scholarly journals Microstructure and Chemical Composition of Fe-Cr Alloy Tempered in High Temperature and Atmosphere Containing Ar-SO2

2016 ◽  
Vol 61 (3) ◽  
pp. 1607-1612 ◽  
Author(s):  
A. Radziszewska ◽  
A. Kranzmann ◽  
I. Dörfel ◽  
M. Mosquera Feijoo ◽  
M. Solecka
Keyword(s):  
Stainless Steel ◽  
Phase Composition ◽  
High Temperature ◽  
Chemical Composition ◽  
Steel Surface ◽  
High Temperature Corrosion ◽  
Corrosion Process ◽  
Gas Atmosphere ◽  
Amorphous Zone ◽  
Scale Surface

AbstractThe paper presents the microstructure, chemical and phase composition of thin scale, obtained as a result of high-temperature corrosion of X20Cr13 stainless steel. Samples were exposed to gas atmosphere of the following composition: 0.25 vol.% of SO2and 99.75 vol.% of Ar at 600 °C for 5 h. As a consequence, thin compact scale was formed on steel surface. This scale consisted of three different zones. An amorphous zone was formed close to steel surface. Then, nanocrystalline zone could be observed. Finally, larger grains were formed during the corrosion process. The analysis of the chemical composition revealed higher concentration of chromium near steel surface. In contrast, to chromium, the content of iron, increased near the scale surface. It was found out that the (Cr, Mn, Fe)5O12phase appeared in the thin scale.

High Temperature Sulphidation Behavior of Fe20Cr6Al-Y,Hf Steel

2008 ◽  
Vol 595-598 ◽  
pp. 763-768
Author(s):  
Martah Homa ◽  
Zbigniew Żurek
Keyword(s):  
High Temperature ◽  
Chemical Composition ◽  
Vapor Pressure ◽  
Phase Analysis ◽  
High Temperature Corrosion ◽  
Vapor Pressures ◽  
Scale Layer ◽  
Phase And Chemical Composition ◽  
Xrd Techniques ◽  
Scale Surface

The high temperature corrosion behavior of Fe20Cr6Al-Y,Hf steel was studied in the range of temperature 800-1000oC in H2/H2S atmospheres at pS2=10-2 ,10-3 and 10-4 Pa sulphur vapor pressures. Kinetics depend on the temperature and sulphur vapor pressure. After 24 hours the whole specimen was practically consumed because the samples were 0,06 cm thick. Morphology of the scales have been performed by SEM techniques. Phase and chemical composition have been studied by EDX and XRD techniques. It was found that scale formed on Fe20Cr6Al-Y,Hf alloy was built with porosity sulphides layer. EDX analysis of the scale surface show that the any aluminum, hafnium and yttrium sulfides were found in the formed scale layer, however small amounts of Al2S3 was detected in scale/steel interface. Also internal sulphidation was observed. A phase analysis of the formed scale revealed that it is composed mainly of an FeS, Fe7S8 phases and CrS, Cr5S6. Result were compared with data obtained on the pure Fe and Cr samples.

Heat-Resistant Sitall Coatings for High-Temperature Corrosion Protection of Nichrome Alloys

2020 ◽  
Vol 992 ◽  
pp. 633-639 ◽  
Author(s):  
E.A. Lazareva
Keyword(s):  
Phase Composition ◽  
High Temperature ◽  
Chemical Composition ◽  
Corrosion Protection ◽  
Contact Layer ◽  
High Temperature Corrosion ◽  
Chemical Processes ◽  
Layer System ◽  
Heat Resistant ◽  
Physical And Chemical

The bases of physical and chemical processes of technology of heat-resistant Sitall coatings are considered. Presents the results of investigations of phase composition and nanostructure of the contact layer system "nichrome - sitelove coverage" depending on the chemical composition of stellamaris coatings and their mode of microcrystallization. Identified and established the theoretical and technological special-news stalowych formation of coatings on the surface Narumov.

NICROFER 5520 Co

Alloy Digest ◽  
1995 ◽  
Vol 44 (3) ◽  
Keyword(s):  
High Temperature ◽  
Chemical Composition ◽  
Physical Properties ◽  
Tensile Properties ◽  
High Temperatures ◽  
Heat Treating ◽  
High Temperature Corrosion ◽  
Creep Properties ◽  
Nickel Chromium ◽  
Temperature Performance

Abstract NICROFER 5520 Co is a nickel-chromium-cobalt-molybdenum alloy with excellent strength and creep properties up to high temperatures. Due to its balanced chemical composition the alloy shows outstanding resistance to high temperature corrosion in the form of oxidation and carburization. This datasheet provides information on composition, physical properties, elasticity, and tensile properties. It also includes information on high temperature performance as well as forming, heat treating, machining, and joining. Filing Code: Ni-480. Producer or source: VDM Technologies Corporation.

