Employing a Cerenkov detector for the thickness measurement of X-rays in a scattering background

AbstractThe fluorescence x-ray method of the coating thickness measurement is theoretically studied. The theoretical formulas of the fluorescence x-ray intensity from the coating and from the substrate are obtained which include the enhancement effect between the coating and the substrate. The formulas are applied to the following examples and are confirmed experimentally: zinc on steel; tin on steel; aluminum on steel and on PMMA. The experimental results agree well with the theoretical results.

Download Full-text

Thickness measurement of organic films using Compton scattering of characteristic X-rays

Applied Radiation and Isotopes ◽

10.1016/j.apradiso.2011.03.048 ◽

2011 ◽

Vol 69 (9) ◽

pp. 1241-1245 ◽

Cited By ~ 6

Author(s):

Jong-Yun Kim ◽

Yong Suk Choi ◽

Yong Joon Park ◽

Kyuseok Song ◽

Sung-Hee Jung ◽

...

Keyword(s):

Compton Scattering ◽

Thickness Measurement ◽

Organic Films ◽

X Rays

Download Full-text

Foil thickness measurement via the intensity ratio of proton-induced X-Rays

Nuclear Instruments and Methods in Physics Research Section B Beam Interactions with Materials and Atoms ◽

10.1016/0168-583x(89)90038-4 ◽

1989 ◽

Vol 43 (2) ◽

pp. 197-202 ◽

Cited By ~ 4

Author(s):

J.L. Campbell ◽

W.J. Teesdale ◽

J.A. Maxwell

Keyword(s):

Intensity Ratio ◽

Thickness Measurement ◽

Foil Thickness ◽

X Rays

Download Full-text

Thickness Determination of Thin Polycrystalline Films by Grazing Incidence X-Ray Diffraction

Materials Science Forum ◽

10.4028/www.scientific.net/msf.443-444.115 ◽

2004 ◽

Vol 443-444 ◽

pp. 115-118 ◽

Cited By ~ 3

Author(s):

J. Lhotka ◽

Radomír Kužel ◽

G. Cappuccio ◽

V. Valvoda

Keyword(s):

Thin Film ◽

High Sensitivity ◽

Grazing Incidence ◽

Thickness Measurement ◽

X Rays ◽

X Ray Diffraction ◽

Average Value ◽

Tin Film ◽

Thin Polycrystalline

The thickness measurement based on absorption of X-rays in thin films has been tested on a polycrystalline titanium nitride films deposited on a tungsten carbide substrate. Intensities of three reflections from each material were measured for incidence angles of the primary beam ranging from 0.5° to 35°. After experimental correction for texture effects, data from the TiN film and the WC substrate were fitted by known functions using least squares routines. The substrate reflection intensities were found to be more suitable for determining the thickness of the overlaying thin film. The average thickness of TiN film (2.00± 0.17 µm) determined from the substrate reflections was in fair agreement with the average value obtained from optical microscopy (2.2± 0.8 µm). The thickness values determined from the TiN thin film reflections are very unreliable due to a high sensitivity of measurements to disturbing instrumental and sample effects at small angles.

Download Full-text

White-Light Coronal Structures: Streamers and CMEs

International Astronomical Union Colloquium ◽

10.1017/s0252921100025045 ◽

1994 ◽

Vol 144 ◽

pp. 82

Author(s):

E. Hildner

Keyword(s):

Emission Line ◽

Electron Density ◽

White Light ◽

Coronal Mass Ejections ◽

X Rays ◽

Solar Cycles ◽

Temperature Function ◽

X Ray ◽

Eclipse Observations ◽

Coronal Structures

AbstractOver the last twenty years, orbiting coronagraphs have vastly increased the amount of observational material for the whitelight corona. Spanning almost two solar cycles, and augmented by ground-based K-coronameter, emission-line, and eclipse observations, these data allow us to assess,inter alia: the typical and atypical behavior of the corona; how the corona evolves on time scales from minutes to a decade; and (in some respects) the relation between photospheric, coronal, and interplanetary features. This talk will review recent results on these three topics. A remark or two will attempt to relate the whitelight corona between 1.5 and 6 R⊙to the corona seen at lower altitudes in soft X-rays (e.g., with Yohkoh). The whitelight emission depends only on integrated electron density independent of temperature, whereas the soft X-ray emission depends upon the integral of electron density squared times a temperature function. The properties of coronal mass ejections (CMEs) will be reviewed briefly and their relationships to other solar and interplanetary phenomena will be noted.

Download Full-text

Emergence of Twisted Magnetic Flux Related Sigmoidal Brightening

International Astronomical Union Colloquium ◽

10.1017/s0252921100064630 ◽

2000 ◽

Vol 179 ◽

pp. 263-264

Author(s):

K. Sundara Raman ◽

K. B. Ramesh ◽

R. Selvendran ◽

P. S. M. Aleem ◽

K. M. Hiremath

Keyword(s):

