scholarly journals Ultrasonic-Supercritical CO2-Assisted Extraction and Component Analysis of Navel Orange Peel Pigment

2015 ◽  
Vol 27 (6) ◽  
pp. 2137-2140
Author(s):  
Xianchun Yu ◽  
Ying Wu ◽  
Delin Sun ◽  
Tian Tian
Foods ◽  
2021 ◽  
Vol 10 (5) ◽  
pp. 1120
Author(s):  
María del Carmen Razola-Diaz ◽  
Eduardo Jesús Guerra-Hernández ◽  
Celia Rodríguez-Pérez ◽  
Ana María Gómez-Caravaca ◽  
Belén García-Villanova ◽  
...  

Orange peel is the main by-product from orange juice industry. It is a known source of bioactive compounds, mostly phenolic compounds, and it has been widely studied for its healthy activities. Thus, this research focuses on the establishment of ultrasound-assisted extraction of phenolic compounds in orange peel using a sonotrode. For this purpose, a Box–Behnken design of 27 experiments was carried out with four independent factors—ratio ethanol/water (v/v), time (min), amplitude (%), and pulse (%). Quantitative analyses of phenolic compounds were performed and the antioxidant activity was measured by ABTS and DPPH methods. The validity of the experimental design was confirmed by ANOVA and the optimal sonotrode extraction conditions were obtained by response surface methodology (RSM). The extracts obtained in the established conditions were analyzed by High Performance Liquid Chromatography (HPLC) coupled to mass spectrometer detector and 74 polar compounds were identified. The highest phenolic content and antioxidant activity were obtained using 45/55 ethanol/water (v/v), 35 min, amplitude 90% (110 W), and pulse 100%. The established method allows an increment of phenolics recovery up to 60% higher than a conventional extraction. Moreover, the effect of drying on phenolic content was also evaluated.


2018 ◽  
Vol 133 ◽  
pp. 65-69 ◽  
Author(s):  
Lucia Baldino ◽  
Giovanna Della Porta ◽  
Libero Sesti Osseo ◽  
Ernesto Reverchon ◽  
Renata Adami

2019 ◽  
Vol 9 (1) ◽  
Author(s):  
Abigail Montero-Calderon ◽  
Clara Cortes ◽  
Ana Zulueta ◽  
Ana Frigola ◽  
Maria J. Esteve

Abstract Byproducts such as orange peel have potential uses because of their bioactive compounds, which are important for their potential to reduce the risk factors of diseases caused by aging. The lack of effective techniques and the high levels of pollution produced by the conventional extraction of bioactive compounds using organic solvents have highlighted the need to enhance the ‘green chemistry’ trend. This study evaluates the use of ultrasound to extract bioactive compounds from orange peel. The antioxidant capacity, phenolic content, ascorbic acid, total carotenoids, and HPLC profile of phenolic compounds from orange peel extracts were obtained by a physicochemical evaluation. The results demonstrate that the optimal conditions for the ultrasound-assisted extraction of bioactive orange peel compounds were a power of 400 W, a time of 30 min, and 50% ethanol in water. These conditions were used to obtain a total carotenoid concentration of 0.63 mg ß-carotene/100 g, vitamin C concentration of 53.78 mg AA/100 g, phenolic concentration of 105.96 mg GAE/100 g, and antioxidant capacity of ORAC = 27.08 mM TE and TEAC = 3.97 mM TE. The major phenolic compound identified in all orange peel extracts was hesperidin, with a maximum concentration of 113.03 ± 0.08 mg/100 g.


2013 ◽  
Vol 815 ◽  
pp. 317-320 ◽  
Author(s):  
Li Jing Min ◽  
Min Xing Zhao

[ObjectivTo study the extraction technology of flavonoids from orange peel in order to provide some theoretical guidance for the industrial production of flavonoids from orange peel. [Metho Taking orange peel as raw material, which was citrus fruit processing waste and the flavonoid yield as index, with ultrasonic assisted extraction, through single factor experiments and orthogonal tests to optimization of the extraction technology, obtain optimum process conditions of orange flavonoid by ultrasonic assisted extraction. [Result As for ultrasonic assisted extraction, the yield of orange flavonoid reached 9.6% under extraction conditions of extracting time 30 min, alcohol concentration 60%, sedimentation ratio 1:25.


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