Microwave Oven Drying in the Gravimetric Phosphorus Method
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Abstract The gravimetric quinolinium molybdophosphate method for determining P2O5 in fertilizers, AOAC 2.026–2.028, has been modified to permit the precipitate to be dried in a microwave oven rather than a conventional drying oven. After the yellow quinolinium molybdophosphate precipitate is formed, cleaned up, and washed, it is placed in a microwave oven at 600 watts until dry. The quantity of precipitate remaining after microwave drying was equal to that obtained by drying according to AOAC 2.028 for several fertilizer samples. A distinct advantage of the described method is that the yellow precipitate will not char with reasonably excessive drying. Also, much less energy is expended with the microwave oven than with the drying oven.