Nondestructive measurements of the resistivity of thin conductive films and the dielectric constant of thin substrates using an open-ended coaxial line

1992 ◽  
Vol 139 (6) ◽  
pp. 500 ◽  
Author(s):  
Yansheng Xu ◽  
R.G. Bosisio
1961 ◽  
Vol 39 (3) ◽  
pp. 526-534 ◽  
Author(s):  
B. D. Ripley ◽  
R. McIntosh

The complex dielectric constants of three compositions of trimethylpentane and nitrobenzene have been measured as a function of temperature for a range near the consolute temperature. The frequency employed was 3300 Mc/sec. The experimental procedure involved the study of the standing wave established in a coaxial line. The chemical systems showed maxima in both the real and imaginary parts of the complex dielectric constant at temperatures above those at which phase separation occurs. The finding of Semenchenko and Azimov is thus confirmed. A discussion of the validity of applying thermodynamic formulae to dielectrics showing loss is given and some qualitative remarks are offered concerning the change of the systems as they are cooled. These remarks are based upon the effect of the applied field upon the entropy of the solutions.


1985 ◽  
Vol 25 (04) ◽  
pp. 502-514 ◽  
Author(s):  
Liang C. Shen

Abstract This paper describes an automated laboratory system that can measure accurately the dielectric properties of core samples in the ultrahigh-frequency properties of core samples in the ultrahigh-frequency (UHF) range. The system consists of a precision coaxial-line sample holder, a network analyzer, a plotter, a printer, and a desk computer. The computer is for measurement control, data acquisition, and data analysis. A new method is developed to measure and to compensate for the error of the network analyzer system. This method uses a brass sample and does not require standard terminations. A procedure for core sample preparation is also recommended to ensure accuracy of the data. Introduction The electromagnetic propagation tool (EPT) is a relatively new wireline sonde developed by Schlumberger for detection and quantification of hydrocarbon. It is operated at 1.1 GHz, which is in the UHF band of the electromagnetic spectrum. The EPT sonde measures the dielectric constant of the formation. Because water has a much higher dielectric constant (about 80 units) than oil (about 2 units) and gas (about 1 unit), the EPT sonde can distinguish hydrocarbon-bearing zones from the water-bearing zones even when the formation water is fresh. The dielectric constant of water at UHF is not very sensitive to salinity. Consequently, EPT is particularly useful in situations where the formation water resistivity is variable or unknown, as a result, for example, of water, steam, or chemical flooding. The EPT log displays the travel time and the rate of attenuation of the electromagnetic wave in the formation. From these data, the calculated complex dielectric constant of the formation may be calculated. This complex dielectric constant is related to water saturation, Sw, by an empirical formula called the complex refractive index method (CRIM): ............................(1) where = porosity, = dielectric constant of the water in the rock, = dielectric constant of oil or gas, and = dielectric constant of the rock grain. To verify the validity of the CRIM formula given by Eq. 1, a computer-controlled laboratory system has been set up to measure the dielectric constants of saturated core samples, dry core samples, and oils. The same system is now being used for routine measurements of cores for EPT log interpretation. Measurement Techniques Two basic techniques can be used to measure the complex dielectric constant of a saline-water-saturated rock at frequencies higher than 100 MHz. The first is the coaxial-line and waveguide method, and the other is the resonant-cavity method. We describe these methods and point out their advantages and disadvantages. Fig. 1 shows the configuration of the coaxial-line and waveguide method. In Figs. 1a and 1b, we see that the core sample is machined into a circular cylinder with a circular concentric hole drilled to fit the coaxial line. The line consists of an outer conductor and an inner conductor. In Fig. 1c, we see that the core sample is machined into a rectangular column to fit into a rectangular waveguide. The latter is a rectangular metal pipe without a central conductor. pipe without a central conductor. Longitudinal slots are cut along the outer conductor of the coaxial line (Fig. 1b) or on top of the rectangular waveguide (Fig. 1c) to allow a probe to be inserted partially into the region where electromagnetic fields are present. The probe travels along the length of the structure and detects the amplitude and the phase of the electromagnetic fields present in the structure. During the measurement, an electromagnetic wave of the selected frequency is sent propagating down the line or the waveguide until it encounters the core sample. Reflection occurs so that part of the wave is absorbed, and part is reflected and travels in the reverse direction. The phase and the amplitude of the reflected wave are determined by the complex dielectric constant of the sample. The reflected wave interacts with the incident wave and creates an interference pattern called the standing wave pattern. The complex dielectric constant of the core sample can be determined from the standing wave pattern recorded by the traveling probe. This method was used by Poley et al. for sandstone samples up to 1.2 GHz. It was also used by Tam to test nine dry rocks, mainly sedimentary, in the frequency range 150 to 1000 MHz. The rectangular waveguide was used by Roberts and Von Hippel to measure a variety of materials at 5 GHz. The configuration shown in Fig. 1a was used by Rau and Wharton to measure formation samples in the frequency range 500 MHz to 1.1 GHz. This arrangement calls for placing the sample at the center, rather than at the end, of a coaxial line. The amplitudes and the phases of both the reflected and the transmitted waves are recorded and are called the scattering matrix parameters. parameters. SPEJ p. 502


