Investigating the effect of acid erosion on degradation and brittle fractures in coal using etching solutions

Author(s):  
Xiangfeng Lv ◽  
Xuan Ji
Keyword(s):  
Open Physics ◽  
2020 ◽  
Vol 18 (1) ◽  
pp. 961-967
Author(s):  
Xiaomin Li ◽  
Jianrong Zhang

Abstract A quasi-static tensile test was performed on a 1.4 mm-thick TRIP780 steel strip with welding points. An MTS810 material test machine was used in the test, and a Split Hopkinson tension bar device was used in performing impact stretch loading at different strain rates. The dynamic tensile stress–strain curve of the spot welding material with different strain rates was obtained through the finely designed Hopkinson rod test, and the strain rate dependence of a TRIP780 steel spot welding material was discussed. According to the dynamic constitutive equation of the TRIP780 steel spot welding material, the test results were numerically simulated, the constitutive description and test curves were compared, and the simulation results and test results were discussed and analyzed. The fractures of the test recovery specimen were scanned with the scanning electron microscope, and the fracture mechanism of the TRIP780 steel spot welding material was explored by observing the fractures. The surfaces of the fractures surface showed obvious cleavage river patterns, and the evolution process of microcracks was determined and used in characterizing brittle fractures in specimen spot welding sample subjected to dynamic stretch loading.


1980 ◽  
Vol 102 (1) ◽  
pp. 15-19 ◽  
Author(s):  
S. T. Rolfe

Since World War II, periodic changes in the fabrication, design, and material specifications for ship steels have been made to preclude brittle fractures. These various changes are described briefly, along with a history of fracture control for ships to serve as background information for a discussion of the present-day structural integrity program for ships in the marine industry. As additional information related to the structural integrity of ship structures, a review of two recent ship failures (e.g., the Ingram Barge in 1972 and the Chester A. Poling in 1977) is presented to demonstrate some of the factors involved in brittle fractures of ships. In both of these failures there were other factors contributing to the final brittle fractures that were more important than the notch toughness levels. These factors are reviewed as the basis for an observation regarding the overall structural integrity of merchant ships.


2021 ◽  
Vol 59 (1) ◽  
pp. 61-66
Author(s):  
Tae Chang Park ◽  
Beom Suk Kim ◽  
Ji Hee Son ◽  
Yeong Koo Yeo

The Charpy impact test is used to identify the transition between ductility and brittleness. The percentages of ductile and brittle fractures in steel can be evaluated based on each fracture area, which is presently determined by an analyzer with the naked eye. This method may lead to subjective judgement, and difficulty accurately quantifying the percentage. To resolve this problem, a new analysis method based on image processing is proposed in this study. A program that can automatically calculate the percentage of the ductile and brittle fractures has been developed. The analysis is performed after converting an RGB fracture image into a binary image using image processing techniques. The final binary image consists of 0 and 1 pixels. The parts with the pixel values of 1 correspond to the brittle fracture areas, and the pixel values of 0 represent the ductile fracture areas. As a result, by counting the number of 0 pixels in the entire area, it is possible to automatically calculate the percentage of ductile fracture. Using the proposed automatic fracture analysis program, it is possible to selectively distinguish only the brittle fracture from the entire fracture area, and to accurately and quantitatively calculate the percentages of ductile and brittle fractures.


2013 ◽  
Vol 50 (12) ◽  
pp. 1165-1177
Author(s):  
Natalie J. Pietrzak-Renaud

The base of the Proterozoic Negaunee Iron Formation is exposed in the open pit at Tilden Mine, Marquette, Michigan. Juxtaposed against the Archean-aged Palmer Gneiss, it is bounded by the regional-scale Southern Shear Zone and cut by two sets of dykes: an older chloritic and schistose set and a younger 1.1 Ga Keweenawan set. Tilden Mine is dominated by a 100 m scale plunging northwest-anticline and is cut by a growth fault locally termed the Tower Hill Fault that intersects the Southern Shear Zone. The base of the exposed iron formation is composed of three lithofacies, including lower clastics that grade into the overlying banded iron formation that in turn grades upward into granular iron formation. This succession is capped by chloritic metadiabases locally termed the Summit Hill Sill and Pillar Intrusive. Petrographic and mineral chemical investigations document primary or early diagenetic hematite, siderite and possibly ferri-hydrite, metamorphic and related hydrothermal magnetite, chlorite, late martite overgrowing earlier magnetite and growth of specularite. All three lithofacies are cut by brittle fractures and late quartz veins. Brittle fractures are coated with chlorite, carbonate minerals, fluor-apatite, and sparse Cu-sulphides. These lithofacies document initial clastic sedimentation of strained detrital quartz into a subsiding fault trough. Over time, as subsidence slowed or sea level fluctuated, clastic deposition competed with quiescent chemical sedimentation, leading to deposition of the banded iron formation facies. As a stable shelf platform emerged, the granular iron formation facies was deposited via wave reworking of hardgrounds. Subsequent diagenesis initiated dissolution of carbonate and chert and promoted diagenetic replacement of primary iron minerals and chert. Regional metamorphism during Penokean orogeny at 1875–1835 Ma produced a suite of secondary metamorphic and related hydrothermal minerals. Metamorphism and hydrothermal flux related to the 1750 Ma development of the Republic Metamorphic Node overprinted the iron formation at Tilden to greenschist facies and infilled brittle fractures with a unique mineral assemblage. This unique mineral assemblage exhibits some striking similarities to Mn, Au, and Cu-sulphides documented at Champion Mine, west of Tilden, and proximal to the core of the Republic Node.


Metals ◽  
2020 ◽  
Vol 10 (3) ◽  
pp. 362 ◽  
Author(s):  
Toshiki Nagahari ◽  
Taigi Nagoya ◽  
Koji Kakehi ◽  
Naoko Sato ◽  
Shizuka Nakano

Selective laser melting (SLM) in a vacuum environment is a relatively new process. Although the material is expected to undergo a gradual heat change, which will influence the microstructure and creep properties of IN718, little research has been conducted to date. Here, we compared specimens built in vacuum (V-SLM) to those built in an Ar atmosphere (Ar-SLM). We investigated the microstructure and creep properties of V-SLM, and compared the V-SLM specimen to a conventional Ar-SLM specimen. The V-SLM specimen had a larger-grained texture, and the quantity of the δ phase was much lower. In addition, the V-SLM specimen had lower amounts of aluminum and titanium oxides, which improved the stability of the γ″ phase. Thus, the V-SLM specimen showed better creep life than the Ar-SLM, due to prevention of brittle fractures along the interdendritic regions.


1989 ◽  
Vol 21 (4) ◽  
pp. 430-435
Author(s):  
A. A. Astaf'ev ◽  
V. M. Goritskii ◽  
G. R. Shneiderov ◽  
A. D. Shur ◽  
V. A. Yukhanov

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