Real-Space Analysis

Author(s):  
Andreas Michels

Spin-misalignment correlations in real space are the subject of this chapter. The correlation function and correlation length of the spin-misalignment SANS cross section are introduced, their properties are discussed within the context of micromagnetic theory, and selected experimental data on Nd-Fe-B-based permanent magnets and nanocrystalline elemental soft (Cobalt and Nickel) and hard (Gadolinium and Terbium) magnets are reviewed.

2019 ◽  
Vol 75 (2) ◽  
pp. 307-313 ◽  
Author(s):  
Sebastian Schenk ◽  
Eva Maria Zollner ◽  
Oliver Krahn ◽  
Berit Schreck ◽  
René Hammer ◽  
...  

The atomically resolved real-space structure of a long-range-ordered dodecagonal quasicrystal is determined based on scanning tunnelling microscopy. For the BaTiO3-derived oxide quasicrystal which spontaneously forms on a Pt(111) surface, 8100 atomic positions have been determined and are compared with an ideal Niizeki–Gähler tiling. Although the Niizeki–Gähler tiling has a complex three-element structure, the abundance of the triangle, square and rhomb tiling elements in the experimental data closely resembles the ideal frequencies. Similarly, the frequencies of all possible next-neighbour tiling combinations are, within the experimental uncertainty, identical to the ideal tiling. The angular and orientational distributions of all individual tiling elements show the characteristics of the dodecagonal quasicrystal. In contrast, the analysis of the orientation of characteristic and more complex tiling combinations indicates the partial decomposition of the quasicrystal into small patches with locally reduced symmetry. These, however, preserve the long-range quasicrystal coherence. The symmetry reduction from dodecagonal to sixfold is assigned to local interaction with the threefold substrate. It leads to atomic flips which preserve the number of quasicrystal tiling elements.


Author(s):  
N. Merk ◽  
A. P. Tomsia ◽  
G. Thomas

A recent development of new ceramic materials for structural applications involves the joining of ceramic compounds to metals. Due to the wetting problem, an interlayer material (brazing alloy) is generally used to achieve the bonding. The nature of the interfaces between such dissimilar materials is the subject of intensive studies and is of utmost importance to obtain a controlled microstructure at the discontinuities to satisfy the demanding properties for engineering applications . The brazing alloy is generally ductile and hence, does not readily fracture. It must also wett the ceramic with similar thermal expansion coefficient to avoid large stresses at joints. In the present work we study mullite-molybdenum composites using a brazing alloy for the weldment.A scanning electron micrograph from the cross section of the joining sequence studied here is presented in Fig. 1.


Author(s):  
J.P. Schroeter ◽  
M.A. Goldstein ◽  
J.P. Bretaudiere ◽  
L.H. Michael ◽  
R.L. Sass

We have recently established the existence of two structural states of the Z band lattice in cross section in cardiac as well as in skeletal muscle. The two structural states are related to the contractile state of the muscle. In skeletal muscle at rest, the Z band is in the small square (ss) lattice form, but tetanized muscle exhibits the basket weave (bw) form. In contrast, unstimu- lated cardiac muscle exhibits the bw form, but cardiac muscles exposed to EGTA show the ss form.We have used two-dimensional computer enhancement techniques on digitized electron micrographs to compare each lattice form as it appears in both cardiac and skeletal muscle. Both real space averaging and fourier filtering methods were used. Enhanced images were displayed as grey-scale projections, as contour maps, and in false color.There is only a slight difference between the lattices produced by the two different enhancement techniques. Thus the information presented in these images is not likely to be an artifact of the enhancement algorithm.


