Experimental Study of Ductile Fracture for Non-Aligned Multiple Flaws in a Plate

Author(s):  
Katsumasa Miyazaki ◽  
Kunio Hasegawa ◽  
Koichi Saito ◽  
Bostjan Bezensek

The fitness-for-service code requires the characterization of non-aligned multiple flaws for the flaw evaluation, which is performed using a flaw proximity rule. Worldwide almost all codes provide own proximity rule, often with unclear technical bases of the application of proximity rule to ductile fracture. To clarify the appropriate proximity rule for non-aligned multiple flaws in fully plastic fracture, fracture tests on flat plate specimen with non-aligned multiple through wall flaws were conducted at ambient temperature. The emphasis of this study was put on the flaw alignment rule, which determines whether non-aligned flaws are treated as independent or aligned onto the same plane for the purpose of flaw evaluations. The effects of the flaw separation and flaw size on the maximum load were investigated. The experimental results were compared with the estimations of the collapse load using the alignment rules in the ASME Section XI, BS7910 and API 579-1 codes. A new estimation procedure specific to the fully plastic fracture was proposed and compared with the comparison with the experimental results.

Author(s):  
Katsumasa Miyazaki ◽  
Kunio Hasegawa ◽  
Koichi Saito

The fitness-for-service codes require the characterization of non-aligned multiple flaws for flaw evaluation, which is performed using a flaw proximity rule. Worldwide, almost all such codes provide their own proximity rule, often with unclear technical bases of the application of proximity rule to ductile or fully plastic fracture. In particular, the effect of flaw dimensions of multiple surface flaws on fully plastic fracture of non-aligned multiple flaws had not been clear. To clarify the effect of the difference of part through-wall and through-wall flaws on the behavior of fully plastic fracture, the fracture tests of flat plate specimens with non-aligned multiple part through-wall flaws were conducted. When the flaw depth a was shallow with 0.4 in ratio of a to thickness t, the maximum load Pmax occurred at penetration of multiple flaws and the effect of vertical distance of non-aligned multiple flaws H on Pmax was not so significant. However, when flaw depth was deep with 0.8 in a/t, Pmax occurred after penetration of flaws and the effect of H on Pmax could be seen clearly. It was judged that the through-wall flaw tests were appropriate for discussion of the effect of H on Pmax and the alignment rule of multiple flaws. In addition, in order to clarify the appropriate length parameter to estimate Pmax of test specimens with dissimilar non-aligned through-wall multiple flaws, the fracture tests of plate specimens were also conducted. The effect of different flaw length on Pmax was discussed with maximum, minimum and averages of dissimilar non-aligned multiple flaw lengths. Experimental results showed that the maximum length lmax would be an appropriate length parameter to estimate Pmax, when the non-aligned multiple through-wall flaws were dissimilar.


Author(s):  
Fuminori Iwamatsu ◽  
Katsumasa Miyazaki ◽  
Hidekazu Takazawa ◽  
Koichi Saito

The fitness-for-service codes such as the ASME Boiler and Pressure Vessel Code Section XI require the characterization of non-aligned multiple flaws for flaw evaluation, which is performed using a flaw alignment rule. Worldwide, almost all such codes provide their own alignment rule, often with an unclear technical basis regarding the application of the rule to plastic collapse due to ductile fracture as prescribed by limit load analysis based on a net-section approach. Therefore, evaluation procedures to calculate collapse load for non-aligned multiple flaws have been proposed in various experimental and analytical studies. In these proposals, a collapse load for non-aligned multiple flaws is evaluated using the net-section stress approach in consideration of the ratio of a distance between flaws to a flaw length parameter. However, because each study proposes its own appropriate length and distance parameters, which are based on a few experimental results limited to that study, the applicability of the proposed parameters to evaluation of collapse load for arbitrary flaw sizes and locations is unclear. In this study, we performed fracture test result on a flat plate with two through-wall flaws in order to determine appropriate parameters for the evaluation procedure of the collapse load for non-aligned multiple flaws. Appropriate parameters were determined by correlation coefficients obtained by comparison of maximum loads of fracture tests and collapse loads of evaluation with various parameters. We found that the appropriate parameters to apply the alignment rule with equations to evaluate collapse load for non-aligned flaws were the ratio of the vertical or direct distance between flaws to the maximum or average flaw length.