Author(s):  
Chunfang Song ◽  
Tian Sang ◽  
Haiying Chen ◽  
Li Zhenfeng ◽  
Li Jing

AbstractThe dielectric properties of blackberry samples with a 20.0–80.0 % w.b (web basis) moisture content were determined with a network analyzer and an open-ended coaxial-line probe over a frequency range from 5 to 3000 MHz and a temperature range from 20 to 100 °C. The results showed that the dielectric constant decreased with increasing temperature but increased with increasing moisture content; however, the loss factor increased with increasing temperature and moisture content. The dielectric constant and the loss factor decreased with increasing frequency. The penetration depth decreased with increasing temperature, frequency and moisture content. A large penetration depth at 915 MHz may provide practical large-scale dielectric drying for blackberries. The dielectric constants and loss factors for blackberry by combining the above mathematical model and temperature and moisture of the sample in the microwave drying process were used to analyze and control blackberry drying technology.


1961 ◽  
Vol 39 (3) ◽  
pp. 425-442 ◽  
Author(s):  
J. D. McCowan ◽  
R. McIntosh

The complex dielectric constant of the system Vycor glass – ethyl chloride has been measured at three temperatures in the range +11 °C to −33 °C and in the frequency range between 500 Mc sec−1 and 4000 Mc sec−1 by the use of a coaxial line. The real and imaginary parts of the dielectric constant of the adsorbate have also been evaluated. Appreciable loss in the adsorbed matter is found for small quantities adsorbed, and loss is again detected at the highest frequencies and lowest temperatures for the matter held in multilayers or condensed in capillaries. The frequency range and accuracy of measurement were not sufficient to classify the type of loss curve, but other evidence suggests that the loss for the first quantities adsorbed will turn out to be that for rotational oscillators. In general earlier observations of this system are confirmed and extended.


1993 ◽  
Vol 64 (6) ◽  
pp. 1622-1626 ◽  
Author(s):  
G. Q. Jiang ◽  
W. H. Wong ◽  
E. Y. Raskovich ◽  
W. G. Clark ◽  
W. A. Hines ◽  
...  

Geophysics ◽  
1984 ◽  
Vol 49 (1) ◽  
pp. 92-92
Author(s):  
Ramesh P. Singh

Huang and Shen presented an interesting paper pointing out a correction due to the presence of unavoidable gaps between the sample and sample holder (coaxial line) on the measurement of dielectric constant and conductivity of core rock samples. Huang and Shen’s following statement on p. 206 is misleading: “Thus low‐frequency tools for measuring the electric properties of a formation can measure the conductivity accurately but not the dielectric constant.” At low frequency below 10 MHz, displacement current is almost negligible for most of the Earth’s materials. Therefore, the question of the dielectric constant with the low‐frequency tools does not arise.


2021 ◽  
Vol 1 (1) ◽  
pp. 4-12
Author(s):  
A. R. Nasybullin ◽  
O. G. Morozov ◽  
R. V. Farkhutdinov ◽  
T. M. Ishkaev

Bragg microwave structures in a coaxial line have found application as converting elements in devices for dielectric control of liquid and bulk medias. A feature of the measuring conversion of the complex dielectric constant in coaxial structures is the introduction of the substance under study into the inner space of the line. The latter circumstance imposes certain restrictions on the design of the external conductor for express control. In this regard, the consideration of half-open coaxial lines based on an external conductor in the form of longitudinal conducting rods is an urgent problem. The article proposes a method for calculating the wave impedance of a half-open coaxial line using a numerical calculation of electromagnetic fields. Based on the results of modeling Bragg microwave structures in a half-open coaxial line, recommendations are made for the construction of conversion elements based on them.


1993 ◽  
Vol 64 (6) ◽  
pp. 1614-1621 ◽  
Author(s):  
G. Q. Jiang ◽  
W. H. Wong ◽  
E. Y. Raskovich ◽  
W. G. Clark ◽  
W. A. Hines ◽  
...  

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