An electron backscatter diffraction investigation of crystallographic orientations of embedded nanoparticles within melt-textured YBCO high temperature superconductors

2006 ◽  
Vol 19 (7) ◽  
pp. S562-S566 ◽  
Author(s):  
A Koblischka-Veneva ◽  
M R Koblischka ◽  
N Hari Babu ◽  
D A Cardwell ◽  
L Shlyk ◽  
...  
Keyword(s):  
High Temperature ◽  
Electron Backscatter Diffraction ◽  
High Temperature Superconductors ◽  
Electron Backscatter ◽  
Embedded Nanoparticles ◽  
Backscatter Diffraction ◽  
Crystallographic Orientations

Application of electron backscatter diffraction in the SEM to textural problems of coated high-temperature superconductors

2003 ◽  
Vol 94 (5) ◽  
pp. 580-586 ◽  
Author(s):  
Bernhard Obst ◽  
Rainer Nast ◽  
Sonja Schlachter ◽  
Bernd de Boer ◽  
Bernhard Holzapfel ◽  
...  
Keyword(s):  
High Temperature ◽  
Electron Backscatter Diffraction ◽  
High Temperature Superconductors ◽  
Electron Backscatter ◽  
Backscatter Diffraction

Surface Crystallization of Cordierite from Glass Studied by High-Temperature X-ray Diffraction and Electron Backscatter Diffraction (EBSD)

2011 ◽  
Vol 11 (10) ◽  
pp. 4660-4666 ◽  
Author(s):  
Wolfgang Wisniewski ◽  
Carlos André Baptista ◽  
Matthias Müller ◽  
Günter Völksch ◽  
Christian Rüssel
Keyword(s):  
High Temperature ◽  
Electron Backscatter Diffraction ◽  
Surface Crystallization ◽  
X Ray Diffraction ◽  
X Ray ◽  
Electron Backscatter ◽  
Backscatter Diffraction

Development of Asymmetric Rolling for the Better Control over Structure and Mechanical Properties in IF Steel

2012 ◽  
Vol 706-709 ◽  
pp. 2788-2793 ◽  
Author(s):  
Dmitry Orlov ◽  
Rimma Lapovok ◽  
László S. Tóth ◽  
Ilana B. Timokhina ◽  
Peter D. Hodgson ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Electron Backscatter Diffraction ◽  
Tensile Tests ◽  
Experimental Investigations ◽  
If Steel ◽  
Asymmetric Rolling ◽  
Electron Backscatter ◽  
Strain Components ◽  
Backscatter Diffraction ◽  
Crystallographic Orientations

In the present study, the effects of kinematic and geometric asymmetries in rolling during multi-pass processing of IF steel are examined. The theoretical investigation by final element simulations and experimental investigations by means of electron-backscatter diffraction analysis and tensile tests suggest that asymmetric rolling increases the total imposed strain compared to symmetric rolling, and largely re-distributes the strain components due to additional shear. This enhances the intensity of grain refinement, strengthens and tilts crystallographic orientations, and increases mechanical strength. The effect is highest in the asymmetric rolling with differential roll diameters.

Inferential statistics of electron backscatter diffraction data from within individual crystalline grains

2010 ◽  
Vol 43 (6) ◽  
pp. 1338-1355 ◽  
Author(s):  
Florian Bachmann ◽  
Ralf Hielscher ◽  
Peter E. Jupp ◽  
Wolfgang Pantleon ◽  
Helmut Schaeben ◽  
...  
Keyword(s):  
Electron Backscatter Diffraction ◽  
Orientation Distribution ◽  
Numerical Determination ◽  
Spatial Statistical Analysis ◽  
Spatial Reference ◽  
Electron Backscatter ◽  
The Mean ◽  
Backscatter Diffraction ◽  
Crystallographic Orientations

Highly concentrated distributed crystallographic orientation measurements within individual crystalline grains are analysed by means of ordinary statistics neglecting their spatial reference. Since crystallographic orientations are modelled as left cosets of a given subgroup of SO(3), the non-spatial statistical analysis adapts ideas borrowed from the Bingham quaternion distribution on {\bb S}^3. Special emphasis is put on the mathematical definition and the numerical determination of a `mean orientation' characterizing the crystallographic grain as well as on distinguishing several types of symmetry of the orientation distribution with respect to the mean orientation, like spherical, prolate or oblate symmetry. Applications to simulated as well as to experimental data are presented. All computations have been done with the free and open-source texture toolboxMTEX.

scholarly journals Texture and Microtexture of Pure (6N) and Commercially Pure Aluminum after Deformation by Extrusion with Forward-Backward Rotating Die (Kobo)

2016 ◽  
Vol 61 (1) ◽  
pp. 461-468 ◽  
Author(s):  
M. Bieda ◽  
S. Boczkal ◽  
P. Koprowski ◽  
K. Sztwiertnia ◽  
K. Pieła
Keyword(s):  
Electron Microscopy ◽  
Grain Size ◽  
Electron Backscatter Diffraction ◽  
Pure Aluminum ◽  
Pure Aluminium ◽  
Commercially Pure ◽  
Transmission Electron ◽  
Electron Backscatter ◽  
Backscatter Diffraction ◽  
Crystallographic Orientations

Pure aluminium (6N) and commercially pure aluminium (99.7) was deformed by KOBO method. Microstructure and texture of both materials after deformation was analyzed by means of scanning and transmission electron microscopy. Advanced methods of crystallographic orientations measurements like Electron Backscatter Diffraction - EBSD (SEM) and microdiffraction (TEM) was used. Grain size distribution and misorientation between grains in cross and longitudinal sections of the samples were analyzed. Differences in size and homogeneity of the grains were observed in both materials. Pure aluminium was characterized by larger grain size in both sections of extruded material. Whereas commercially pure aluminium reveals smaller grain size and more homogeneous and stable microstructure.

β-Ca11B2Si4O22: six-fold twinning, crystal structure and thermal expansion

2018 ◽  
Vol 233 (6) ◽  
pp. 379-390 ◽  
Author(s):  
Sergey N. Volkov ◽  
Valentina A. Yukhno ◽  
Rimma S. Bubnova ◽  
Vladimir V. Shilovskikh
Keyword(s):  
Crystal Structure ◽  
Thermal Expansion ◽  
High Temperature ◽  
Electron Backscatter Diffraction ◽  
Monoclinic Structure ◽  
X Ray Diffraction ◽  
X Ray ◽  
Electron Backscatter ◽  
Backscatter Diffraction ◽  
Relationship Of

Abstract The low-temperature polymorph β-Ca11B2Si4O22 crystallizes as a monoclinic structure [space group is P21/c, a=14.059(9), b=6.834(5), c=10.597(7) Å, β=100.735(8)°]. The crystal investigated by single-crystal X-ray diffraction was a twin composed of six individuals. The crystal structure is similar to that of mineral spurrite, Ca5(SiO4)2CO3, and can be described as a framework of [CaO5] and [CaO6] polyhedra, the cavities of which are filled with [SiO4] and [BO3] groups. The orientation relationship of twin domains was investigated by electron backscatter diffraction (EBSD). Thermal expansion was studied by high-temperature X-ray powder diffraction. It is slightly anisotropic: α11=10, α22=16, α33=12×10−6°C−1 at 200°C.

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