scholarly journals Measurement of Spontaneous Imbibition Capillary Pressure, Saturation and Resistivity Index by Counter Current Technique at Net Reservoir Stress and Elevated Temperature

2019 ◽  
Vol 89 ◽  
pp. 02002
Author(s):  
Stefano Pruno ◽  
Hans Erik Rodvelt ◽  
Ola Skjæveland

Capillary pressure and resistivity index spontaneous imbibition experiments by the porous plate method, in a core holder at elevated temperature and net reservoir stress, are both difficult and time consuming special core analysis measurements to perform. In this type of experiment, low capillary forces act against a low permeable porous plate and only one face of the cylindrical core sample is in capillary contact with the fluid saturated porous plate. In this paper, core samples having different lithology, petrophysical properties and wettability are analysed by counter current spontaneous imbibition, starting at initial water saturation (Swi), at net confining pressure and elevated temperature. Synthetic brine is used as the wetting phase and Isopar L mineral oil as the non-wetting phase. This methodology is applied to investigate and evaluate how to obtain more reliable, more efficient and faster saturation imbibition data combined with electrical measurements, during spontaneous imbibition measurements. Resistivity index (RI), saturation exponent (n) (by single saturation equilibrium point using Archie’s second law RI= Sw-n) and wettability information using representative fluids, confining pressure and temperature are also obtained by applying this specific counter current imbibition technique and improved procedural approach.

2014 ◽  
Vol 2014 ◽  
pp. 1-12 ◽  
Author(s):  
Olugbenga Falode ◽  
Edo Manuel

An understanding of the mechanisms by which oil is displaced from porous media requires the knowledge of the role of wettability and capillary forces in the displacement process. The determination of representative capillary pressure (Pc) data and wettability index of a reservoir rock is needed for the prediction of the fluids distribution in the reservoir: the initial water saturation and the volume of reserves. This study shows how wettability alteration of an initially water-wet reservoir rock to oil-wet affects the properties that govern multiphase flow in porous media, that is, capillary pressure, relative permeability, and irreducible saturation. Initial water-wet reservoir core samples with porosities ranging from 23 to 33%, absolute air permeability of 50 to 233 md, and initial brine saturation of 63 to 87% were first tested as water-wet samples under air-brine system. This yielded irreducible wetting phase saturation of 19 to 21%. The samples were later tested after modifying their wettability to oil-wet using a surfactant obtained from glycerophtalic paint; and the results yielded irreducible wetting phase saturation of 25 to 34%. From the results of these experiments, changing the wettability of the samples to oil-wet improved the recovery of the wetting phase.


Molecules ◽  
2020 ◽  
Vol 25 (15) ◽  
pp. 3385 ◽  
Author(s):  
Abdulrauf R. Adebayo ◽  
Abubakar Isah ◽  
Mohamed Mahmoud ◽  
Dhafer Al-Shehri

Laboratory measurements of capillary pressure (Pc) and the electrical resistivity index (RI) of reservoir rocks are used to calibrate well logging tools and to determine reservoir fluid distribution. Significant studies on the methods and factors affecting these measurements in rocks containing oil, gas, and water are adequately reported in the literature. However, with the advent of chemical enhanced oil recovery (EOR) methods, surfactants are mixed with injection fluids to generate foam to enhance the gas injection process. Foam is a complex and non-Newtonian fluid whose behavior in porous media is different from conventional reservoir fluids. As a result, the effect of foam on Pc and the reliability of using known rock models such as the Archie equation to fit experimental resistivity data in rocks containing foam are yet to be ascertained. In this study, we investigated the effect of foam on the behavior of both Pc and RI curves in sandstone and carbonate rocks using both porous plate and two-pole resistivity methods at ambient temperature. Our results consistently showed that for a given water saturation (Sw), the RI of a rock increases in the presence of foam than without foam. We found that, below a critical Sw, the resistivity of a rock containing foam continues to rise rapidly. We argue, based on knowledge of foam behavior in porous media, that this critical Sw represents the regime where the foam texture begins to become finer, and it is dependent on the properties of the rock and the foam. Nonetheless, the Archie model fits the experimental data of the rocks but with resulting saturation exponents that are higher than conventional gas–water rock systems. The degree of variation in the saturation exponents between the two fluid systems also depends on the rock and fluid properties. A theory is presented to explain this phenomenon. We also found that foam affects the saturation exponent in a similar way as oil-wet rocks in the sense that they decrease the cross-sectional area of water available in the pores for current flow. Foam appears to have competing and opposite effects caused by the presence of clay, micropores, and conducting minerals, which tend to lower the saturation exponent at low Sw. Finally, the Pc curve is consistently lower in foam than without foam for the same Sw.


