Determination of Argon in RF Sputtered SiO2 by X-Ray Emission

1968 ◽  
Vol 12 ◽  
pp. 601-611
Author(s):  
J. Charles Lloyd

AbstractArgon is commonly used as the sputtering medium for RF sputtering of insulators and is entrapped in the deposits. X-ray emission determination of argon in RF sputtered SiO2 was required as part of a study of the relationships between argon concentration in the deposits and their electrical and physical properties.Concentrations ranging from 0.05 to 7.4 weight % argon were measured in deposits 0.5 to 5μ thick. Two techniques were used for standardization: (1) weight loss of deposits heated for several hours in a helium atmosphere at 600°C; (2) potassium Kα and chlorine Kα measurements on a KCl film of known thickness to infer argon mass/argon Kα net counts. Calibrations made using these procedures agreed to within 10% and are reliable to about ±25% on an absolute basis. Absorption of radiation by the deposits was taken into account and used to correct measured argon intensities for absorption.Sputtering parameters which had major effects on argon concentration were the substrate temperature and the magnetic field applied during sputtering. Argon pressure and RF power were found to have lesser effects.

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Evgeny D. Filippov ◽  
Sergey S. Makarov ◽  
Konstantin F. Burdonov ◽  
Weipeng Yao ◽  
Guilhem Revet ◽  
...  

AbstractWe analyze, using experiments and 3D MHD numerical simulations, the dynamic and radiative properties of a plasma ablated by a laser (1 ns, 10$$^{12}$$ 12 –10$$^{13}$$ 13 W/cm$$^2$$ 2 ) from a solid target as it expands into a homogeneous, strong magnetic field (up to 30 T) that is transverse to its main expansion axis. We find that as early as 2 ns after the start of the expansion, the plasma becomes constrained by the magnetic field. As the magnetic field strength is increased, more plasma is confined close to the target and is heated by magnetic compression. We also observe that after $$\sim 8$$ ∼ 8  ns, the plasma is being overall shaped in a slab, with the plasma being compressed perpendicularly to the magnetic field, and being extended along the magnetic field direction. This dense slab rapidly expands into vacuum; however, it contains only $$\sim 2\%$$ ∼ 2 % of the total plasma. As a result of the higher density and increased heating of the plasma confined against the laser-irradiated solid target, there is a net enhancement of the total X-ray emissivity induced by the magnetization.


2021 ◽  
Author(s):  
jialu wu ◽  
Bo Li ◽  
Hong Wang ◽  
Ying Zhen Lai ◽  
Yue Ye ◽  
...  

A pair of enantiomers {[Cu(L-pro)(L-tyr)]·2H2O}n (L-1) and {[Cu(D-pro)(D-tyr)]·2H2O}n (D-1) based on the chiral ligands L/D-proline and L/D-tyrosine were synthesized and investigated by single-crystal X-ray structure analysis, IR, thermogravimetric analysis, solid-state...


1992 ◽  
Vol 9 ◽  
pp. 211-215
Author(s):  
Y. Tanaka

AbstractBased on the recent Ginga results, following topics on X-ray binaries are briefly discussed: The cyclotron resonnance features observed from several X-ray pulsars, and related problem of the magnetic field decay. Search for millisec. pulsations from LMXRBs. Very bright transients which are suspected to be new black hole candidates, and an estimation of the number of such black hole sources in our galaxy.


1972 ◽  
Vol 27 (4) ◽  
pp. 597-600 ◽  
Author(s):  
D. Sutter ◽  
L. Charpentier ◽  
H. Dreizler

Abstract The rotational Zeeman-Effect in the microwave spectrum of dimethylketene was investigated at fieldstrengths close to 22 kG. Only ΔJ= 1 rotational transitions with ΔM = ± 1 selection rules did show appreciable splittings due to the magnetic field. From the splittings the diagonal elements of the molecular gr-tensor were determined to be: gaa = ∓ 0.020(3) ; gbb = ∓ 0.0165(8) ; gcc= + 0.0126(5). (Only the relative signs of the g-values are obtained from the experiment). The susceptibility anisotropics were found to be close to zero.


