In-Situ and Real-Time TEM Observation of the Reaction at Solid-Liquid Interface

2008 ◽  
2020 ◽  
Vol 10 (16) ◽  
pp. 5362-5385
Author(s):  
Leila Negahdar ◽  
Christopher M. A. Parlett ◽  
Mark A. Isaacs ◽  
Andrew M. Beale ◽  
Karen Wilson ◽  
...  

Many industrially important chemical transformations occur at the interface between a solid catalyst and liquid reactants. In situ and operando spectroscopies offer unique insight into the reactivity of such catalytically active solid–liquid interfaces.


1991 ◽  
Vol 237 ◽  
Author(s):  
Richard D. Robinson ◽  
Ioannis N. Miaoulis

ABSTRACTThis paper presents a new experimental method to investigate solid-liquid interface morphologies during Zone-Melting-Recrystallization at lower than the typical processing temperatures. Gallium films were used as a substitute for silicon films. In situ preliminary investigation identified three phenomena typically occurring during ZMR of silicon films: a) Transition from planar to dendritic to cellular morphologies was observed for different processing conditions; b) cell period proved to be dependant on scanning velocity; c) instabilities at the solidification interface at low heating strip temperatures were caused by supercooling and optical property variations as the material changed phase.


2005 ◽  
Vol 33 (5) ◽  
pp. 931-933 ◽  
Author(s):  
J. Popplewell ◽  
N. Freeman ◽  
S. Carrington ◽  
G. Ronan ◽  
C. McDonnell ◽  
...  

An optical technique, dual-polarization interferometry, has been used to examine lipid structures at the solid/liquid interface. Changes in the lipid structures, in real time, were examined as a consequence of challenging them with a peptide (melittin) that is known to induce liposome rupture. This work suggests that it should be possible to obtain a better understanding of the detail of the melittin rupture process.


2005 ◽  
Vol 16 (1-4) ◽  
pp. 107-110
Author(s):  
A. P. Shpak ◽  
O. P. Fedorov ◽  
E. L. Zhivolub ◽  
Y. J. Bersudskyy ◽  
O. V. Shuleshova

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