Transmission electron microscopy of magnetic minerals

1978 ◽  
Vol 36 (1) ◽  
pp. 482-483
Author(s):  
P.P.K. Smith
Keyword(s):  
Critical Size ◽  
Magnetic State ◽  
Magnetic Domain ◽  
Continental Drift ◽  
Axial Ratio ◽  
Igneous Rocks ◽  
Interacting Particles ◽  
Magnetic Minerals ◽  
The Earth ◽  
Transmission Electron

The study of palaeomagnetism has had a great impact on the earth sciences, providing the first conclusive proof that continental drift has occurred. Although it is generally accepted that the primary magnetisation of basic igneous rocks is a thermal remanent magnetisation (TRM) carried by opaque iron-titanium oxide minerals, particularly those of the magnetite-ulvospinel series, there is still some doubt as to the exact magnetic state of the grains responsible for this palaeomagnetic TRM. The great stability of the TRM in many igneous rocks suggests a population of non-interacting particles, each consisting of a single magnetic domain, but it has been argued that the grain size of magnetic minerals in rocks is much greater than the critical size for this behaviour. For magnetite this critical size is about 0. 05 μm for equidimensional particles, rising to about 1 μm for elongated grains with an axial ratio of 10 : 1 (Evans, 1972). Thus single-domain particles would not be detected by conventional (optical) petrographic techniques.

The direct determination of magnetic domain wall profiles using a split detector STEM

1978 ◽  
Vol 36 (1) ◽  
pp. 466-467
Author(s):  
J.N. Chapman ◽  
P.E. Batson ◽  
E.M. Waddell ◽  
R.P. Ferrier
Keyword(s):  
Electron Microscope ◽  
Domain Wall ◽  
Transmission Electron Microscope ◽  
Domain Walls ◽  
Photographic Plate ◽  
Magnetic Domain ◽  
Direct Determination ◽  
Quantitative Information ◽  
Scanning Transmission Electron Microscope ◽  
Transmission Electron

By far the most commonly used mode of Lorentz microscopy in the examination of ferromagnetic thin films is the Fresnel or defocus mode. Use of this mode in the conventional transmission electron microscope (CTEM) is straightforward and immediately reveals the existence of all domain walls present. However, if such quantitative information as the domain wall profile is required, the technique suffers from several disadvantages. These include the inability to directly observe fine image detail on the viewing screen because of the stringent illumination coherence requirements, the difficulty of accurately translating part of a photographic plate into quantitative electron intensity data, and, perhaps most severe, the difficulty of interpreting this data. One solution to the first-named problem is to use a CTEM equipped with a field emission gun (FEG) (Inoue, Harada and Yamamoto 1977) whilst a second is to use the equivalent mode of image formation in a scanning transmission electron microscope (STEM) (Chapman, Batson, Waddell, Ferrier and Craven 1977), a technique which largely overcomes the second-named problem as well.

Magnetic Material Observation Assembly for Tem with a Eucentric Goniometer

1976 ◽  
Vol 34 ◽  
pp. 540-541
Author(s):  
K. Shi rota ◽  
A. Yonezawa ◽  
K. Shibatomi ◽  
T. Yanaka
Keyword(s):  
Magnetic Material ◽  
Electron Microscope ◽  
Magnetic Domain ◽  
Objective Lens ◽  
Magnetic Domains ◽  
Lorentz Microscopy ◽  
Transmission Electron ◽  
Correction Of Astigmatism ◽  
Single Orientation ◽  
Conventional Transmission Electron Microscope

As is well known, it is not so easy to operate a conventional transmission electron microscope for observation of magnetic materials. The reason is that the instrument requires re-alignment of the axis and re-correction of astigmatism after each specimen shift, as the lens field is greatly disturbed by the specimen. With a conventional electron microscope, furthermore, it is impossible to observe magnetic domains, because the specimen is magnetized to single orientation by the lens field. The above mentioned facts are due to the specimen usually being in the lens field. Thus, special techniques or systems are usually required for magnetic material observation (especially magnetic domain observation), for example, the technique to switch off the objective lens current and Lorentz microscopy. But these cannot give high image quality and wide magnification range, and furthermore Lorentz microscopy is very complicated.