Author(s):  
Masao Itatani ◽  
Takuya Ogawa ◽  
Toshiyuki Saito ◽  
Chihiro Narazaki ◽  
Kazuo Ogawa

The objective of this study is to establish the fracture assessment method for nuclear power components made of Ni-based alloy weld metal. Fracture tests of butt welded plates of alloys 182 and 82 with a surface flaw were conducted in tension at 300°C. The dimensions and shapes of weld groove of the test plates were intended to simulate the weld joint of BWR shroud support. Semi-elliptical surface flaws were introduced by EDM. Fatigue pre-crack was introduced from an EDM notch for one test plate of alloy 182 to investigate the effect of crack tip shape on the fracture. It was found that the fracture load is conservatively estimated by using plastic collapse load with 2.7Sm for flow stress. It was also understood that the plastic collapse load using flow stress of actual data of tested materials gives good estimation for the experimental fracture load. The net section stresses at the maximum load of both fatigue pre-cracked and EDM notched alloy 182 test plates were almost the same. Consequently, the fracture mode of butt welded joint of alloys 182 and 82 at 300°C is characterized to be plastic collapse.


Author(s):  
Fuminori Iwamatsu ◽  
Katsumasa Miyazaki ◽  
Koichi Saito ◽  
Tetsuya Hamanaka ◽  
Yoshiaki Takahashi

Flaw characterization of multiple flaws for ductile fractures was verified by comparing results of flat plate fracture tests and flaw combination rules in typical fitness-for-service codes. Single or double coplanar surface flaws were introduced into flat plate specimens made of Type 304 stainless steel using an electric discharge machine. Fracture tests of sixteen flat plates with flaws were conducted using a tensile testing machine. According in results of the fracture tests, collapse behavior for flat plates with double coplanar flaws was divided into two broad categories. One was coalescence behavior, in which the double flaws combined before the wall was penetrated. The other was penetration behavior, in which the wall was penetrated before coalescence. Rules for characterizing multiple flaws in fitness-for-service codes in Japan, the United States, and Europe were surveyed in order to compare them with test results. When the multiple flaws satisfy the criteria of rules in fitness-for service codes, a single combined flaw is assumed to conservatively estimate the limit load analysis for a ductile fracture. Flaw combination rules in typical fitness-for-service codes were found to conservatively estimate ductile fractures.


Author(s):  
Tian Lu ◽  
Qinxue Chen ◽  
Zeyu Liu

Although cyclo[18]carbon has been theoretically and experimentally investigated since long time ago, only very recently it was prepared and directly observed by means of STM/AFM in condensed phase (Kaiser et al., <i>Science</i>, <b>365</b>, 1299 (2019)). The unique ring structure and dual 18-center π delocalization feature bring a variety of unusual characteristics and properties to the cyclo[18]carbon, which are quite worth to be explored. In this work, we present an extremely comprehensive and detailed investigation on almost all aspects of the cyclo[18]carbon, including (1) Geometric characteristics (2) Bonding nature (3) Electron delocalization and aromaticity (4) Intermolecular interaction (5) Reactivity (6) Electronic excitation and UV/Vis spectrum (7) Molecular vibration and IR/Raman spectrum (8) Molecular dynamics (9) Response to external field (10) Electron ionization, affinity and accompanied process (11) Various molecular properties. We believe that our full characterization of the cyclo[18]carbon will greatly deepen researchers' understanding of this system, and thereby help them to utilize it in practice and design its various valuable derivatives.


Author(s):  
Tian Lu ◽  
Qinxue Chen ◽  
Zeyu Liu

Although cyclo[18]carbon has been theoretically and experimentally investigated since long time ago, only very recently it was prepared and directly observed by means of STM/AFM in condensed phase (Kaiser et al., <i>Science</i>, <b>365</b>, 1299 (2019)). The unique ring structure and dual 18-center π delocalization feature bring a variety of unusual characteristics and properties to the cyclo[18]carbon, which are quite worth to be explored. In this work, we present an extremely comprehensive and detailed investigation on almost all aspects of the cyclo[18]carbon, including (1) Geometric characteristics (2) Bonding nature (3) Electron delocalization and aromaticity (4) Intermolecular interaction (5) Reactivity (6) Electronic excitation and UV/Vis spectrum (7) Molecular vibration and IR/Raman spectrum (8) Molecular dynamics (9) Response to external field (10) Electron ionization, affinity and accompanied process (11) Various molecular properties. We believe that our full characterization of the cyclo[18]carbon will greatly deepen researchers' understanding of this system, and thereby help them to utilize it in practice and design its various valuable derivatives.


