Effect of Powder Feed Rate on Adhesion Strength and Microhardness of APS NiTi Coating: A Microstructural Investigation

Author(s):  
Biswajit Kumar Swain ◽  
Ajit Behera
Author(s):  
Peter Kayode Farayibi

Laser deposition is an advanced manufacturing technology capable of enhancing service life of engineering components by hard-facing their functional surfaces. There are quite a number of parameters involved in the process and also desirable output characteristics. These output characteristics are often independently optimised and which may lead to poor outcome for other characteristics, hence the need for multi-objective optimisation of all the output characteristics. In this study, a laser deposition of Ti-6Al-4V wire and tungsten carbide powder was made on a Ti-6Al-4V substrate with a view to achieve a metallurgical bonded metal matrix composite on the substrate. Single clads were deposited with a desire to optimise the composite clad characteristics (height, width and reinforcement fraction) for the purpose of surface coating. Processing parameters (laser power, traverse speed, wire feed rate, powder feed rate) were varied, the experiment was planned using Taguchi method and output characteristics were analysed using principal component analysis approach. The results indicated that the parameters required for optimised clad height, width, and reinforcement fraction necessary for surface coating is laser power of 1800 W, traverse speed of 200 mm/min, wire feed rate 700 mm/min and powder feed rate of 30 g/min. The powder feed rate was found to most significantly contribute 43.99%, followed by traverse speed 39.77%, laser power 15.87% with wire feed rate having the least contribution towards the multi-objective optimisation. Confirmation results showed that clad width and reinforcement fraction were significantly improved by the optimised parameters. The multi-objective optimisation procedure is a useful tool necessary to identify the process factors required to enhance output characteristics in laser processing.


Author(s):  
Shaowu Liu ◽  
Michel Moliere ◽  
Hanlin Liao

Abstract In this work; a novel liquid fuel HVOF process fueled with ethanol was used to prepare 75wt%Cr3C2–25wt%NiCr coatings on AISI304 stainless steel substrate. Taguchi method was employed to optimize the spray parameters (ethanol flow rate; oxygen flow rate; powder feed rate and standoff distance) to achieve better erosion resistance at 90° impact angle. The results indicated that ethanol flow rate and oxygen flow rate were identified as the highly contributing parameters on the erosion wear loss. The important sequence of the spray parameter is ethanol flow rate > oxygen flow rate > standoff distance > powder feed rate. The optimal spray parameter (OSP) for minimum erosion wear loss was obtained under ethanol flow rate of 28slph; oxygen flow rate of 420slpm; powder feed rate of 76.7 g/min and standoff distance of 300mm. The phase composition; microstructure; hardness; porosities; and the erosion wear behaviors of the coatings have been studied in detail. Besides; erosion wear testing of the optimized coating was conducted at 30°; 60° and 90° impact angle using air jet erosion testing machine. The SEM images of the erodent samples were taken to analyze the erosion mechanism.


Metals ◽  
2020 ◽  
Vol 10 (4) ◽  
pp. 521 ◽  
Author(s):  
Qiang Zhang ◽  
Siyu Zhang ◽  
Min Zheng ◽  
Yongchao Ou ◽  
Shang Sui ◽  
...  

A near β titanium alloy, Ti5Al2Sn2Zr4Mo4Cr, was fabricated by directed energy deposition (DED) with different powder feed rates to investigate the formation of fully equiaxed β grains. A two-dimensional numerical model was developed to investigate the thermal conditions of the molten pool. Experimental results showed that the formation of an epitaxial cellular structure at the bottom of the molten pool is almost unavoidable. An increase in the powder feed rate produces a moderate thermal condition and promotes the formation of equiaxed grains in a single cladding layer. However, it could not guarantee the formation of a fully equiaxed microstructure in a block sample. From a low to high powder feed rate, fully columnar, mixed equiaxed–columnar, and fully equiaxed microstructures were obtained. Grain morphology was also affected by the remolten process. Increasing the powder feed rate reduced the remolten depth and broke the continuity of the epitaxial cellular structure, leading to different grain morphologies.


2006 ◽  
Vol 15-17 ◽  
pp. 193-198 ◽  
Author(s):  
Marek Piec ◽  
Leszek Adam Dobrzański ◽  
Krzysztof Labisz ◽  
Ewa Jonda ◽  
Andrzej Klimpel

Investigations include alloying the X38CrMoV5-3 hot-work tool steel surface layer with the tungsten carbide, using the high power diode laser (HPDL). The tungsten carbide ceramic particles of the medium grain size according to FSSS = 50 /m were introduced using the rotor conveyer to improve the properties of the surface layer. The powder feed rate was set at the steady level of 8.64g/min. Remelting and alloying were carried out several times in the laser power range of 1.2 – 2.3 kW in the remelting/alloying, alloying/remelting sequences. The structural mechanism was determined of gradient layer development, effect was studied of alloying parameters, gas protection method, and powder feed rate on its mechanical properties, and especially on its hardness, abrasive wear resistance, and roughness. Structure changes were revealed consisting, in particular, in its refining, and also hardness and microhardness changes in comparizon to the nonremelted steel. Examination results obtained with the EDX microanalysis, surface and linear analysis of the chemical composition, as well as the X-ray qualitative phase analysis are presented.


