scholarly journals Effects of crystalline growth on structural and luminescence properties of Ca(10−3x)Eu2x(PO4)6F2 nanoparticles fabricated by using a microwave driven hydrothermal process

CrystEngComm ◽  
2017 ◽  
Vol 19 (46) ◽  
pp. 6936-6949 ◽  
Author(s):  
Katarzyna Zawisza ◽  
Paulina Sobierajska ◽  
Guillaume Renaudin ◽  
Jean-Marie Nedelec ◽  
Rafal J. Wiglusz

The structural and luminescence properties of Eu3+ doped nanofluorapatites obtained by hydrothermal method were investigated.

CrystEngComm ◽  
2018 ◽  
Vol 20 (43) ◽  
pp. 7030-7030
Author(s):  
Katarzyna Zawisza ◽  
Paulina Sobierajska ◽  
Guillaume Renaudin ◽  
Jean-Marie Nedelec ◽  
Rafal J. Wiglusz

Correction for ‘Effects of crystalline growth on structural and luminescence properties of Ca(10−3x)Eu2x(PO4)6F2 nanoparticles fabricated by using a microwave driven hydrothermal process’ by Katarzyna Zawisza et al., CrystEngComm, 2017, 19, 6936–6949.


2006 ◽  
Vol 24 (6) ◽  
pp. 757-760 ◽  
Author(s):  
Yang Kuisheng ◽  
Li Yan ◽  
Yu Chaoyi ◽  
Lu Liping ◽  
Ye Chanhua ◽  
...  

Author(s):  
Zhengyang Zhang ◽  
Jinkai Li ◽  
Wenzhi Wang ◽  
Weilin Zhao ◽  
Zongming Liu

2018 ◽  
Vol 29 (17) ◽  
pp. 15068-15068
Author(s):  
Xiaohui Zhang ◽  
Haiming Zhang ◽  
Lijuan Wei ◽  
Yue Zhang ◽  
Biao Zhang

2018 ◽  
Vol 16 (2) ◽  
pp. 138 ◽  
Author(s):  
Yulius Dala Ngapa ◽  
Sri Sugiarti ◽  
Zaenal Abidin

A synthetic zeolite was produced from natural zeolite from Ende-Nusa Tenggara Timur (NTT) by hydrothermal method. This study aims to produce synthetic zeolite from Ende natural zeolite to remove cation dye through the adsorption process. Temperature of crystal formation (ageing) was performed at 60 °C for 6 h and hydrothermal process was at 100 °C for 24 h. The natural zeolite produced synthetic NaP1 and synthetic Faujasite. Based on the research results, the synthesis of zeolite by the hydrothermal method can enhance the adsorption capacity and Cation Exchange Capacity (CEC). The adsorption capacity in the natural zeolites of type ZG, ZL and ZC before the hydrothermal process were 17.289, 17.276, and 16.483 mg/g, respectively, and after hydrothermal they increased to 37.398, 37.369 and 37.362 mg/g, respectively. In addition, the CEC increased from 84.154, 81.042, and 77.474 cmol/kg, respectively, to 244.063, 216.354, and 211.432 cmol/kg, respectively. The Langmuir model most closely matched the isothermal adsorption equilibrium process.


2012 ◽  
Vol 174-177 ◽  
pp. 592-595
Author(s):  
Lin Lin Yang ◽  
Yong Gang Wang ◽  
Yu Jiang Wang ◽  
Xiao Feng Wang

The organization of nanostructures across extended length scales is a key challenge in the design of integrated materials with advanced functions. PbZr0.52Ti0.48O3multilayer disks which were constructed by oriented rectangle nanoparticles were easily prepared by a simple surfactant-free hydrothermal process. The as-prepared powders were characterized by X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The results indicated that the as-prepared PZT disks were constructed by self-assembly of rectangle nanoparticles by a perfect manner. The formation mechanism of the products was discussed.


2013 ◽  
Vol 575-576 ◽  
pp. 45-49
Author(s):  
Ai Qing Wu ◽  
Xin Zuo Fang ◽  
Xin Hua Lin ◽  
Huan Qin Wang ◽  
Ying Xian Wang ◽  
...  

Rutile Ti1xSnxO2(0.2x<1) solid solutions had been prepared using a sol-hydrothermal method, which combined the conventional sol-gel process with hydrothermal method. Hybrid alkoxides of Ti4+and Sn4+were used as precursors in the sol-gel process and Sn4+served as crystal-inducing agent during the formation of rutile crystal lattice in the hydrothermal process at 200°C. The microstructures and morphologies of nanoparticles were detected with XRD and TEM. Rutile Ti1xSnxO2solid solutions nanoparticles with well-distributed crystallite sizes about 10nm were obtained with Sn4+content above 20mol% without any high temperature calcination. The oxygen sensitivity properties of Ti1xSnxO2solid solutions had also been investigated. It is proved Ti1xSnxO2solid solutions exhibited higher oxygen responses than single TiO2or SnO2. A typical sample of Ti0.5Sn0.5O2presented the best sensitivity is approximately 6 under 400°C.


2015 ◽  
Vol 41 (5) ◽  
pp. 6683-6686 ◽  
Author(s):  
Xiaolei Shi ◽  
Yun Liu ◽  
Jin Zhang ◽  
Kun Zhang ◽  
Jinyang Li ◽  
...  

2014 ◽  
Vol 597 ◽  
pp. 109-112
Author(s):  
Jia Yue Sun ◽  
Bing Xue ◽  
Qiu Mei Di ◽  
Qi Guang Xu ◽  
Liu Han

Yb3+, Tm3+ co-doped Gd6MoO12 phosphors were prepared by the hydrothermal method. After tuning the PH value and EDTA, phosphors present different morphologies including hexagonal prisms, spindles, and spheres. Under 980nm excitation, the upconversion luminescence properties of the as-prepared phosphors are studied based on changing the synthesis condition. It is found that usage of EDTA and pH changing both play crucial key in the formation of morphology. Pumping power on the UC luminescence properties and level diagram mechanism of Gd6MoO12:Yb3+/Tm3+phosphor have also been discussed.


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