2005 ◽  
Vol 127 (3) ◽  
pp. 240-247 ◽  
Author(s):  
D. Brant Bennion ◽  
F. Brent Thomas

Very low in situ permeability gas reservoirs (Kgas<0.1mD) are very common and represent a major portion of the current exploitation market for unconventional gas production. Many of these reservoirs exist regionally in Canada and the United States and also on a worldwide basis. A considerable fraction of these formations appear to exist in a state of noncapillary equilibrium (abnormally low initial water saturation given the pore geometry and capillary pressure characteristics of the rock). These reservoirs have many unique challenges associated with the drilling and completion practices required in order to obtain economic production rates. Formation damage mechanisms affecting these very low permeability gas reservoirs, with a particular emphasis on relative permeability and capillary pressure effects (phase trapping) will be discussed in this article. Examples of reservoirs prone to these types of problems will be reviewed, and techniques which can be used to minimize the impact of formation damage on the productivity of tight gas reservoirs of this type will be presented.


Energies ◽  
2019 ◽  
Vol 12 (14) ◽  
pp. 2714
Author(s):  
Tao Li ◽  
Ying Wang ◽  
Min Li ◽  
Jiahao Ji ◽  
Lin Chang ◽  
...  

The determination of microscopic residual gas distribution is beneficial for exploiting reservoirs to their maximum potential. In this work, both forced and spontaneous imbibition (waterflooding) experiments were performed on a high-pressure displacement experimental setup, which was integrated with nuclear magnetic resonance (NMR) to reveal the impacts of capillary number (Ca) and initial water saturation (Swi) on the residual gas distribution over four magnitudes of injection rates (Q = 0.001, 0.01, 0.1 and 1 mL/min), expressed as Ca (logCa = −8.68, −7.68, −6.68 and −5.68), and three different Swi (Swi = 0%, 39.34% and 62.98%). The NMR amplitude is dependent on pore volumes while the NMR transverse relaxation time (T2) spectrum reflects the characteristics of pore size distribution, which is determined based on a mercury injection (MI) experiment. Using this method, the residual gas distribution was quantified by comparing the T2 spectrum of the sample measured after imbibition with the sample fully saturated by brine before imbibition. The results showed that capillary trapping efficiency increased with increasing Swi, and above 90% of residual gas existed in pores larger than 1 μm in the spontaneous imbibition experiments. The residual gas was trapped in pores by different capillary trapping mechanisms under different Ca, leading to the difference of residual gas distribution. The flow channels were mainly composed of micropores (pore radius, r < 1 μm) and mesopores (r = 1–10 μm) at logCa = −8.68 and −7.68, while of mesopores and macropores (r > 10 μm) at logCa = −5.68. At both Swi= 0% and 39.34%, residual gas distribution in macropores significantly decreased while that in micropores slightly increased with logCa increasing to −6.68 and −5.68, respectively.


SPE Journal ◽  
2012 ◽  
Vol 18 (02) ◽  
pp. 296-308 ◽  
Author(s):  
Y.. Zhou ◽  
J.O.. O. Helland ◽  
D.G.. G. Hatzignatiou

