scholarly journals Production and investigation of powders for additive synthesis from a new beta-solidifying TiAl-based alloy

2021 ◽  
Vol 2144 (1) ◽  
pp. 012004
Author(s):  
P V Panin ◽  
I A Bogachev ◽  
E A Lukina

Abstract Chemical composition, structure, and technological properties have been investigated for metal powder compositions (MPCs) of a new six-component TiAl-based alloy with Gd microadditions: Ti-31.0Al-2.5V-2.5Nb-2.5Cr-0.4Gd, wt.% (Ti-44.5Al-2V-1Nb-2Cr-0.1Gd, at.%). Three MPCs fractions (10–63, 40–100, 80–120 μm) were produced by electrode induction melting and inert gas atomization technique and targeted for the additive synthesis of parts. It is shown that the chemical composition of the MPCs for the main elements corresponds to that of the electrode. In contrast, a 1.5-fold increase of the oxygen content in the MPCs was observed, which is being the result of natural oxidation of powder particles upon air environment due to developed specific surface. It has been determined that the phase composition of the MPCs (γ+α(α2)+β) differs from the equilibrium phase composition of the electrode (γ+α2)+β0/B2) and corresponds to a rapidly quenched metastable state, which indicates high solidification rates in the atomization process, exceeding critical cooling rates of the alloy. The technological properties, specifically the powder flowability, were found to be improved for 40–100 and 80–120 μm fractions, making them applicable for additive synthesis of parts from the studied alloy by selective electron-beam melting method

2013 ◽  
Vol 203-204 ◽  
pp. 351-354 ◽  
Author(s):  
Grzegorz Moskal ◽  
Krzysztof Szymański ◽  
Agnieszka Tomaszewska ◽  
Hanna Myalska

In this paper results of tests concerning the WC/Co fine-crystalline composite powders type 88/12 and 83/17 provided for thermal spraying of layers resistant to abrasion are presented. Tests which characterize basic technological properties were performed since these properties are essential from thermal spraying point of view. Microstructural properties are essential as well because they allow evaluation of morphology of powders by SEM method with an analysis of chemical composition in micro-areas. Moreover, the phase composition was characterized by XRD in macro scale and by EBSD in microareas including distribution maps of individual phase components in all particles of the powders.


Author(s):  
V. V. Kozlov ◽  
A. P. Shevchik ◽  
S. A. Suvorov ◽  
N. V. Arbuzova ◽  
D. V. Kuznetsov

The modeling technique was proposed for the phase formation in the CaO‒MgO‒Al2O3‒SiO2‒FeO‒Fe2O3multicomponent oxide system. The technique can be used to predict the equilibrium phase composition for both the refractory and refractory-slag systems, as well as to modify the metallurgical slag's chemical composition, to extent the metallurgical unit's refractory service life, and in order to attaint the refractory-slag systems the mineral binding properties.Ill. 2. Ref. 7. Tab. 8.


2007 ◽  
Vol 1 (1-2) ◽  
pp. 11-17
Author(s):  
M.G. Pavlovic ◽  
B.M. Jovic ◽  
V.D. Jovic ◽  
U. Lacnjevac ◽  
V.M. Maksimovic

Electrodeposition of Ni-Mo alloy powders from ammonium sulfate and ammonium chloride containing electrolytes of different Ni/Mo ions concentration ratios was investigated by polarization measurements. The morphology, chemical composition and phase composition of electrodeposited Ni-Mo alloy powders were investigated using DSC, TGA, SEM, EDS and XRD analysis. EDS results showed that powder composition depends on Ni/Mo ions concentration ratio, as well as on the position where the EDS analysis was performed. As-deposited alloy powders were nanocrystalline showing no XRD peaks with undefined morphology (SEM). After recrystallization for 2 h in N2 atmosphere at 600?C the presence of NiMoO4 phase was identified in the powder electrodeposited from chloride electrolyte at the Ni/Mo ions concentration ratio 1/3, with well defined crystalline powder particles.


2020 ◽  
Vol 2020 (12) ◽  
pp. 1439-1445
Author(s):  
I. O. Bannykh ◽  
O. A. Bannykh ◽  
L. G. Rigina ◽  
E. N. Blinova ◽  
K. Yu. Demin ◽  
...  

2020 ◽  
Vol 236 ◽  
pp. 116000 ◽  
Author(s):  
Biljana M. Pejić ◽  
Ana D. Kramar ◽  
Bratislav M. Obradović ◽  
Milorad M. Kuraica ◽  
Andrijana A. Žekić ◽  
...  

2015 ◽  
Vol 57 (4) ◽  
pp. 348-355 ◽  
Author(s):  
S. V. Stefanovsky ◽  
O. I. Stefanovskaya ◽  
S. E. Vinokurov ◽  
S. S. Danilov ◽  
B. F. Myasoedov

2021 ◽  
Vol 316 ◽  
pp. 1019-1024
Author(s):  
O. A. Ignatova ◽  
A. A. Dyatchina

The paper presents the studies’ results of chemical composition, structure, and physico-mechanical properties of high-calcium ashes from the Kansk-Achinsk coals (2017-2019 selection). It was found that ash has a complex poly-mineral composition and contains hydraulically active minerals and oxides of СаОfr, β-C2S, CA, C3A, C4AF, C2F, CaSO4. According to the content of CaOfr, MgO does not meet standards’ requirements. The uniformity of the volume change is maintained by the composition with 50% of cement. The structure and hardening kinetics of ash and ash-cement stone compositions, obtained from the test of normal density, were analyzed. It was established that the hardening of compositions with ash from the Kansk-Achinsk coals was largely influenced by ash minerals. An equivalent amount of cement in composite binders cannot be replaced. In order to obtain a positive effect, compositions with ash instead cement of no more than 30% and a part of fine aggregate, without exceeding the ratio of ash: cement = 1: 1, should be used.


2018 ◽  
Vol 383 ◽  
pp. 31-35 ◽  
Author(s):  
Alexey Rodin ◽  
Nataliya Goreslavets

The study of diffusion processes in the aluminum - copper system was carried out at the temperature 350 and 520 °C. Special attention was paid on the chemical composition of the system near Al/Cu interface. It was determined that the intermediate phases in the system, corresponding to the equilibrium phase diagram, were not formed at low temperature. At high temperature the intermediate phases forms starting with Cu - rich phases. In both cases supersaturated solid solution of copper in aluminum could be observed near the interface.


2016 ◽  
Vol 0 (4(36)) ◽  
pp. 6-27
Author(s):  
М. Б. Галкін ◽  
В. О. Іваниця ◽  
Б. М. Галкін ◽  
Т. О. Філіпова

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