α-MoO3/polyaniline composite for effective scavenging of Rhodamine B, Congo red and textile dye effluent

RSC Advances ◽  
2016 ◽  
Vol 6 (34) ◽  
pp. 28871-28886 ◽  
Author(s):  
S. Dhanavel ◽  
E. A. K. Nivethaa ◽  
K. Dhanapal ◽  
V. K. Gupta ◽  
V. Narayanan ◽  
...  

Polyaniline modified MoO3 composites were synthesized via a chemical oxidative polymerization method and employed as a novel adsorbent for Rhodamine B (RhB), Congo red (CR) and textile dye effluent.

Author(s):  
R. K. Shukla ◽  
Susheel Kumar Singh ◽  
Akhilesh Tripathi

Polyaniline (PANI) is synthesized by chemical oxidative polymerization method. The, characterization were made using XRD (X-ray diffraction), FT-IR (Fourier transform spectroscopy), UV -vis (ultra-violet visible spectrophotometer) technique which confirms the synthesis of the Polyaniline. The surface morphology of Polyaniline was studied with scanning electron microscope (SEM).


2019 ◽  
Vol 16 (1) ◽  
pp. 55-63
Author(s):  
Naglaa Shahin ◽  
Reham Kamal Abd El Hamid

Polyvinyl alcohol- polypyrrole (PVA-PPy) nanocomposites with metal chlorides (FeCl3, NiCl2, CuCl2 and ZnCl2) have been synthesized by chemical oxidative polymerization method. These synthesized nanocomposites are characterized by using FTIR, X-ray diffraction, Transition electron microscope (TEM) and Conductivity measurement. TEM exhibit that all of the composites have uniform sizes and morphologies.  The diameter of PVA/PPy nanocompsite is 58nm when the metals added to the PVA/PPy the diameters becomes smaller. The variation of electrical conductivity (log ?) with 1000/T for PVA/PPy nanocomposite with metal chlorides revealed that the increase in conductivity s at temperature (393K) with added metals can be attributed to the creation of induced charge carriers in PVA/PPy matrix


2018 ◽  
Vol 1 (1) ◽  
pp. 9-20 ◽  
Author(s):  
M Haridevi ◽  
S Prabu ◽  
M Lakshmi Devi ◽  
E Bhakya Lakshmi ◽  
K Mohanraj ◽  
...  

The Co3O4-PANI nanocomposites has been synthesized by chemical oxidative polymerization method using cobalt chloride. It is a simple and low cost method to prepare nanocomposite. The prepared samples were characterized by using Scanning Electron Microscope (SEM), X-ray diffraction (XRD) and Fourier Transform Spectroscopy (FTIR) to get surface morphology, idea of getting particles of nano sized range so that further characterization can be done, to study the net surface charge of the nanoparticles by Zeta potential, photoluminescence of synthesized nanocomposite and measure photocatalytic activity of the synthesized nanomaterials was successfully tested for photo degradation of dye under UV light were studied


Author(s):  
Sang Nguyen Xuan

Polypyrrole (PPy) nanocomposites reinforced with zinc oxide (ZnO) nanorod and nano flower were fabricated by chemical oxidative polymerization method using an ammonium per-sulphate (APS, (NH4)2S2O8) as an oxidizing agent. The polymer nanocomposite were characterized by X-ray diffractometer (XRD), scanning electron microscopy (SEM), and Fourier transform infrared (FTIR). The results were compared with pure as-prepared PPy. The SEM images of the nanocomposites show homogeneous dispersion characteristics and different morphologies of ZnO structures such as rod and flower-like shapes.  In the FTIR spectra, composite samples showed characteristic peaks of PPy shifted to higher positions confirmed the interfacial interactions between ZnO and PPy matrix.


2020 ◽  
Vol 3 (2) ◽  
Author(s):  
Dhachanamoorthi N ◽  
Padmapriya B

Scientific zone has a great attention to the polyaniline (PANI) nanomaterials which is an organic, conductive and a conjugated polymer. It has variety of applications such as in batteries, microelectronics displays, antistatic coatings, electromagnetic shielding materials and actuators [1]. PANI was synthesized by using chemical oxidative polymerization method. The preparation process carried out by the main reagent aniline (C6H7N) with the ammonium peroxydisulpate (APS) ((NH4)2S2O8) which act as an oxidant and hydrochloric acid (HCL) as a dopant in an ambient temperature. The synthesized polymer materials are annealed at different temperatures such as 200°C,300°C and 400°C. After annealed treatment, the weight percentage of polymer material are changed were decreases with increase the temperature of pure PANI (0.441g),200°C(0.172g), 300°C(0.147g), 400°C (0.105g). Then the obtained polymer materials are characterized by FTIR, UV-Visible, Particle size analysis (PSA) and Antibacterial analysis. FTIR is used to determine the functional group of polymer nanomaterials. UVVisible exhibits the quantitative information about the polymer nanomaterials by using its band gap. The size of the individual particles and the size distribution range of the respective samples are determined by the Particle Size Analyzer (PSA). Antibacterial activity is used to find the polymer nanomaterials which kills bacteria, or bacteriostatic,which slow down the growth of bacteria. These profiling techniques are used to find the properties like functional group, quantitative information, particle size, antibacterial activity of respective polyaniline nanomaterial samples.


2018 ◽  
Vol 42 (9) ◽  
pp. 6918-6931 ◽  
Author(s):  
Madhurima Das ◽  
Saptarshi Ghosh ◽  
Somenath Roy

This article describes the non-covalent functionalization of multiwall carbon nanotubes (MWCNTs) with polycarbazole (PCz) via an in situ chemical oxidative polymerization method and subsequent fabrication of resistive humidity sensors.


RSC Advances ◽  
2015 ◽  
Vol 5 (84) ◽  
pp. 68964-68971 ◽  
Author(s):  
D. K. Bandgar ◽  
S. T. Navale ◽  
M. Naushad ◽  
R. S. Mane ◽  
F. J. Stadler ◽  
...  

We report for the first time a room temperature smart NH3sensor based on PAni–Fe2O3nanocomposite loading on flexible PET substrate byin situchemical oxidative polymerization method.


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