ACI TYPE HN

Alloy Digest ◽  
1982 ◽  
Vol 31 (6) ◽  
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
High Temperature ◽  
Steel Casting ◽  
Nickel Content ◽  
Heat Treating ◽  
High Temperature Corrosion ◽  
Temperature Performance ◽  
Wide Range ◽  
Iron Chromium

Abstract Type HN is an iron-chromium-nickel alloy containing sufficient chromium for good high-temperature corrosion resistance and with nickel content in excess of the chromium. This alloy has properties somewhat similar to the more widely used ACI Type HT alloy but with better ductility. Type HN is used for highly stressed components in the 1800-2000 F temperature range. It is used in the aircraft, automotive, petroleum, petrochemical and power industries for a wide range of components and parts. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties as well as creep. It also includes information on high temperature performance and corrosion resistance as well as casting, heat treating, machining, and joining. Filing Code: SS-410. Producer or source: Various stainless steel casting companies.

The structure, phase composition, and residual stresses of diffusion boride layers formed by thermal-chemical treatment on the die steel surface

2021 ◽  
Vol 23 (2) ◽  
pp. 147-162
Author(s):  
Undrakh Mishigdorzhiyn ◽  
◽  
Nikolay Ulakhanov ◽  
Aleksandr Tikhonov ◽  
Pavel Gulyashinov ◽  
...  
Keyword(s):  
Phase Composition ◽  
High Temperature ◽  
Low Temperature ◽  
Residual Stresses ◽  
Diffusion Layer ◽  
Chemical Treatment ◽  
Steel Surface ◽  
Boron Content ◽  
Die Steel ◽  
Temperature Mode

Introduction. Control and management of technological residual stresses (TRS) are among the most critical mechanical engineering technology tasks. Boriding can provide high physical and mechanical properties of machine parts and tools with minimal impact on the stress state in the surface layers. The purpose of this work is to determine the temperature modes of diffusion boriding, contributing to a favorable distribution of TRS in the surface layer of die steel 3Kh2V8F. The paper considers the results of studies on the TRS determination by the experimental method on the UDION-2 installation in diffusion layers on the studied steel surface. Boriding was carried out in containers with a powder mixture of boron carbide and sodium fluoride as an activator at a temperature of 950 °C and 1050 °C for 2 hours. The obtained samples of steels with a diffusion layer were examined using an optical microscope and a scanning electron microscope (SEM); determined the layers' microhardness, elemental, and phase composition. The experiments resulted in the following findings: as the boriding temperature rose from 950 °C to 1050 °C, the diffusion layer's thickness increased from 20 to 105 μm. The low-temperature mode of thermal-chemical treatment (TCT) led to the formation of iron boride Fe2B with a maximum boron content of 6 % and a microhardness up to 1250 HV. A high-temperature mode resulted in FeB formation with a top boron content of 11 % and a microhardness up to 1880 HV. Results and Discussions. It is found that boriding at 950 °C led to a more favorable distribution of compression TRS in the diffusion layer. However, significant TRS fluctuations in the diffusion layer and the adjacent (transitional) zone could affect the operational properties after TCT at a given temperature. An increase in the TCT temperature led to tensile TRS's appearance in the layer's upper zone at a depth of up to 50 μm from the surface. Despite tensile stresses on the diffusion layer surface after high-temperature TCT, the distribution of TCT is smoother than low-temperature boriding.

scholarly journals Determination of Chromite Sands Suitability for Use in Moulding Sands

2017 ◽  
Vol 17 (2) ◽  
pp. 107-110
Author(s):  
K. Stec ◽  
J. Podwórny ◽  
B. Psiuk ◽  
Ł. Kozakiewicz
Keyword(s):  
Phase Composition ◽  
High Temperature ◽  
Chemical Composition ◽  
Chemical Properties ◽  
Grinding Process ◽  
X Ray Diffraction ◽  
Scanning Microscope ◽  
Spectroscopy Technique ◽  
X Ray

Abstract Using the available analytical methods, including the determination of chemical composition using wavelength-dispersive X-ray fluorescent spectroscopy technique and phase composition determined using X-ray diffraction, microstructural observations in a highresolution scanning microscope equipped with an X-ray microanalysis system as well as determination of characteristic softening and sintering temperatures using high-temperature microscope, the properties of particular chromite sands were defined. For the study has been typed reference sand with chemical properties, physical and thermal, treated as standard, and the sands of the regeneration process and the grinding process. Using these kinds of sand in foundries resulted in the occurrence of the phenomenon of the molding mass sintering. Impurities were identified and causes of sintering of a moulding sand based on chromite sand were characterized. Next, research methods enabling a quick evaluation of chromite sand suitability for use in the preparation of moulding sands were selected.

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