scholarly journals Applied spectroscopy methods application in the defluorinated phosphate production technological process control problem

2021 ◽  
Vol 2094 (2) ◽  
pp. 022042
Author(s):  
M A Vaganov ◽  
V I Kazakov ◽  
V F Lebedev ◽  
A R Bestugin ◽  
V V Kitaev
Keyword(s):  
Chemical Composition ◽  
Technological Process ◽  
Spectral Characteristics ◽  
Product Yield ◽  
Spectral Lines ◽  
Control Mode ◽  
Emission Spectrometry ◽  
Composition Analysis ◽  
Real Time Control ◽  
Study Results

Abstract The paper considers the applied optical spectroscopy methods application in the defluorinated phosphate production, controlling the technological process task. The emission spectral analysis using the method possibilities to control the charge hydrothermal acid processing process, which takes place in special furnaces with natural gas burning and a temperature of 1340 – 1400°C, have been studied. Experiments have been carried out in production conditions, and the radiation spectral characteristics study results from the furnace during the defluorination technological process are presented. It is shown that, by measuring individual spectral lines, it is possible to provide an automatic control mode for the defluorination technological process in the furnace burner controlling the combustion mode terms without the need for visual observation by the operator to ensure a better product yield. The work second part is devoted to the defluorinated phosphate chemical composition study by the laser-spark emission spectrometry method (LIBS). The LIBS method application for the defluorinated phosphate chemical composition analysis is proposed, which allows the production process parameters real-time control. The plasma spectra measurement and interpretation results from the ready-made defluorinated phosphate sample, obtained using the LIBS method, are presented.

scholarly journals The gaseous hydrocarbon fuel combustion process diagnostics using laser-spark emission spectrometry

2021 ◽  
Vol 2094 (2) ◽  
pp. 022055
Author(s):  
M A Vaganov ◽  
V I Kazakov
Keyword(s):  
Spectral Characteristics ◽  
Combustion Process ◽  
Hydrocarbon Fuel ◽  
Fuel Combustion ◽  
Plasma Radiation ◽  
Emission Spectrometry ◽  
Gaseous Hydrocarbon ◽  
Study Results ◽  
Laser Spark ◽  
Combustion Processes

Abstract To solve the gaseous hydrocarbon fuel combustion process control and diagnostics problem, it is proposed to apply the laser-spark emission spectrometry methods. In propane-air mixture combustion, three modes are investigated: stoichiometric combustion, an enriched mixture, and a lean mixture. A laboratory stand has been developed to study combustion processes by laser-spark emission spectrometry. The plasma radiation spectral characteristics an experimental study results formed in a flame when exposed to laser radiation are presented.

scholarly journals Correction: Yu, D.Q., et al. Microscopic Characteristic and Chemical Composition Analysis of Three Medicinal Plants and Surface Frosts. Molecules 2019, 24, 4548

Molecules ◽  
2021 ◽  
Vol 26 (2) ◽  
pp. 379
Author(s):  
Da Qing Yu ◽  
Xiao Jing Han ◽  
Ting Yu Shan ◽  
Rui Xu ◽  
Jin Hu ◽  
...  
Keyword(s):  
Chemical Composition ◽  
Medicinal Plants ◽  
Composition Analysis ◽  
Microscopic Characteristic ◽  
Chemical Composition Analysis

The authors would like to correct an error in the title paper [...]

Chemical composition analysis of carbohydrate fragmentation products

2021 ◽  
Vol 156 ◽  
pp. 105112
Author(s):  
Samin Fathalinejad ◽  
Esben Taarning ◽  
Peter Christensen ◽  
Jan H. Christensen
Keyword(s):  
Chemical Composition ◽  
Composition Analysis ◽  
Chemical Composition Analysis

Mechanical Behaviour of CoCrMo Alloy with Si Content

2015 ◽  
Vol 754-755 ◽  
pp. 1017-1022 ◽  
Author(s):  
Petrică Vizureanu ◽  
Mirabela Georgiana Minciună ◽  
Dragoş Cristian Achiţei ◽  
Andrei Victor Sandu ◽  
Kamarudin Hussin
Keyword(s):  
Tensile Strength ◽  
Chemical Composition ◽  
Testing Machine ◽  
Base Material ◽  
Optical Emission ◽  
Experimental Tests ◽  
Optical Emission Spectrometry ◽  
Emission Spectrometry ◽  
Standard Samples