Author(s):  
T. A. Epicier ◽  
G. Thomas

Mullite is an aluminium-silicate mineral of current interest since it is a potential candidate for high temperature applications in the ceramic materials field.In the present work, conditions under which the structure of mullite can be optimally imaged by means of High Resolution Electron Microscopy (HREM) have been investigated. Special reference is made to the Atomic Resolution Microscope at Berkeley which allows real space information up to ≈ 0.17 nm to be directly transferred; numerous multislice calculations (conducted with the CEMPAS programs) as well as extensive experimental through-focus series taken from a commercial “3:2” mullite at 800 kV clearly show that a resolution of at least 0.19 nm is required if one wants to get a straightforward confirmation of atomic models of mullite, which is known to undergo non-stoichiometry associated with the presence of oxygen vacancies.Indeed the composition of mullite ranges from approximatively 3Al2O3-2SiO2 (referred here as 3:2-mullite) to 2Al2O3-1SiO2, and its structure is still the subject of refinements (see, for example, refs. 4, 5, 6).


2015 ◽  
Vol 11 (2) ◽  
pp. 2972-2978
Author(s):  
Fouad A. Majeed ◽  
Yousif A. Abdul-Hussien

In this study the calculations of the total fusion reaction cross section have been performed for fusion reaction systems 17F + 208Pb and 15C + 232Th which involving halo nuclei by using a semiclassical approach.The semiclassical treatment is comprising the WKB approximation to describe the relative motion between target and projectile nuclei, and Continuum Discretized Coupled Channel (CDCC) method to describe the intrinsic motion for both target and projectile nuclei. For the same of comparsion a full quantum mechanical clacualtions have been preforemd using the (CCFULL) code. Our theorticalrestuls are compared with the full quantum mechaincialcalcuations and with the recent experimental data for the total fusion reaction  checking the stability of the distancesThe coupled channel calculations of the total fusion cross section σfus, and the fusion barrier distribution Dfus. The comparsion with experiment proves that the semiclassiacl approach adopted in the present work reproduce the experimental data better that the full quantal mechanical calcautions. 


Author(s):  
Л. Р. Маилян ◽  
С. А. Стельмах ◽  
Е. М. Щербань ◽  
М. П. Нажуев

Состояние проблемы. Железобетонные элементы изготавливаются, как правило, по трем основным технологиям - вибрированием, центрифугированием и виброцентрифугированием. Однако все основные расчетные зависимости для определения их несущей способности выведены, исходя из основного постулата - постоянства и равенства характеристик бетона по сечению, что реализуется лишь в вибрированных колоннах. Результаты. В рамках диаграммного подхода предложены итерационный, приближенный и упрощенный способы расчета несущей способности железобетонных вибрированных, центрифугированных и виброцентрифугированных колонн. Выводы. Расчет по диаграммному подходу показал существенно более подходящую сходимость с опытными данными, чем расчет по методике норм, а также дал лучшие результаты при использовании дифференциальных характеристик бетона, чем при использовании интегральных и, тем более, нормативных характеристик бетона. Statement of the problem. Reinforced concrete elements are typically manufactured according to three basic technologies - vibration, centrifugation and vibrocentrifugation. However, all the basic calculated dependencies for determining their bearing capacity were derived using the main postulate, i.e., the constancy and equality of the characteristics of concrete over the cross section, which is implemented only in vibrated columns. Results. Within the framework of the diagrammatic approach, iterative, approximate and simplified methods of calculating the bearing capacity of reinforced concrete vibrated, centrifuged and vibrocentrifuged columns are proposed. Conclusions. The calculation according to the diagrammatic approach showed a significantly better convergence with the experimental data than that using the method of norms, and also performs better when using differential characteristics of concrete than when employing integral and particularly standard characteristics of concrete.


2019 ◽  
Vol 108 (1) ◽  
pp. 11-17
Author(s):  
Mert Şekerci ◽  
Hasan Özdoğan ◽  
Abdullah Kaplan

Abstract One of the methods used to treat different cancer diseases is the employment of therapeutic radioisotopes. Therefore, many clinical, theoretical and experimental studies are being carried out on those radioisotopes. In this study, the effects of level density models and gamma ray strength functions on the theoretical production cross-section calculations for the therapeutic radioisotopes 90Y, 153Sm, 169Er, 177Lu and 186Re in the (n,γ) route have been investigated. TALYS 1.9 code has been used by employing different level density models and gamma ray strength functions. The theoretically obtained data were compared with the experimental data taken from the literature. The results are presented graphically for better interpretation.


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