Summary It has been demonstrated experimentally that Leverett's J-function yields almost unique dimensionless drainage capillary pressure curves in relatively homogeneous rocks at strongly water-wet conditions, whereas for imbibition at mixed-wet conditions, it does not work satisfactorily because the permeability dependency on capillary pressure has been reported to be weak. The purpose of this study is to formulate a new dimensionless capillary pressure function for mixed-wet conditions on the basis of pore-scale modeling, which could overcome these restrictions. We simulate drainage, wettability alteration, and imbibition in 2D rock images by use of a semianalytical pore-scale model that represents the identified pore spaces as cross sections of straight capillary tubes. The fluid configurations occurring during drainage and imbibition in the highly irregular pore spaces are modeled at any capillary pressure and wetting condition by combining the free-energy minimization with an arc meniscus (AM)-determining procedure that identifies the intersections of two circles moving in opposite directions along the pore boundary. Circle rotation at pinned contact lines accounts for mixed-wet conditions. Capillary pressure curves for imbibition are simulated for different mixed-wet conditions in Bentheim sandstone samples, and the results are scaled by a newly proposed improved J-function that accounts for differences in formation wettability induced by different initial water saturations after primary drainage. At the end of primary drainage, oil-wet-pore wall segments are connected by many water-wet corners and constrictions that remain occupied by water. The novel dimensionless capillary pressure expression accounts for these conditions by introducing an effective contact angle that depends on the initial water saturation and is related to the wetting property measured at the core scale by means of a wettability index. The accuracy of the proposed J-function is tested on 36 imbibition capillary pressure curves for different mixed-wet conditions that are simulated with the semianalytical model in scanning-electron-microscope (SEM) images of Bentheim sandstone. The simulated imbibition capillary pressure curves and the reproduced curves, based on the proposed J-function, are in good agreement for the mixed-wet conditions considered in this study. The detailed behavior is explained by analyzing the fluid displacements occurring in the pore spaces. It is demonstrated that the proposed J-function could be applied to mixed-wet conditions to generate a family of curves describing different wetting states induced by assigning different wetting properties on the solid surfaces or by varying the initial water saturation after primary drainage. The variability of formation wettability and permeability could be described more accurately in reservoir-simulation models by means of the proposed J-function, and hence the opportunity arises for improved evaluation of core-sample laboratory experiments and reservoir performance.


2013 ◽  
Vol 291-294 ◽  
pp. 2657-2661
Author(s):  
Xiu Mei Qiu ◽  
Han Bing Bian

The mechanical behavior of a compacted unsaturated clay soil was experimentally investigated. Volume changes were investigated using a conventional odometer cell under a series of constant confining pressures, following a wetting path. The special loading paths were utilized to reflect field conditions associated with the compacted earth structure in earth filled embankment. The soils used in the experiments were taken from an earth dam. The compacted specimens were consolidated under k0-oedometer conditions. The volume change and the water content variation were measured during the tests. The influence of the confining pressure and the initial water saturation were taking into considerations. The experimental results show that the volumetric deformation properties of the remolded unsaturated soil could be expansive and/or contractive, depending on the confining pressure and the initial water saturation. It is also observed that for the mediate confining stress, there volumetric deformation of specimen applied to wetting loads has a transition from dilation to contraction.


2021 ◽  
Vol 11 (4) ◽  
pp. 1577-1595
Author(s):  
Rasoul Ranjbar-Karami ◽  
Parisa Tavoosi Iraj ◽  
Hamzeh Mehrabi

AbstractKnowledge of initial fluids saturation has great importance in hydrocarbon reservoir analysis and modelling. Distribution of initial water saturation (Swi) in 3D models dictates the original oil in place (STOIIP), which consequently influences reserve estimation and dynamic modelling. Calculation of initial water saturation in heterogeneous carbonate reservoirs always is a challenging task, because these reservoirs have complex depositional and diagenetic history with a complex pore network. This paper aims to model the initial water saturation in a pore facies framework, in a heterogeneous carbonate reservoir. Petrographic studies were accomplished to define depositional facies, diagenetic features and pore types. Accordingly, isolated pores are dominant in the upper parts, while the lower intervals contain more interconnected interparticle pore types. Generally, in the upper and middle parts of the reservoir, diagenetic alterations such as cementation and compaction decreased the primary reservoir potential. However, in the lower interval, which mainly includes high-energy shoal facies, high reservoir quality was formed by primary interparticle pores and secondary dissolution moulds and vugs. Using huge number of primary drainage mercury injection capillary pressure tests, we evaluate the ability of FZI, r35Winland, r35Pittman, FZI* and Lucia’s petrophysical classes in definition of rock types. Results show that recently introduced rock typing method is an efficient way to classify samples into petrophysical rock types with same pore characteristics. Moreover, as in this study MICP data were available from every one meter of reservoir interval, results show that using FZI* method much more representative sample can be selected for SCAL laboratory tests, in case of limitation in number of SCAL tests samples. Integration of petrographic analyses with routine (RCAL) and special (SCAL) core data resulted in recognition of four pore facies in the studied reservoir. Finally, in order to model initial water saturation, capillary pressure data were averaged in each pore facies which was defined by FZI* method and using a nonlinear curve fitting approach, fitting parameters (M and C) were extracted. Finally, relationship between fitting parameters and porosity in core samples was used to model initial water saturation in wells and between wells. As permeability prediction and reservoir rock typing are challenging tasks, findings of this study help to model initial water saturation using log-derived porosity.


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