.The paper present aspects about the obtaining of non-precious dental alloys (type CoCrMo and CoCrMoSi7), the determination of chemical composition by optical emission spectrometry and the experimental tests for determining the tensile strength, made on standard plate samples. The base material used in experiments was a commercial alloy, from CoCrMo system, which belongs to the class of dental non-precious alloys, intended to medical applications. The obtaining of studied alloy was made on arc re-melting installation, under vacuum, type MRF ABJ 900. The process followed to realize a rapid melting, with a maximum admissible current intensity. The samples for tests were obtained by casting in an electric arc furnace, under vacuum, in optimal conditions for melting and solidification and processing by electro-erosion, to eliminate all the disturbing factors which come by processing conditions for the samples. The determination of chemical composition for cobalt based alloys, by optical emission spectrometry, was made on SpectromaxX equipment with spark. The electrical discharge is made with the elimination of an energy quantity, fact which determine plasma forming and light issue. Tensile tests for standard samples, made from cobalt based alloy, was made on Instron 3382 testing machine, and assisted by computer. The obtained results are: elongation, elasticity modulus, tensile strength and offer complete information about the analyzed mechanical properties. For the certitude of obtained experimental results, the tests were made on samples with specific dimensions according ISO 6892-1:2009(E) standard, both for the tensile strength, and also machine operation.

Research on Process Mineralogy of Potassium-Rich Shale

2010 ◽  
Vol 158 ◽  
pp. 197-203 ◽  
Author(s):  
Jie Liu ◽  
Yue Xin Han ◽  
Wan Zhong Yin
Keyword(s):  
Chemical Composition ◽  
Mineral Composition ◽  
Potassium Feldspar ◽  
Composition Analysis ◽  
Research Results ◽  
Dsc Analyses ◽  
Process Mineralogy ◽  
Mineral Compositions ◽  
Chemical Composition Analysis

The process mineralogy of potassium-rich shale from Chaoyang of Liaoning, China, was studied. Research results showed there are much less variety and smaller quantities in mineral compositions. Calculated mineral composition by means of chemical composition analysis combined with XRD, MLA, IR and TG-DSC analyses showed that main minerals with were Potassium-feldspar, muscovite, biotite and illite, and gangue minerals were quartz and small amounts of hematite. Potassium-rich minerals such as potassium-feldspar and muscovite contact smoothly with quartz respectively, and there was the direction arrangement among potassium-feldspar, quartz and muscovite in the shale. And quartz and hematite were main cement in the shale. The influences of the research results on the potassium extraction from potassium-rich shale were distinct.

Determination of Al, Cu, Ni in Zr-Based Amorphous Alloy by Inductively Coupled Plasma Atomic Emission Spectrometry

2015 ◽  
Vol 1095 ◽  
pp. 218-221
Author(s):  
Lan Ma ◽  
Guang He Qin ◽  
Qiong Yu ◽  
Jing Zhou
Keyword(s):  
Amorphous Alloy ◽  
Inductively Coupled Plasma ◽  
Atomic Emission ◽  
Spectral Lines ◽  
Atomic Emission Spectrometry ◽  
Emission Spectrometry ◽  
Plasma Atomic Emission ◽  
Plasma Atomic Emission Spectrometry ◽  
Inductively Coupled

A Method was studied for the determination of Al、Cu、Ni in Zr-based amorphous alloy by inductively coupled plasma atomic emission spectrometry (ICP-AES). Samples were dissolved by hydrochloric acid,nitric acid and hydrofluoric acid,analytical spectral lines for aluminum,copper,nickle are 308.215nm,327.396nm and 231.604nm.Interference of zinc was eliminated by the matrix-matching method, the experiments were done with optimized Operating Parameters. The correlation coefficients of the calibration curve are all 0.999,detection limits are 0.0010%,0.005% and 0.0006% respectively,and the range of recovery is 98%-104%.

scholarly journals A Label-free, Fast and High-specificity Technique for Plant Cell Wall Imaging and Composition Analysis

2020 ◽  
Author(s):  
Huimin Xu ◽  
Yuanyuan Zhao ◽  
Yuanzhen Suo ◽  
Yayu Guo ◽  
Yi Man ◽  
...  
Keyword(s):  
Cell Wall ◽  
Chemical Composition ◽  
Raman Scattering ◽  
Plant Cell ◽  
Cell Walls ◽  
Plant Cell Wall ◽  
Composition Analysis ◽  
Plant Cell Walls ◽  
Label Free ◽  
Wall Imaging

Abstract Background: Cell wall imaging can considerably permit direct visualization of the molecular architecture of cell walls and provide the detailed chemical information on wall polymers, which is imperative to better exploit and use the biomass polymers; however, detailed imaging and quantifying of the native composition and architecture in the cell wall remains challenging.Results: Here, we describe a label-free imaging technology, coherent Raman scattering microscopy (CRS), including coherent anti-Stokes Raman scattering (CARS) microscopy and stimulated Raman scattering (SRS) microscopy, which images the major structures and chemical composition of plant cell walls. The major steps of the procedure are demonstrated, including sample preparation, setting the mapping parameters, analysis of spectral data, and image generation. Applying this rapid approach, which will help researchers understand the highly heterogeneous structures and organization of plant cell walls.Conclusions: This method can potentially be incorporated into label-free microanalyses of plant cell wall chemical composition based on the in situ vibrations of molecules.

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