In-situ SEM observation of tensile deformation in rapidly solidified Ni3Al ribbons

1997 ◽  
Vol 230 (1-2) ◽  
pp. 146-154 ◽  
Author(s):  
P. Pérez ◽  
J. Ibáñez ◽  
P. Gonzalez ◽  
P. Adeva
Keyword(s):  
Tensile Deformation ◽  
Sem Observation ◽  
Rapidly Solidified

Devitrification products of rapidly solidified Ni-Nb amorphous alloys.

1990 ◽  
Vol 48 (4) ◽  
pp. 950-951
Author(s):  
G. A. Bertero ◽  
W.H. Hofmeister ◽  
N.D. Evans ◽  
J.E. Wittig ◽  
R.J. Bayuzick
Keyword(s):  
Electron Microscopy ◽  
Amorphous Structure ◽  
Sulphuric Acid Solution ◽  
X Ray Diffraction ◽  
High Fracture ◽  
Transmission Electron ◽  
Xrd Techniques ◽  
Rapidly Solidified ◽  
Electromagnetically Levitated

Rapid solidification of Ni-Nb alloys promotes the formation of amorphous structure. Preliminary results indicate promising elastic properties and high fracture strength for the metallic glass. Knowledge of the thermal stability of the amorphus alloy and the changes in properties with temperature is therefore of prime importance. In this work rapidly solidified Ni-Nb alloys were analyzed with transmission electron microscopy (TEM) during in-situ heating experiments and after isothermal annealing of bulk samples. Differential thermal analysis (DTA), scanning electron microscopy (SEM) and x-ray diffraction (XRD) techniques were also used to characterize both the solidification and devitrification sequences.Samples of Ni-44 at.% Nb were electromagnetically levitated, melted, and rapidly solidified by splatquenching between two copper chill plates. The resulting samples were 100 to 200 μm thick discs of 2 to 3 cm diameter. TEM specimens were either ion-milled or alternatively electropolished in a methanol-10% sulphuric acid solution at 20 V and −40°C.

scholarly journals In-situ FE-SEM observation of the growth behaviors of Fe particles at magmatic temperatures

2021 ◽  
Vol 560-561 ◽  
pp. 126043
Author(s):  
Mayumi Mujin ◽  
Michihiko Nakamura ◽  
Megumi Matsumoto
Keyword(s):  
Sem Observation

scholarly journals Study on Microstructure and In Situ Tensile Deformation Behavior of Fe-25Mn-xAl-8Ni-C Alloy Prepared by Vacuum Arc Melting

Metals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 814
Author(s):  
Yaping Bai ◽  
Meng Li ◽  
Chao Cheng ◽  
Jianping Li ◽  
Yongchun Guo ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Deformation Behavior ◽  
Tensile Deformation ◽  
Austenite Phase ◽  
Vacuum Arc ◽  
Al Content ◽  
Arc Melting ◽  
Vacuum Arc Melting ◽  
Tensile Deformation Behavior

In this study, Fe-25Mn-xAl-8Ni-C alloys (x = 10 wt.%, 11 wt.%, 12 wt.%, 13 wt.%) were prepared by a vacuum arc melting method, and the microstructure of this series of alloys and the in situ tensile deformation behavior were studied. The results showed that Fe-25Mn-xAl-8Ni-C alloys mainly contained austenite phase with a small amount of NiAl compound. With the content of Al increasing, the amount of austenite decreased while the amount of NiAl compound increased. When the Al content increased to 12 wt.%, the interface between austenite and NiAl compound and austenitic internal started to precipitate k-carbide phase. In situ tensile results also showed that as the content of Al increased, the alloy elongation decreased gradually, and the tensile strength first increased and then decreased. When the Al content was up to 11 wt.%, the elongation and tensile strength were 2.6% and 702.5 MPa, respectively; the results of in situ tensile dynamic observations show that during the process of stretching, austenite deformed first, and crack initiation mainly occurred at the interface between austenite and NiAl compound, and propagated along the interface, resulting in fracture of the alloy.