scholarly journals Reductive dissolution of biogenic magnetite

2020 ◽  
Vol 72 (1) ◽  
Author(s):  
Toshitsugu Yamazaki
Keyword(s):  
Japan Sea ◽  
Depth Interval ◽  
Reductive Dissolution ◽  
Magnetic Minerals ◽  
Specific Chemical ◽  
Biogenic Magnetite ◽  
Transmission Electron ◽  
Dissolution Zone ◽  
Central Ridge ◽  
Redox Boundary

Abstract Reductive dissolution of magnetite is known to occur below the Fe-redox boundary in sediments. In this study, detailed processes associated with biogenic magnetite dissolution are documented. A sediment core from the Japan Sea was used for this purpose, in which reductive dissolution of magnetic minerals is known to start at depths of about 1.15 m and is mostly complete within a depth interval of about 0.35 m. Using first-order reversal curve diagrams, preferential dissolution of biogenic magnetite within this interval is estimated from the observation that a narrow peak that extends along the coercivity axis (central ridge), which is indicative of biogenic magnetite, diminishes downcore. Transmission electron microscopy is used to demonstrate that the sediments contain three magnetofossil morpho-types: octahedra, hexagonal prisms, and bullet-shaped forms. Within the reductive dissolution zone, partially etched crystals are commonly observed. With progressive dissolution, the proportion of bullet-shaped magnetofossils decreases, whereas hexagonal prisms become more dominant. This observation can be explained by the differences in resistance to dissolution among crystal planes of magnetite and the differences in surface area to volume ratios. Magnetofossil morphology may reflect the preference of magnetotactic bacterial lineages for inhabiting specific chemical environments in sediments. However, it could also reflect alteration of the original morphological compositions during reductive diagenesis, which should be considered when using magnetofossil morphology as a paleoenvironmental proxy.

Uncertainty Estimation for Magnetic Maps

2021 ◽  
Author(s):  
Richard Saltus ◽  
Arnaud Chulliat ◽  
Brian Meyer ◽  
Christopher Amante
Keyword(s):  
Local Level ◽  
Uncertainty Estimation ◽  
Measured Data ◽  
Magnetic Minerals ◽  
Geochemical Environment ◽  
The Earth ◽  
Uncertainty Estimates ◽  
Wide Range ◽  
Machine Learning Applications ◽  
Map Data

<p>Magnetic maps depict spatial variations in the Earth’s magnetic field.  These variations occur at a wide range of scales and are produced via a variety of physical processes related to factors including structure and evolution of the Earth’s core field and the geologic distribution of magnetic minerals in the lithosphere.  Mankind has produced magnetic maps for 100’s of years with increasing fidelity and accuracy and there is a general understanding (particularly among the geophysicists who produce and use these maps) of the approximate level of resolution and accuracy of these maps.  However, few magnetic maps, or the digital grids that typically underpin these maps, have been produced with accompanying uncertainty quantification.  When uncertainty is addressed, it is typically a statistical representation at the grid or survey level (e.g., +- 10 nT overall uncertainty based on line crossings for a modern airborne survey) and not at the cell by cell local level.</p><p>As magnetic map data are increasingly used in complex inversions and in combination with other data or constraints (including in machine learning applications), it is increasingly important to have a handle on the uncertainties in these data.  An example of an application with need for detailed uncertainty estimation is the use of magnetic map information for alternative navigation.  In this application data from an onboard magnetometer is compared with previously mapped (or modeled) magnetic variations.  The uncertainty of this previously mapped information has immediate implications for the potential accuracy of navigation.</p><p>We are exploring the factors contributing to magnetic map uncertainty and producing uncertainty estimates for testing using new data collection in previously mapped (or modeled) map areas.  These factors include (but are likely not limited to) vintage and type of measured data, spatial distribution of measured data, expectation of magnetic variability (e.g., geologic or geochemical environment), statistics of redundant measurement, and spatial scale/resolution of the magnetic map or model.  The purpose of this talk is to discuss the overall issue and our initial results and solicit feedback and ideas from the interpretation community.</p>

scholarly journals Geometrical Characterisation of the Mamfe Basin, Cameroon, from the Earth, Gravitational Model (EGM 2008)