2019 ◽  
Author(s):  
Chem Int

Liquid effluents discharged by hospitals may contain chemical and biological contaminants whose main source is the different substances used for the treatment of patients. This type of rejection can present a sanitary potentially dangerous risk for human health and can provoke a strong degradation of diverse environmental compartments mainly water and soils. The present study focuses on the quality of the liquid effluents of Hassani Abdelkader’s hospital of Sidi Bel-Abbes (West of Algeria). The results reveal a significant chemical pollution (COD: 879 mgO2/L, BOD5: 850 mgO2/L, NH4+ : 47.9 mg/l, NO2- : 4.2 mg/l, NO3- : 56.8 mg/l with respect to WHO standard of 90 mgO2/L, 30 mgO2/L, 0.5 mg/l, 1 mg/l and 1 mg/l respectively). However, these effluents are biodegradable since the ratio COD/BOD5 do not exceeded the value of 2 in almost all samples. The presence of pathogen germs is put into evidence such as pseudomonas, the clostridium, the staphylococcus, the fecal coliforms and fecal streptococcus. These results show that the direct discharge of these effluents constitutes a major threat to human health and the environment.


Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 931
Author(s):  
Ioana-Codruţa Mirică ◽  
Gabriel Furtos ◽  
Ondine Lucaciu ◽  
Petru Pascuta ◽  
Mihaela Vlassa ◽  
...  

The aim of this research was to develop new electrospun membranes (EMs) based on polycaprolactone (PCL) with or without metronidazole (MET)/nano-hydroxyapatite (nHAP) content. New nHAP with a mean diameter of 34 nm in length was synthesized. X-ray diffraction (XRD) and attenuated total reflectance Fourier transform infrared spectroscopy (FTIR-ATR) were used for structural characterization of precursors and EMs. The highest mechanical properties (the force at maximum load, Young’s modulus and tensile strength) were found for the PCL membranes, and these properties decreased for the other samples in the following order: 95% PCL + 5% nHAP > 80% PCL + 20% MET > 75% PCL + 5% nHAP + 20% MET. The stiffness increased with the addition of 5 wt.% nHAP. The SEM images of EMs showed randomly oriented bead-free fibers that generated a porous structure with interconnected macropores. The fiber diameter showed values between 2 and 16 µm. The fiber diameter increased with the addition of nHAP filler and decreased when MET was added. New EMs with nHAP and MET could be promising materials for guided bone regeneration or tissue engineering.


2018 ◽  
Vol 115 (17) ◽  
pp. E3969-E3977 ◽  
Author(s):  
Sasikumar Rajoo ◽  
Pascal Vallotton ◽  
Evgeny Onischenko ◽  
Karsten Weis

The nuclear pore complex (NPC) is an eightfold symmetrical channel providing selective transport of biomolecules across the nuclear envelope. Each NPC consists of ∼30 different nuclear pore proteins (Nups) all present in multiple copies per NPC. Significant progress has recently been made in the characterization of the vertebrate NPC structure. However, because of the estimated size differences between the vertebrate and yeast NPC, it has been unclear whether the NPC architecture is conserved between species. Here, we have developed a quantitative image analysis pipeline, termed nuclear rim intensity measurement (NuRIM), to precisely determine copy numbers for almost all Nups within native NPCs of budding yeast cells. Our analysis demonstrates that the majority of yeast Nups are present at most in 16 copies per NPC. This reveals a dramatic difference to the stoichiometry determined for the human NPC, suggesting that despite a high degree of individual Nup conservation, the yeast and human NPC architecture is significantly different. Furthermore, using NuRIM, we examined the effects of mutations on NPC stoichiometry. We demonstrate for two paralog pairs of key scaffold Nups, Nup170/Nup157 and Nup192/Nup188, that their altered expression leads to significant changes in the NPC stoichiometry inducing either voids in the NPC structure or substitution of one paralog by the other. Thus, our results not only provide accurate stoichiometry information for the intact yeast NPC but also reveal an intriguing compositional plasticity of the NPC architecture, which may explain how differences in NPC composition could arise in the course of evolution.


Sign in / Sign up

Export Citation Format

Share Document