2019 ◽  
Vol 622 ◽  
pp. A61 ◽  
Author(s):  
R. Staubert ◽  
J. Trümper ◽  
E. Kendziorra ◽  
D. Klochkov ◽  
K. Postnov ◽  
...  

Cyclotron lines, also called cyclotron resonant scattering features are spectral features, generally appearing in absorption, in the X-ray spectra of objects containing highly magnetized neutron stars, allowing the direct measurement of the magnetic field strength in these objects. Cyclotron features are thought to be due to resonant scattering of photons by electrons in the strong magnetic fields. The main content of this contribution focusses on electron cyclotron lines as found in accreting X-ray binary pulsars (XRBP) with magnetic fields on the order of several 1012Gauss. Also, possible proton cyclotron lines from single neutron stars with even stronger magnetic fields are briefly discussed. With regard to electron cyclotron lines, we present an updated list of XRBPs that show evidence of such absorption lines. The first such line was discovered in a 1976 balloon observation of the accreting binary pulsar Hercules X-1, it is considered to be the first direct measurement of the magnetic field of a neutron star. As of today (end 2018), we list 35 XRBPs showing evidence of one ore more electron cyclotron absorption line(s). A few have been measured only once and must be confirmed (several more objects are listed as candidates). In addition to the Tables of objects, we summarize the evidence of variability of the cyclotron line as a function of various parameters (especially pulse phase, luminosity and time), and add a discussion of the different observed phenomena and associated attempts of theoretical modeling. We also discuss our understanding of the underlying physics of accretion onto highly magnetized neutron stars. For proton cyclotron lines, we present tables with seven neutron stars and discuss their nature and the physics in these objects.


1996 ◽  
Vol 158 ◽  
pp. 161-164
Author(s):  
G. A. Wynn ◽  
A. R. King

The large-scale accretion flow in the intermediate polars (IPs) is still a matter of vigorous debate. It is known that the magnetic field of the white dwarf (WD) controls the accretion flow close to the surface, channeling the plasma onto the polecaps and giving rise to X-ray emission modulated at the WD spin period (Pspin). After their discovery it was assumed that IPs were the WD analogues of the pulsing X-ray binaries, where a magnetic neutron star accretes from a disrupted accretion disc. However, a number of authors have pointed out that the criteria for disc formation in IPs are less certain than those for the X-ray binaries.The simplest possible criterion for disc formation in a binary is that the accretion flow should be able to orbit freely about the primary star (see Frank, King & Raine 1991 for a review). In non-magnetic systems this is merely the condition that the minimum approach distance of the free stream (Rmin) should exceed the radius of the primary. The situation in magnetic systems is more complex, as the magnetic field of the primary presents an obstacle to the infalling accretion stream. In many treatments of IPs it is assumed that the plasma stream is able to orbit freely about the WD until the ram pressure of the stream is of the same order as the magnetic pressureρv2~B2/8π, whereρis the stream density,vthe stream velocity andBthe local magnetic field strength. This condition fixes the magnetospheric radius,Rmag, inside which the magnetic field is assumed to thread the stream material and direct the accretion flow along the fieldlines.


1989 ◽  
Vol 169 ◽  
Author(s):  
F.H. Garzon ◽  
J. G. Beery ◽  
D. K. Wilde ◽  
I. D. Raistrick

AbstractThin films of Y‐Ba‐Cu‐O were produced by RF sputtering of YBa2Cu3O7‐x ceramic targets, using a variety of plasma compositions, RF power levels, and substrate temperatures. Post annealing of these films in oxygen produced superconducting films with Tc values between 40‐60 K, broad transition widths and semiconductor‐like electrical behavior above Tc. Subsequent annealing at 850°C in an inert gas with a residual oxygen partial pressure of ≤10 ppm followed by an oxygen anneal produced high quality thin films: Tc> 85 K with narrow transition widths. The structure and morphology of these films during reduction‐oxidation processing were monitored using X‐ray diffraction and electron microscopy.


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