Statistical analysis of correlations in the x-ray induced Coulomb explosion of iodopyridine

2021 ◽

Author(s):

Fabian Jaeger ◽

Alessandro Franceschi ◽

Holger Hoche ◽

Peter Groche ◽

Matthias Oechsner

Keyword(s):

Residual Stress ◽

Statistical Analysis ◽

Stress Measurement ◽

Industrial Applications ◽

Cold Extrusion ◽

X Ray Diffraction ◽

Forming Process ◽

X Ray ◽

Stress States ◽

Key Aspects

AbstractCold extruded components are characterized by residual stresses, which originate from the experienced manufacturing process. For industrial applications, reproducibility and homogeneity of the final components are key aspects for an optimized quality control. Although striving to obtain identical deformation and surface conditions, fluctuation in the manufacturing parameters and contact shear conditions during the forming process may lead to variations of the spatial residual stress distribution in the final product. This could lead to a dependency of the residual stress measurement results on the relative axial and circumferential position on the sample. An attempt to examine this problem is made by the employment of design of experiments (DoE) methods. A statistical analysis of the residual stress results generated through X-Ray diffraction is performed. Additionally, the ability of cold extrusion processes to generate uniform stress states is analyzed on specimens of austenitic stainless steel 1.4404 and possible correlations with the pre-deformed condition are statistically examined. Moreover, the influence of the coating, consisting of oxalate and a MoS2 based lubricant, on the X-Ray diffraction measurements of the surface is investigated.

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Statistical analysis of soft X-ray solar flares during solar cycles 22, 23, and 24

Astrophysics and Space Science ◽

10.1007/s10509-020-03909-z ◽

2021 ◽

Vol 366 (1) ◽

Author(s):

Bo Xiong ◽

Ting Wang ◽

Xiaolin Li ◽

Yunxing Yin

Keyword(s):

Statistical Analysis ◽

Solar Flares ◽

Solar Cycles ◽

X Ray

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Chemical Species, Micromorphology, and XRD Fingerprint Analysis of Tibetan MedicineZuotaiContaining Mercury

Bioinorganic Chemistry and Applications ◽

10.1155/2016/7010519 ◽

2016 ◽

Vol 2016 ◽

pp. 1-11 ◽

Cited By ~ 8

Author(s):

Cen Li ◽

Hongxia Yang ◽

Yuzhi Du ◽

Yuancan Xiao ◽

Zhandui ◽

...

Keyword(s):

Statistical Analysis ◽

Multivariate Statistical Analysis ◽

Chemical Species ◽

Physicochemical Characteristics ◽

Chemical Substance ◽

Tibetan Medicine ◽

Fingerprint Analysis ◽

Multivariate Statistical ◽

Positive Role ◽

X Ray

Zuotai(gTso thal) is one of the famous drugs containing mercury in Tibetan medicine. However, little is known about the chemical substance basis of its pharmacodynamics and the intrinsic link of different samples sources so far. Given this, energy dispersive spectrometry of X-ray (EDX), scanning electron microscopy (SEM), atomic force microscopy (AFM), and powder X-ray diffraction (XRD) were used to assay the elements, micromorphology, and phase composition of nineZuotaisamples from different regions, respectively; the XRD fingerprint features ofZuotaiwere analyzed by multivariate statistical analysis. EDX result shows thatZuotaicontains Hg, S, O, Fe, Al, Cu, and other elements. SEM and AFM observations suggest thatZuotaiis a kind of ancient nanodrug. Its particles are mainly in the range of 100–800 nm, which commonly further aggregate into 1–30 μm loosely amorphous particles. XRD test shows thatβ-HgS, S8, andα-HgS are its main phase compositions. XRD fingerprint analysis indicates that the similarity degrees of nine samples are very high, and the results of multivariate statistical analysis are broadly consistent with sample sources. The present research has revealed the physicochemical characteristics ofZuotai, and it would play a positive role in interpreting this mysterious Tibetan drug.

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