Magnetic Field ◽

Magnetic Fields ◽

Magnetic Flux ◽

Ultra Violet ◽

Active Regions ◽

Morphological Properties ◽

Energy Storage And Conversion ◽

The Sun ◽

X Rays ◽

The Magnetic Field

Extended AbstractWe have examined the morphological properties of a sigmoid associated with an SXR (soft X-ray) flare. The sigmoid is cospatial with the EUV (extreme ultra violet) images and in the optical part lies along an S-shaped Hαfilament. The photoheliogram shows flux emergence within an existingδtype sunspot which has caused the rotation of the umbrae giving rise to the sigmoidal brightening.It is now widely accepted that flares derive their energy from the magnetic fields of the active regions and coronal levels are considered to be the flare sites. But still a satisfactory understanding of the flare processes has not been achieved because of the difficulties encountered to predict and estimate the probability of flare eruptions. The convection flows and vortices below the photosphere transport and concentrate magnetic field, which subsequently appear as active regions in the photosphere (Rust & Kumar 1994 and the references therein). Successive emergence of magnetic flux, twist the field, creating flare productive magnetic shear and has been studied by many authors (Sundara Ramanet al.1998 and the references therein). Hence, it is considered that the flare is powered by the energy stored in the twisted magnetic flux tubes (Kurokawa 1996 and the references therein). Rust & Kumar (1996) named the S-shaped bright coronal loops that appear in soft X-rays as ‘Sigmoids’ and concluded that this S-shaped distortion is due to the twist developed in the magnetic field lines. These transient sigmoidal features tell a great deal about unstable coronal magnetic fields, as these regions are more likely to be eruptive (Canfieldet al.1999). As the magnetic fields of the active regions are deep rooted in the Sun, the twist developed in the subphotospheric flux tube penetrates the photosphere and extends in to the corona. Thus, it is essentially favourable for the subphotospheric twist to unwind the twist and transmit it through the photosphere to the corona. Therefore, it becomes essential to make complete observational descriptions of a flare from the magnetic field changes that are taking place in different atmospheric levels of the Sun, to pin down the energy storage and conversion process that trigger the flare phenomena.

Download Full-text

The Clinical, Roentgenological and Morphological Effects of an Acute Exposure of Phosgene on the Lungs of Dogs

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100065237 ◽

1971 ◽

Vol 29 ◽

pp. 236-237

Author(s):

R. F. Bils ◽

W. F. Diller ◽

F. Huth

Keyword(s):

Latent Period ◽

Chemical Industry ◽

Toxic Substance ◽

Lung Edema ◽

X Rays ◽

Beagle Dogs ◽

Male And Female ◽

Morphological Alterations ◽

Before And After ◽

Electron Microscopes

Phosgene still plays an important role as a toxic substance in the chemical industry. Thiess (1968) recently reported observations on numerous cases of phosgene poisoning. A serious difficulty in the clinical handling of phosgene poisoning cases is a relatively long latent period, up to 12 hours, with no obvious signs of severity. At about 12 hours heavy lung edema appears suddenly, however changes can be seen in routine X-rays taken after only a few hours' exposure (Diller et al., 1969). This study was undertaken to correlate these early changes seen by the roengenologist with morphological alterations in the lungs seen in the'light and electron microscopes.Forty-two adult male and female Beagle dogs were selected for these exposure experiments. Treated animals were exposed to 94.5-107-5 ppm phosgene for 10 min. in a 15 m3 chamber. Roentgenograms were made of the thorax of each animal before and after exposure, up to 24 hrs.

Download Full-text

Chemical Species Identification in an SEM by Changes in Emitted X-Ray Energies

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100052869 ◽

1974 ◽

Vol 32 ◽

pp. 570-571

Author(s):

R. H. Duff

Keyword(s):

Species Identification ◽

Valence Electron ◽

Chemical Species ◽

X Rays ◽

Chemical Bonds ◽

Small Shift ◽

X Ray ◽

Electron Transitions ◽

Peak Energy ◽

Chemical Combination

A material irradiated with electrons emits x-rays having energies characteristic of the elements present. Chemical combination between elements results in a small shift of the peak energies of these characteristic x-rays because chemical bonds between different elements have different energies. The energy differences of the characteristic x-rays resulting from valence electron transitions can be used to identify the chemical species present and to obtain information about the chemical bond itself. Although these peak-energy shifts have been well known for a number of years, their use for chemical-species identification in small volumes of material was not realized until the development of the electron microprobe.

Download Full-text

Influence of X-Ray Induced Fluorescence on Energy Dispersive X-Ray Analysis of Thin Foils

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100079164 ◽

1977 ◽

Vol 35 ◽

pp. 328-329

Author(s):

E. A. Kenik ◽

J. Bentley

Keyword(s):

Thin Foil ◽

Electron Excitation ◽

Simple Approach ◽

Foil Thickness ◽

X Rays ◽

X Ray ◽

Hole Spectrum ◽

Illumination System ◽

Thin Foils ◽

Intensity Ratios

Cliff and Lorimer (1) have proposed a simple approach to thin foil x-ray analy sis based on the ratio of x-ray peak intensities. However, there are several experimental pitfalls which must be recognized in obtaining the desired x-ray intensities. Undesirable x-ray induced fluorescence of the specimen can result from various mechanisms and leads to x-ray intensities not characteristic of electron excitation and further results in incorrect intensity ratios.In measuring the x-ray intensity ratio for NiAl as a function of foil thickness, Zaluzec and Fraser (2) found the ratio was not constant for thicknesses where absorption could be neglected. They demonstrated that this effect originated from x-ray induced fluorescence by blocking the beam with lead foil. The primary x-rays arise in the illumination system and result in varying intensity ratios and a finite x-ray spectrum even when the specimen is not intercepting the electron beam, an ‘in-hole’ spectrum. We have developed a second technique for detecting x-ray induced fluorescence based on the magnitude of the ‘in-hole’ spectrum with different filament emission currents and condenser apertures.

Download Full-text