Preparation of ultrafine silicon oxycarbide fiber mats via electrospinning/sol–gel method: Investigation of the solution spinnability

2019 ◽  
Vol 34 (01n03) ◽  
pp. 2040004
Author(s):  
Yixuan Wang ◽  
Ting Zhang ◽  
Xiaoyu Yue ◽  
Junyao Wu ◽  
Wei Gao

Ultrafine silicon oxycarbide (SiOC) fiber mats were prepared through a sol–gel method combined electrospinning technique. The influence of sol–gel solution viscosity on its spinnability has been studied. By partially removing solvents after the sol–gel preparation, the solution could be stably spun and resulted in fiber mats with an average fiber diameter of 560 nm. The formation, morphology and composition of the SiOC fiber mats have been studied by TGA, FT-IR, SEM, XPS and XRD. Due to flexibility and free-standing property, the SiOC fiber mats will have a wide range of applications.

2021 ◽  
Vol 283 ◽  
pp. 128696
Author(s):  
Yixuan Wang ◽  
Zoran Zujovic ◽  
Junyao Wu ◽  
Han Wang ◽  
Wei Gao

Author(s):  
H. Brequel ◽  
G.D. Sorarù ◽  
Florence Babonneau ◽  
Dj. Bahloul-Hourlier ◽  
Stefano Enzo

2019 ◽  
Vol 293 ◽  
pp. 83-95
Author(s):  
Marek Szindler

The use of thin films in optoelectronic and photovoltaic devices is aimed at improving the physical properties of the substrate material. The modification of the surface of the silicon substrate is thus one of the greatest challenges in research on photovoltaic materials, in order to achieve even greater efficiency or better adapt their properties depending on the application. The technologies of applying layers vary depending on the effect to be obtained and the material from which the layer is formed. In practice, the most common method is chemical vapor deposition and physical vapor deposition, and the most commonly applied optical materials are SiO2, TiO2 and Si3N4.This paper presents the results of investigations on morphology and optical properties of the prepared aluminium oxide thin films. Thin films were prepared with use of sol-gel spin coating method. Surface morphology studies were carried out using an atomic force microscope. To characterize the surface of the thin films, 3D images and histograms of the frequency of individual inequalities were made. In order to characterize the optical properties of Al2O3 thin films, the reflectance and light transmission tests were performed using a spectrophotometer. Optical constants were determined using a spectroscopic ellipsometer. Results and their analysis show that the sol-gel method allows the deposition of homogenous thin films of Al2O3 with the desired geometric characteristics and good optical properties. Uniform, continuous thin layers with a roughness not exceeding a few nanometres were deposited. Their deposition enabled to reduce the reflection of light from the polished substrate below 15% in a wide range (425-800nm) while maintaining high transparencies (over 90%). The obtained results causes that mentioned thin films are good potential material for optics, optoelectronics and photovoltaics.


1999 ◽  
Vol 312-314 ◽  
pp. 411-416 ◽  
Author(s):  
H. Brequel ◽  
G.D. Sorarù ◽  
Florence Babonneau ◽  
Dj. Bahloul-Hourlier ◽  
Stefano Enzo

2019 ◽  
Vol 807 ◽  
pp. 68-73
Author(s):  
Xiu Xia Zhang ◽  
Hai Sheng Zhang ◽  
Guan Nan Du ◽  
Shu Yi Wei ◽  
Kai Nan Zhang ◽  
...  

Through continuous experiments, scientists have found that nanomaterials have self-cleaning properties. Solar cells coated with nanometer film can keep their surface clean for a long time and maintain high photoelectric conversion efficiency. nanodiamond films were prepared on glass substrate by sol-gel method. nanosilicon carbide was also selected as the contrast material. Silicon carbide (SiC) has good chemical stability, corrosion resistance and other characteristics. nanosic films were prepared by sol-gel method on glass substrate. The production cost of sol-gel method was relatively low, the coating uniformity was suitable for mass production


2021 ◽  
Author(s):  
Pingyun Li ◽  
Haitao Ni ◽  
Shengxiang Jiang ◽  
Han Wang

Sol-gel method was conducted to prepare Ni12P5/N-doped carbon and amorphous Ni-P-C materials where heating treatments of the dried gel precursors were operated under N2 protecting atmosphere in a tube furnace....


Crystals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 439
Author(s):  
Jesús Alberto Garibay’Alvarado ◽  
Simón Yobanny Reyes-López

Surface Enhanced Infrared Absorption Spectroscopy and Surface Enhanced Raman Spectroscopy are analytic techniques that have not been massively adopted since there are issues that still need to be solved with regard to the nature of the signal enhancement substrates used. The sol–gel method for the obtention of ceramics provides an alternative for the production of said substrates. Ceramics are very wear- and heat-resistant, properties that can be used for their regeneration, and through the sol–gel method, ceramics can be produced with high purity as well as can be fashioned in many ways through different techniques, which can be helpful in the pursuit of reproducibility. This paper discusses the different advantages of sol–gel ceramics, their use in the electrospinning technique, and their application in infrared and Raman surface-enhanced spectroscopy.


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