scholarly journals Beneficiation research on a low grade linnaeite ore with hema-tite-pyrite type

2019 ◽  
Vol 136 ◽  
pp. 02008
Author(s):  
Xinfang Zhang ◽  
Qinqin Wang ◽  
Chengdong Wang ◽  
Lang Zhu ◽  
Shujie Shi ◽  
...  

Mineralogy and separation experiments were carried out for a low-grade linnaeite ore (0.052%), which belonged to limonite-hematite-pyrite type complex mineral. Under the grinding fineness of 80% -0.074 mm, linnaeite concentrate which contained cobalt grade of 0.51%, recovery rate of 80.99%, sulfur grade of 23.79%, recovery of 88.03% was obtained by closed-circuit processes of one roughing, two scaenging and one cleaning, which used sulfate acid (4500 g/t) and copper sulfate (300 g/t) as activator, so-dium silicate (1000 g/t) and CMC (30 g/t) as inhibitor, ethyl xanthate(100 g/t)and butyl xanthate (100 g/t) as collector, 2# oil (40 g/t) as forther in roughing, no agent in cleaing and first scavenging, used ethyl xan-thate(50 g/t)and butyl xanthate (50 g/t) as collector, 2# oil (20 g/t) as forther in second scavenging.

Processes ◽  
2019 ◽  
Vol 7 (8) ◽  
pp. 536 ◽  
Author(s):  
Xiao ◽  
Zhang

There is 0.032% cobalt and 0.56% sulfur in the cobalt-bearing V–Ti tailings in the Panxi Region, with the metal sulfide minerals mainly including FeS2, Fe1−xS, Co3S4, and (Fe,Co)S2, and the gangue minerals mainly including aluminosilicate minerals. The flotation process was used to recover cobalt and sulfur in the cobalt-bearing V–Ti tailings. The results showed that an optimized cobalt–sulfur concentrate with a cobalt grade of 2.08%, sulfur content of 36.12%, sulfur recovery of 85.79%, and cobalt recovery and 84.77% were obtained by flotation process of one roughing, three sweeping, and three cleaning under roughing conditions, which employed pulp pH of 8, grinding fineness of < 0.074 mm occupying 80%, flotation concentration of 30%, and dosages of butyl xanthate, copper sulfate, and pine oil of 100 g/t, 30 g/t, and 20 g/t, respectively. Optimized one sweeping, two sweeping, and three sweeping conditions used a pulp pH of 9, and dosages of butyl xanthate, copper sulfate, and pine oil of 50 g/t, 15 g/t, 10 g/t; 25 g/t, 7.5 g/t, 5 g/t; 20 g/t, 5 g/t, 5 g/t, respectively. Optimized one cleaning, two cleaning, and three cleaning condition dosages of sodium silicate of 200 g/t, 100 g/t, 50 g/t, respectively. Study of analysis and characterization of cobalt–sulfur concentrate by X-ray diffraction (XRD), automatic mineral analyzer (MLA), scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS) showed that the main minerals in cobalt–sulfur concentrate are FeS2, Co3S4 and (Fe,Co)S2, of which FeS2 and (Fe,Co)S2 accounted for 65.64% and Co3S4 for 22.64%. Gangue minerals accounted for 11.72%. The element Co in (Fe,Co)S2 is closely related to pyrite in the form of isomorphism, and the flotability difference between cobalt and pyrite is very small, which makes it difficult to separate cobalt and sulfur. Cobalt–sulfur concentrate can be used as raw material for further separation of cobalt and sulfur in smelting by pyrometallurgical or hydrometallurgical methods.


2015 ◽  
Vol 1090 ◽  
pp. 188-192
Author(s):  
Xin Zhang ◽  
Ling Yan Zhang ◽  
Yang Shuai Qiu ◽  
Xin Qu

The graphite ore from Australia is a sort of the low-grade and fine-scaled graphite ore. On the basis of the optimum rough grinding fineness, an open and a closed circuit tests were conducted which consist of one rougher, one scavenging, then four-time-regrinding and five-time-cleaning to the rough concentrate, one grinding and scavenging to the mixture of middling1~3, and the middling4~6 returned to the rougher, cleaning1 and cleaning2 respectively. Taking the kerosene, pine oil, lime as flotation reagents, the concentrate with grade improvement from 12.78% to 90.5% was achieved through the routine flotation method, as the flotation recovery rate reached to 92.46%.


2014 ◽  
Vol 490-491 ◽  
pp. 160-163
Author(s):  
Zhi Guo Zhang ◽  
Quan Jun Liu ◽  
Jin Cheng Ran

The experimental ore belongs to high-sulfur Cu-Zn poly-metallic ore, the mineral composition of ore is complex, cupriferous pyrite most are disseminated. The Cu grade of raw ore is 0.76%, Zn grade is 1.48% and S about 25.02%. on the basis of best reagent system and control flotation time, the author did closed circuit process. the results of closed circuit process as follows: the copper concentrate grade is 20.35% and recovery rate is 86.081%; the zinc concentrate grade is 54.32% and recovery rate is 84.20%.


