Mathematical Modeling of Essential Oil Extraction by Steam Distillation for Native Plants from Southern Brazil

2012 ◽  
Vol 15 (5) ◽  
pp. 839-846 ◽  
Author(s):  
Rubem M.F. Vargas ◽  
Aline M. Lucas ◽  
Máurean S.T. Barroso ◽  
Débora V. Dutra ◽  
Marília V. Becker ◽  
...  
Processes ◽  
2021 ◽  
Vol 9 (11) ◽  
pp. 2075
Author(s):  
Tan Phat Dao ◽  
Thanh Viet Nguyen ◽  
Thi Yen Nhi Tran ◽  
Xuan Tien Le ◽  
Ton Nu Thuy An ◽  
...  

Pomelo peel-derived essential oils have been gaining popularity due to greater demand for stress relief therapy or hair care therapy. In this study, we first performed optimization of parameters in the pomelo essential oil extraction process on a pilot scale to gain better insights for application in larger scale production. Then extraction kinetics, activation energy, thermodynamics, and essential oil quality during the extraction process were investigated during the steam distillation process. Three experimental conditions including material mass, steam flow rate, and extraction time were taken into consideration in response surface methodology (RSM) optimization. The optimal conditions were found as follows: sample weight of 422 g for one distillation batch, steam flow rate of 2.16 mL/min and extraction time of 106 min with the coefficient of determination R2 of 0.9812. The nonlinear kinetics demonstrated the compatibility of the kinetic model with simultaneous washing and unhindered diffusion with a washing rate constant of 0.1515 min−1 and a diffusion rate constant of 0.0236 min−1. The activation energy of the washing and diffusion process was 167.43 kJ.mol−1 and 96.25 kJ.mol−1, respectively. The thermodynamic value obtained at the ΔG° value was −35.02 kJ.mol−1. The quality of pomelo peel essential oil obtained by steam distillation was characterized by its high limonene content (96.996%), determined by GC-MS.


1990 ◽  
Vol 30 (5) ◽  
pp. 681 ◽  
Author(s):  
E Diatloff

Three native species of Leptospermum (L. petersonii, L. Flavescens, L. luehmannii) were grown in an amended podsolic soil under 4 nitrogen (N) levels, 0, 20, 40 and 60 kg Nha, supplied as NH4N03. Plants were harvested after 16 weeks growth, leaves were separated from stems, and essential oil was distilled from leaves by steam distillation. Extracted oils were analysed for their components by gas chromatography. Oil density from L. petersonii was also determined. Growth and oil yield of the 3 Leptospermum species showed no response to N fertilisation. However, the oil composition in L. petersonii and L. flavescens leaves was affected. The greatest response was in the geranial and citronella1 contents in L. petersonii, which peaked in the 40 kg N/ha treatment. This is the first known report of the manipulation of essential oil composition of Australian native plants by N fertilisation. The low optimal level of N fertiliser required for maximum production of valuable oil components indicates that Leptospermum spp. are suitable for infertile soils. The low �-pinene yield of L. luehmannii makes it unsuitable for commercial exploitation.


Author(s):  
Nurhani Kasuan ◽  
Zakiah Mohd Yusoff ◽  
Zuraida Muhammad ◽  
Mohd Noor Nashriq Nordin ◽  
Mohd Hezri Fazalul Rahiman ◽  
...  

2021 ◽  
pp. 1-16
Author(s):  
Arslan Afzal ◽  
Anjum Munir ◽  
Waseem Amjad ◽  
Jorge L. Alvarado ◽  
Muhammad Umair ◽  
...  

Abstract Solar distillation system has recently been explored and used for the extraction of essential oil from different agricultural herbs. The efficiency of conventional distillation systems is low and most are driven by hot gases. On the other hand, the solar-driven distillation system has higher efficiency and is based on renewable energy. The modified solar distillation system comprises a Scheffler reflector “concentrator”, newly design steam receiver, distillation still, steam condenser, florentine flask and biomass-based boiler. A perforated circular pan added at the still bottom and pattern of steam flow and temperature distribution was examined using the Computational Fluid Dynamics (CFD) technique. The CFD simulation results showed that homogeneity in the steam distribution in the distillation still which is required to get maximum essential oil extraction efficiency. The energy dissemination at different parts of newly design solar distillation system was estimated using mathematical modeling. The results of different experiments showed that the yield of essential oils from fresh Rosemary and Cumin were 0.17% w/w and 1.11% w/w respectively. The efficiency of the modified solar distillation system with a perforated pan and steam receiver was found to be 8% higher than the previous system.


Author(s):  
Nik ‘Amirah Farhana Nik Ahmad Lutfi ◽  
Mohd Farid Atan ◽  
Nazeri Abdul Rahman ◽  
Shanti Faridah Salleh ◽  
Noraziah Abdul Wahab

The main objective of this study is to improve the mathematical modelling of Cymbopogon winterianus essential oil extraction by steam distillation proposed by Cassel and Vargas by minimum 5% error reduction. Two process variable of steam distillation which are extraction time and raw material state (dry or natural) has been optimized by using factorial experimental planning to obtain high yields of citronella essential oil from twig and leaves of lemongrass species Cymbopogon winterianus (C.winterianus). The optimal condition for maximum yield (0.942%) were found to be an extraction time, 4 hr, state, natural plant. The study of Cassel and Vargas was subsequently continued with five proposed kinetics model of the extraction process. The modelling of the extraction process is optimized by using one adjustable parameter of the model and the adequacy of the fit of the models to the experimental data are analyzed by using three statistical criteria that are correlation coefficient (r) ,the root mean square error (RMSE) and the mean relative deviation modulus (E). The result has shown that the mathematical model developed by Ana based on mass transfer fundamentals is the optimum mathematical model for the extraction of Cymbopogon winterianus essential oil by steam distillation.


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