2018 ◽  
Vol 7 (1) ◽  
pp. 94
Author(s):  
Anatole Eugene Djieto Lordon ◽  
Mbohlieu YOSSA ◽  
Christopher M Agyingi ◽  
Yves Shandini ◽  
Thierry Stephane Kuisseu
Keyword(s):  
Average Length ◽  
Gravity Data ◽  
Bouguer Anomaly ◽  
Igneous Rocks ◽  
Average Depth ◽  
The Earth ◽  
Gravitational Model ◽  
Petroleum Generation ◽  
Anomaly Map ◽  
Bouguer Anomaly Map

Gravimetric studies using the ETOPO1-corrected high resolution satellite-based EGM2008 gravity data was used to define the surface extent, depth to basement and shape of the Mamfe basin. The Bouguer anomaly map was produced in Surfer 11.0. The Fast Fourier Transformed data was analyzed by spectral analysis to remove the effect of the regional bodies in the study area. The residual anomaly map obtained was compared with the known geology of the study area, and this showed that the gravity highs correspond to the metamorphic and igneous rocks while the gravity lows match with Cretaceous sediments. Three profiles were drawn on the residual anomaly map along which 2D models of the Mamfe basin were drawn. The modeling was completed in Grav2dc v2.06 software which uses the Talwini’s algorithm and the resulting models gave the depth to basement and the shape of the basement along the profiles. After processing and interpretation, it was deduced that the Mamfe basin has an average length and width of 77.6 km and 29.2 km respectively, an average depth to basement of 5 km and an overall U-shape basement. These dimensions (especially the depth) theoretically create the depth and temperature conditions for petroleum generation. 

scholarly journals Gravitational differentiation in the regimes from stokes settling to Rayleigh–Raylor flows

2019 ◽  
pp. 15-30
Author(s):  
V. P. Trubitsyn
Keyword(s):  
Viscous Fluid ◽  
Interacting Particles ◽  
Small Particles ◽  
Continuous Transition ◽  
New Approach ◽  
Earth's Core ◽  
The Core ◽  
The Earth ◽  
Large Particles ◽  
Two Component

The Earth’s core was formed under gravitational differentiation in the course of the separation of iron and silicates. Most of the iron has gone into the core as early as when the Earth was growing. However, iron continued to precipitate even during the subsequent partial solidification which developed from the bottom upwards. At the different stages and in the different layers of the mantle, iron was deposited in different regimes. In this paper, the mechanisms of the deposition of a cloud of heavy interacting particles (or drops) in a viscous fluid are considered. A new approach suitable for analytical and numerical tracing the changes in the structure of the flows in a two-component suspension under continuous transition from the Stokessettling (for the case of a cloud of large particles) to the Rayleigh–Taylor flows and heavy diapirs (for the case of a cloud of small particles) is suggested. It is numerically and analytically shown that the both regimes are the different limiting cases of the sedimentation convection in suspensions.

scholarly journals Synthesis and ESR Study of Transition from Ferromagnetism to Superparamagnetism in La0.8Sr0.2MnO3 Nanomanganite

2020 ◽  
Author(s):  
Mondher Yahya ◽  
Faouzi Hosni ◽  
Ahmed Hichem Hamzaoui
Keyword(s):  
Crystallite Size ◽  
Magnetic State ◽  
Resonance Field ◽  
Magnetic Domain ◽  
Single Domain ◽  
State Transitions ◽  
G Factor ◽  
Domain Structures ◽  
Crystallite Sizes ◽  
Superparamagnetic State

