An experimental apparatus for EDXD of high pressure specimens using synchrotron radiation at BSRF

Author(s):  
Jing Liu ◽  
R.Z. Che ◽  
J. Zhao ◽  
Y.H. Jing ◽  
Y. Yang ◽  
...  
Crystals ◽  
2020 ◽  
Vol 11 (1) ◽  
pp. 34
Author(s):  
Akun Liang ◽  
Robin Turnbull ◽  
Enrico Bandiello ◽  
Ibraheem Yousef ◽  
Catalin Popescu ◽  
...  

We report the first high-pressure spectroscopy study on Zn(IO3)2 using synchrotron far-infrared radiation. Spectroscopy was conducted up to pressures of 17 GPa at room temperature. Twenty-five phonons were identified below 600 cm−1 for the initial monoclinic low-pressure polymorph of Zn(IO3)2. The pressure response of the modes with wavenumbers above 150 cm−1 has been characterized, with modes exhibiting non-linear responses and frequency discontinuities that have been proposed to be related to the existence of phase transitions. Analysis of the high-pressure spectra acquired on compression indicates that Zn(IO3)2 undergoes subtle phase transitions around 3 and 8 GPa, followed by a more drastic transition around 13 GPa.


1990 ◽  
Vol 68 (6) ◽  
pp. 2719-2722 ◽  
Author(s):  
A. Matsumuro ◽  
M. Kobayashi ◽  
T. Kikegawa ◽  
M. Senoo

2006 ◽  
Vol 49 (1-2) ◽  
pp. 92-95
Author(s):  
A. Sacchetti ◽  
M. Cestelli Guidi ◽  
E. Arcangeletti ◽  
P. Postorino ◽  
A. Nucara ◽  
...  

2013 ◽  
Vol 21 (01) ◽  
pp. 1350004 ◽  
Author(s):  
KOJI FUMOTO ◽  
TSUYOSHI KAWANAMI ◽  
TAKAO INAMURA

A cold thermal energy storage system has been developed for HVAC. There are many ice-based cooling systems operating around the world. Ice slurry, which is a mixture of fine ice crystals and liquid water, is utilized in ice storage systems owing to its good flowability and large latent heat of fusion. For slurry ice production techniques, there are presently a number of commercially available ice slurry generators (e.g., Supercooled slurry ice generator, Scraper type generator, and Vacuum type generator, etc.). In the present study, a new method was developed to generate ice slurry without the deposition of an ice layer on a cooled surface. The basic components of the experimental apparatus is a cooling brine circulating loop, a high pressure pump, a valve, an aqueous solution flow loop containing the test section, which is made of transparent acrylic, and the associated instrumentation. This new method is based on freezing-point depression of the aqueous solution, which is maintained under high-pressure conditions. To control the timing for solidification and to generate ice slurry, we investigated the relationships among the pressure and temperature of the aqueous solution. The freezing phenomenon of the aqueous solution in the test section was observed in detail. As a result, we developed a new ice slurry generator based on the new method that controls the pressure and temperature of the aqueous solution. Experimental results showed that the characteristics of the ice slurry generation were closely related to the pressure and initial stage temperature of the test fluid. Finally, the optimum operation condition of the ice slurry generator based on visualization experiment was discussed.


1986 ◽  
Vol 15 (10) ◽  
pp. 1663-1666 ◽  
Author(s):  
Shigeho Sueno ◽  
Izumi Nakai ◽  
Masayuki Imafuku ◽  
Hideki Morikawa ◽  
Mitsuyoshiv Kimata ◽  
...  

1992 ◽  
Vol 8 (5-6) ◽  
pp. 711-713
Author(s):  
Yuechao Zhao ◽  
Rongzheng Che ◽  
Esheng Tang ◽  
Dingchang Xian

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