MRS Advances ◽  
2017 ◽  
Vol 2 (26) ◽  
pp. 1381-1386 ◽  
Author(s):  
Takeshi Okuno ◽  
Yasuyuki Kaneno ◽  
Takuto Yamaguchi ◽  
Takayuki Takasugi ◽  
Satoshi Semboshi ◽  
...  

ABSTRACTNi base intermetallic alloy coating was fabricated by laser cladding, controlling the laser power and powder feed rate. Atomized powder of the Ni base intermetallic alloy was laser-cladded on the substrate of stainless steel 304. The hardness and microstructure of the clad layers were investigated by Vickers hardness test, SEM, XRD and TEM observations. The hardness of the cladding layer was affected by the dilution with the substrate; it increased with decreasing laser power and increasing powder feed rate. By optimizing the dilution with the substrate, the cladding layer with an almost identical hardness level to that of the Ni base intermetallic alloy fabricated by ingot metallurgy was obtained. The TEM observations revealed that a very fine-sized microstructure composed of Ni3Al and Ni3V was partially formed even in the as-cladded state. After annealing, the two-phase microstructure composed of Ni3Al and Ni3V was developed in the cladding layer, resulting in enhanced hardness in the cladding layers fabricated in the majority of cladding conditions.


Coatings ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1085
Author(s):  
Bingtao Lin ◽  
Baohong Zhang ◽  
Minglong Ma ◽  
Kui Zhang ◽  
Yongjun Li ◽  
...  

In this study, the effects of the six technological parameters of atmospheric plasma spraying (including spraying current, spraying distance, main gas flow, auxiliary gas flow, spraying speed, and powder feeding rate) on the microhardness, density, and rate of deposition of nanoparticle cluster-oxidized yttria partially stabilized zirconia (YSZ) powder-ceramic coating were investigated through an orthogonal experiment. The structures of the powder and coating were observed by a scanning electron microscope. The hardness measurements were carried out on the samples, and the cross-section experimental results were analyzed by combining the structure of the coating and range analysis method, thereby obtaining the optimized technological parameters. The results show that the coating was primarily composed of melted ZrO2, and the coating section was a characteristic of concave–convex occlusions. Mechanical bonding played the dominant role. Main gas flow was the primary influencing parameter of performances of the atmospheric plasma spraying ZrO2 coating, followed by spraying current, auxiliary gas flow, powder feed rate, spraying speed, and spraying distance, successively. The optimal technological parameters for atmospheric plasma spraying ZrO2 coating were 75 standard cubic foot per hour (SCFH) of main gas flow, 875 A of spraying current, 45 SCFH of auxiliary gas flow, 30 g/min of powder feed rate, 400 mm/s of spraying speed, and 85 mm of spraying distance. The bonding microhardness, density, and rate of deposition of the prepared coating were HV388, 5.25 g/cm3, and 31.58%, respectively. The electrode potential and corrosion resistance of the prepared coating increased remarkably compared with that of the substrate, whereas the corrosion current decreased significantly.


Author(s):  
Fanrong Kong ◽  
Radovan Kovacevic

The present work studies the heat and mass transfer process in the laser multilayered cladding of H13 tool steel powder by numerical modeling and experimental validation. A solid-liquid-gas unified transient model was developed to investigate the evolution of temperature distribution and flow velocity of the liquid phase in the molten pool. In this model, an enthalpy-porosity approach was applied to deal with the solidification and melting occurring in the clad, and a level-set method was used to track the evolution of the molten pool free surface. Moreover, heat loss due to forced convection and heat radiation and laser heat input occurring on the top surface of deposited layer and substrate have been incorporated into the source term of governing equations. The effects of laser power, scanning speed, and powder feed rate on the dilution and height of the multilayered clad are investigated based on the numerical model and experimental measurement. The results show that increasing the laser power and powder feed rate, or reducing the scanning speed, can increase the clad height and directly influence the remelted depth of each layer of deposition. The numerical results have a qualitative agreement with the experimental measurements.


2011 ◽  
Vol 22 (2) ◽  
pp. 162-166 ◽  
Author(s):  
Ranjit M. Dhenge ◽  
James J. Cartwright ◽  
David G. Doughty ◽  
Michael J. Hounslow ◽  
Agba D. Salman

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