Electron spin resonance (ESR) spectroscopy was used to determine the magnetic state transitions of nanocrystalline La0.8Sr0.2MnO3 at room temperature, as a function of crystallite size. Ferromagnetic nanoparticles having an average crystallite size ranging from 9 to 57 nm are prepared by adopting the autocombustion method with two-step synthesis process. Significant changes of the ESR spectra parameters, such as the line shape, resonance field (Hr), g-factor, linewidth (∆Hpp), and the low-field microwave absorption (LFMA) signal, are indicative of the change in magnetic domain structures from superparamagnetism to single-domain and multi-domain ferromagnetism by increase in the crystallite size. Samples with crystallite sizes less than 24.5 nm are in a superparamagnetic state. Between 24.5 and 32 nm, they are formed by a single-domain ferromagnetic. The multi-domain state arises for higher sizes. In superparamagnetic region, the value of g-factor is practically constant suggesting that the magnetic core size is invariant with decreasing crystallite size. This contradictory observation with the core-shell model was explained by the phenomenon of phase separation that leads to the formation of a new magnetic state that we called multicore superparamagnetic state.

Partial Castastrophism and Pick & Choose Empiricism: The Science of “Creationist” Geology

1984 ◽  
Vol 1 ◽  
pp. 50-65
Author(s):  
William J. Frazier
Keyword(s):  
Magnetic Field ◽  
Sedimentary Rocks ◽  
Decay Rates ◽  
Igneous Rocks ◽  
Earth’S Magnetic Field ◽  
Organic Evolution ◽  
The Earth ◽  
Scientific Principles ◽  
Earth's Magnetic Field ◽  
Repeated Use

“Scientific creationists” have created their own version of geology in order to defend their axiomatic insistance on a young Earth. To “prove” the Earth's youth, they cite (among other things) measured decay-rates of Earth's magnetic field and concentrations of elements in seawater. They also state that all plutons are quick frozen, that plutonic igneous rocks bear no relation to modern volcanism, and that all sedimentary rocks must be interpreted in terms of a “global hydrologic singularity,” i.e. Noah's Flood.Having explicitly denied uniformitarianism and embraced catastrophism, “Creationists” renege by using uniformitarian reasoning over and again. They practice “pick & choose” empiricism by citing only those data which seem to support their case. “Creationists” even choose when and if to apply scientific principles, e.g. their use of thermodynamics to “disprove” organic evolution while ignoring thermodynamics' implications for magma cooling and metamorphism.The methods of “Creationism” are clearly intended not to increase knowledge of the Earth but to delude the scientifically unsophisticated. Thus, “Creationism” can hardly be considered a science. Further, its repeated use of fallacious thinking brands “Creationism” as hopelessly illogical and its disingenuous statements and tactics disqualify it from even the ranks of nonempirical epistemological systems.

scholarly journals III. A General View of the Phenomena displayed in the neighbourhood of Edinburgh by the Igneous Rocks, in their relations with the Secondary Strata; with reference to a more particular description of the Section which has been exposed to view on the south side of the Castle Hill

1835 ◽  
Vol 13 (1) ◽  
pp. 39-45
Author(s):  
Greenock
Keyword(s):  
Large Volume ◽  
Igneous Rocks ◽  
General View ◽  
The South ◽  
Alluvial Deposits ◽  
True Nature ◽  
South Side ◽  
The Earth ◽  
Igneous Origin ◽  
Great Pressure

The country in which Edinburgh is situated has no great elevation above the level of the sea, presenting a gently undulating surface, except where hills of igneous origin, in groups, or perfectly insulated, rise abruptly through the strata, which consist of the sandstones and shales of the coal-formation, with occasional beds of limestone, which they overlie, and this country is more or less covered by old and new alluvial deposits.The views suggested by these hills to the penetrating genius of Hutton, who may be justly considered the founder of modern geology, first led to the knowledge of the true nature and origin of the trap-rocks. Their analogy to those produced by existing volcanoes, and the phenomena observed in their relations with the secondary strata, leave no doubt as to their having been poured out from the interior of the earth in a fluid or viscid state, through fissures in the strata occasioned by subterranean convulsions—not, however, in the open air, like currents of lava from recent craters, but in sheets or masses at the bottom of the sea, their cooling and consolidation having evidently been slow and gradual, under great pressure, such as might be produced by a large volume of superincumbent water, as was ably illus trated by the experiments of the late Sir James Hall; or by their having been originally formed as dykes, at considerable depths, either below or among the strata.

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