In-situ EBSD study of the degradation behavior in a type 316 Austenitic Stainless Steel during plastic deformation

2021 ◽  
pp. 030932472098493
Author(s):  
Xiao Wang ◽  
Yuetao Zhang ◽  
Huaying Li ◽  
Ming-yu Huang
Keyword(s):  
Plastic Deformation ◽  
Stainless Steel ◽  
Austenitic Stainless Steel ◽  
Tensile Deformation ◽  
Target Surface ◽  
Local Orientation ◽  
Deformation Degree ◽  
Band Contrast

Type 316 steels have been heavily utilized as the structural material in many construction equipment and infrastructures. This paper reports the characterization of degradation in 316 austenitic stainless steel during the plastic deformation. The in-situ EBSD results revealed that, with the increase of plastic strain, the band contrast (BC) value progressively decreased in both grain and grain boundaries, and the target surface becomes uneven after the plastic tensile, which indicates that the increase of surface roughness. Meanwhile, the KAM and ρGND values are low in the origin specimen but increased significantly after the in-situ tensile. The results indicated that the KAM and ρGND are closely related to the deformation degree of the materials, which can be used as the indicator for assessing the degradation of 316 steel. Besides, the re-orientation of grain occurred after the tensile deformation, which can be recognized from the lattice orientation and local orientation maps.

Experimental study on tensile deformation process of graphitized high carbon steel sheet

2021 ◽  
Vol 4 ◽  
pp. 74-80
Author(s):  
Zhang Yong Jun ◽  
◽  
Li Xin Peng ◽  
Wang Jiu Hua ◽  
Han Jing Tao ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
Carbon Steel ◽  
Steel Sheet ◽  
Tensile Deformation ◽  
High Carbon Steel ◽  
Ferrite Matrix ◽  
High Carbon ◽  
Graphite Inclusion ◽  
Carbon Steel Sheet

As the object for the study, graphitized high-carbon steel sheet with a carbon content of 0.66 % was used, the tensile test of this sheet using a universal testing (breaking) machine was performed; as well as in-situ observation of the microstructure in the process of tensile deformation of this sheet using in-situ technology of scanning electron microscopy (SEM) was made. The test results show that the main mechanical properties in different directions of tested graphitized high-carbon steel sheet are relatively the same, that is, for a tensile sample of different directions, the ratio of the yield strength σ0,2 to the tensile strength σв is approximately 0.73; the strain hardening index n is approximately 0.24; the plastic deformation coefficient r is approximately 0.83. This indicates that this sheet did not exhibit significant anisotropy. In the process of tensile, deformation of the specimen is mainly developed from local plastic deformation of the graphite inclusions to the total deformation in the deformation zone of the sample; with the increase of displacement, micro-gap between the graphite inclusion and ferrite grain along the direction of the axis of tensile gradually formed and propagated along the direction perpendicular to the axis of tensile; number of slip lines in the ferrite matrix gradually increased, and the distance between them gradually decreases; when the sample breaks, in the fracture large dimple with the core of graphite inclusion and small dimples in the ferrite appears. And the ferrite matrix near the fracture is covered with slip lines, this shows that the ferritic matrix underwent severe plastic deformation before breaking.

scholarly journals In situ neutron diffraction under tensile deformation for patented pearlite steels

2004 ◽  
Vol 2004 (0) ◽  
pp. 89-90
Author(s):  
Tomoya Shinozaki ◽  
Satoshi Morooka ◽  
Tetsuya Suzuki ◽  
Yo Tomota
Keyword(s):  
Neutron Diffraction ◽  
Tensile Deformation ◽  
In Situ Neutron Diffraction

In situ transmission electron microscope measurements of solid Al-solid Pb and solid Al-liquid Pb surface-energy anisotropy in rapidly solidified Al-5% Pb (by mass)

1987 ◽  
Vol 414 (1847) ◽  
pp. 499-507 ◽  
Keyword(s):  
Electron Microscope ◽  
Melting Point ◽  
Surface Energy ◽  
Transmission Electron Microscope ◽  
Room Temperature ◽  
Transmission Electron ◽  
Increasing Temperature ◽  
Rapidly Solidified ◽  
Al Matrix

Alloys of Al-5% Pb and Al-5% Pb-0.5% Si (by mass) have been manufactured by rapid solidification and then examined by transmission electron microscopy. The rapidly solidified alloy microstructures consist of 5-60 nm Pb particles embedded in an Al matrix. The Pb particles have a cube-cube orientation relation with the Al matrix, and are cub-octahedral in shape, bounded by {100} Al, Pb and {111} Al, Pb facets. The equilibrium Pb particle shape and therefore the anisotropy of solid Al-solid Pb and solid Al-liquid Pb surface energies have been monitored by in situ heating in the transmission electron microscope over the temperature range between room temperature and 550°C. The ani­sotropy of solid Al-solid Pb surface energy is constant between room temperature and the Pb melting point, with a {100} Al, Pb surface energy about 14% greater than the {111} Al, Pb surface energy, in good agreement with geometric near-neighbour bond energy calculations. The {100} AI, Pb facet disappears when the Pb particles melt, and the anisotropy of solid Al-liquid Pb surface energy decreases gradually with increasing temperature above the Pb melting point, until the Pb particles become spherical at about 550°C.

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