Total-scattering-based automatic centring of capillary samples within powder diffractometers
2008 ◽
Vol 41
(6)
◽
pp. 1038-1045
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Keyword(s):
A computer-controlled method for the automatic mechanical centring of a powder capillary sample onto the rotation centre of a powder diffractometer, using total scattering of the radiation beam into one-dimensional or two-dimensional detectors, and only a 90° rotation of the sample stage, is described. This method is particularly useful for situations where powder capillaries are within non-ambient experimental apparatus or loadedviaan automatic sample changer. Irregularly shaped samples, potentially subject to absorption effects, are aligned and centred on the sample's `scattering centre'.
1966 ◽
Vol 25
◽
pp. 46-48
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2014 ◽
Vol 12
(6)
◽
pp. 485-506
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Keyword(s):
1982 ◽
Vol 14
(1-2)
◽
pp. 241-261
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Keyword(s):
2010 ◽
Vol 7
◽
pp. 90-97
Keyword(s):
2016 ◽
Vol 11
(1)
◽
pp. 119-126
◽
2012 ◽
Vol 9
(1)
◽
pp. 47-52
Keyword(s):