2013 ◽  
Vol 641-642 ◽  
pp. 256-261
Author(s):  
Qing Mei Jia ◽  
Feng Jiu Li ◽  
Hui Jing Wang

This article conducts mineral processing experimental study on a certain iron tailing ore in Hebei. According to the ore characteristics, the final flowsheet of stage grinding - weak magnetic - strong magnetic - anionic reverse flotation is determined to sort the ore. Under the conditions that grinding fineness is -200 mesh accounting for 60.0%, collector is butyl xanthate and activator is copper sulfate, this test can obtain zinc concentrate that grade is 36.25% and recovery is 84.15%


2012 ◽  
Vol 524-527 ◽  
pp. 1124-1129
Author(s):  
Dan Dan Wu ◽  
Shu Ming Wen ◽  
Jian Liu ◽  
Hai Ying Shen ◽  
Shao Jun Bai

In this study, factors influencing zinc oxide flotation are investigated. These factors include the dosages of sulfidizing reagent, the pH of the regulator and the activator, the use of sodium carbonate as the pH regulator and activator, the use of copper sulfate as the activator and the use of isoamyl xanthate as the collector. All of the above factors are essential to the effective recovery of zinc oxide. Flotation using mixed collectors (isoamyl xanthogenate + dithionphosphate) showed promising results. The ratio of the mixed collectors and the addition sequence of the mixed collectors were important in attaining a true mixed collector for zinc oxide flotation. In the closed circuit experiment, these agents helped to produce a zinc concentrate with 12.41% Zn, 80.03% recovery and 17.29% Zn in the tailings. The zinc concentrate with 12.41% Zn was used as a material for hydrometallurgy to collect zinc.


2012 ◽  
Vol 581-582 ◽  
pp. 1110-1114
Author(s):  
Hong Xiao ◽  
Quan Jun Liu ◽  
Mei Guang Jiang ◽  
Jun Long Yang

The lead-zinc mine is a low grade of refractory oxide mineral. The grade of lead is 2.84%, with the oxidation rate of 90.95%.The grade of zinc is 3.223%, and with the oxidation rate of 87.9%.The grade of silver is 99.5g/t.This test used the silver-lead sulphide flotation at first, then depressing zinc oxide and floating lead oxide mineral. As a result, in silver-lead sulphide concentrate, the silver grade for 1180 g/t, lead 11.45%. Lead and silver recovery rate were 18.41% and 51.14% respectively. Lead oxide concentrate grade is 32.59%, and the silver is 518g/t. Lead and silver recovery rate were 68.34% and 29.18%. Zinc oxide concentrate grade is 32.65%, including 1.14% lead; zinc recovery rate is 80.11%.


Minerals ◽  
2018 ◽  
Vol 9 (1) ◽  
pp. 2 ◽  
Author(s):  
Haïfa Boujlel ◽  
Ghassen Daldoul ◽  
Haïfa Tlil ◽  
Radhia Souissi ◽  
Noureddine Chebbi ◽  
...  

The enrichment of the low-grade-phosphate ore of the Tozeur-Nefta deposit was investigated using scrubbing-attrition, ball grinding and anionic/cationic reverse flotation in order to separate phosphate-rich particles from their gangue. The choice of the beneficiation process was based on the petrographic, mineralogical and chemical analyses. The petrographic and mineralogical studies have revealed the abundance of phosphatic (carbonate-fluorapatite-CFA) particles) coupled with carbonates (calcite, dolomite,) and silicates (quartz, illite, kaolonite) that constitute the (endo/exo) gangue of these ores. Chemical analysis has demonstrated that the raw phosphate sample contains low amounts of P2O5 (12.0%) and MgO (4.9%) and high amounts of CaO (40.7%) and SiO2 (20.5%). Microscopic observation/counting has shown that the release mesh occurs in the 71–315 μm size. Scrubbing-attrition, grinding and reverse flotation methods were applied to the +71μm fraction. Scrubbing-attrition tests of the 71–315 μm fraction have helped to improve the P2O5 grade to 15.5%. Ball-grinding tests were used to reduce the coarse fraction +315 μm. Grounded materials were sieved to 71–315 μm and combined with the scrubbed fraction in the flotation feed. Reverse-flotation tests of the phosphate-rich fraction (71–315 μm) have helped to improve the P2O5 grade to 27.1%, with a recovery rate of 92.4%.


2013 ◽  
Vol 634-638 ◽  
pp. 3466-3471 ◽  
Author(s):  
Yi Jie Wang ◽  
Shu Ming Wen ◽  
Jian Liu ◽  
Qi Cheng Feng ◽  
Meng Yang Lv

The mineral processing flow sheet and reagent system of flotation copper minerals from a large copper-iron deposit in Yunnan were fully investigated. The results indicate that the optimum conditions for flotation of copper minerals from the material were identified as grinding fineness of 85%, dosage of CaO at 2000g/t , dosage of Na2S at 200 g/t, dosage of butyl xanthate 40g/t. Under such a condition, a copper recovery of 88.17% with a concentrate grade of 26.86% was achieved from the material using a closed circuit flow sheet of "one-stage roughing flotation, one-stage cleaning flotation and one-stage scavenging flotation.


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