of luting agents that need to be better classified in terms of bond strength and chemical/mechanical properties.


Author(s):  
Ronaldo Luís Almeida de CARVALHO ◽  
Jean Soares MIRANDA ◽  
Rodrigo Furtado de CARVALHO ◽  
Michelly Rocha DUARTE ◽  
Estevão Tomomitsu KIMPARA ◽  
...  

ABSTRACT Objective Evaluate the influence of silane heat treatment in bond durability between two resin cements and CAD/CAM feldspathic ceramic. Methods 40 feldspathic ceramic blocks were obtained, and were duplicated in microhybrid composite. All ceramic blocks were etched with 10% hydrofluoric acid for 20 s and received application of silane agent. The blocks were randomizedinto eight groups (n=5) according to the surface treatments and luting agents: P- Panavia F; PAg- Panavia F + Aging; HP- Heat Treatment + Panavia F; HPAg- Heat Treatment + Panavia F + Aging; R- RelyX ARC; Rag- RelyX ARC + Aging; HR- Heat Treatment + RelyX ARC; HRAg- Heat Treatment + RelyX ARC + Aging. The heat treatment was performed in furnace at 100 °C for 2 min. All blocks were cemented and cut to obtain samples with adhesive area of 1 mm2. Aging was performed with 10000 thermal cycles. The samples were subjected to microtensile bond strength test. Results The three-way ANOVA test revealed a significant interaction between cement versus heat treatment (p=0.001) and heat treatment versus thermal cycling (p=0.001) indicating that there was a change in bond strength due to surface treatment and aging. Conclusion Therefore, the heat treatment of the silane at 100 ºC for 2 minutes obtained higher values of bond strength between the resin cement and a feldspathic ceramicafter aging.


2012 ◽  
Vol 2012 ◽  
pp. 1-5 ◽  
Author(s):  
Tomoko Abo ◽  
Shigeru Uno ◽  
Masahiro Yoshiyama ◽  
Toshimoto Yamada ◽  
Nobuhiro Hanada

2010 ◽  
Vol 26 ◽  
pp. e7
Author(s):  
V.D. Hipolito ◽  
P.H.P. D’alpino ◽  
F.B. Piveta ◽  
N. Silikas ◽  
F.P. Rodrigues ◽  
...  

2015 ◽  
Vol 40 (3) ◽  
pp. E102-E111 ◽  
Author(s):  
AC Peixoto ◽  
AA Bicalho ◽  
CP Isolan ◽  
TT Maske ◽  
RR Moraes ◽  
...  

SUMMARY Objectives To evaluate the bond strength of adhesive luting agents applied to caries-affected dentin (CAD). Methods Thirty-six noncarious human third molars were abraded to expose an occlusal dentin surface. Caries lesions were induced in half of the samples using a microcosm biofilm model. Biofilm was cultivated under an anaerobic atmosphere for 14 days in a medium enriched with mucin. The same medium containing 1% sucrose was alternated for 4 hours per day. Cylinders of resin cement (RelyX ARC, RelyX U200, or BisCem) were built up over the dentin substrate and submitted to shear bond load. The samples were then longitudinally sectioned. The hardness and elastic modulus of dentin were measured at different depths from the occlusal surface. A three-dimensional finite element simulation was performed to analyze the residual stress distribution during the shear bond strength test. Bond strength data were analyzed by two-way analysis of variance (ANOVA) and hardness and elastic modulus by split-plot ANOVA. Multiple comparisons were performed with the SNK test (α=0.05). Results For all cements, the highest bond strengths were observed in sound dentin. Relyx ARC bond strength was similar to that of RelyX U200 for both substrates; BisCem had the lowest values. CAD had lower hardness (above a depth of 100 μm) and elastic modulus (above a depth of 150 μm) values than sound dentin. Stress distribution during the bond strength test was similar under all experimental conditions. Conclusion Impairment of the mechanical properties of dentin promoted by carious lesions reduced the bond strength of adhesive luting agents.


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