Phase Composition, Structure, and Plastic Deformation Localization in Zr1%Nb alloys

Author(s):  
LB Zuev ◽  
SY Zavodchikov ◽  
TM Poletika ◽  
GS Cheremnykh ◽  
VB Filippov ◽  
...  
2006 ◽  
Vol 3 (1) ◽  
pp. 12336
Author(s):  
LB Zuev ◽  
SY Zavodchikov ◽  
TM Poletika ◽  
GS Cheremnykh ◽  
VB Filippov ◽  
...  

2016 ◽  
Vol 838-839 ◽  
pp. 344-349 ◽  
Author(s):  
Galina P. Grabovetskaya ◽  
Ekaterina N. Stepanova ◽  
Ilya V. Ratochka ◽  
I.P. Mishin ◽  
Olga V. Zabudchenko

Hydrogenation effect on the development of superplastic deformation in the submicrocrystalline Ti–6Al–4V alloy at temperatures (0.4–0.5)Тmelt is investigated. Hydrogenation of the submicrocrystalline Ti–6Al–4V alloy to 0.26 mass% during superplastic deformation is found to result in solid solution strengthening, plastic deformation localization, and as a consequence, decrease of the deformation to failure. Possible reasons for the decrease of the flow stress and increase of the deformation to failure in the submicrocrystalline Ti–6Al–4V–0.26H alloy during deformation under conditions of superplasticity and simultaneous hydrogen degassing from the alloy are discussed.


2016 ◽  
Vol 685 ◽  
pp. 525-529
Author(s):  
Zhanna G. Kovalevskaya ◽  
Margarita A. Khimich ◽  
Andrey V. Belyakov ◽  
Ivan A. Shulepov

The changes of the phase composition, structure and physicomechanical properties of Ti‑40 mas % Nb after severe plastic deformation are investigated in this paper. By the methods of microstructural, X-ray diffraction analysis and scanning electron microscopy it is determined that phase and structural transformations occur simultaneously in the alloy after severe plastic deformation. The martensitic structure formed after tempering disappears. The inverse α'' → β transformation occurs. The structure consisting of oriented refined grains is formed. The alloy is hardened due to the cold working. The Young modulus is equal to 79 GPa and it is less than that of initial alloy and close to the value obtained after tempering. It is possible that Young modulus is reduced by additional annealing.


2015 ◽  
Vol 57 (4) ◽  
pp. 348-355 ◽  
Author(s):  
S. V. Stefanovsky ◽  
O. I. Stefanovskaya ◽  
S. E. Vinokurov ◽  
S. S. Danilov ◽  
B. F. Myasoedov

Author(s):  
E.G. Astafurova ◽  
◽  
K.A. Reunova ◽  
S.V. Astafurov ◽  
M.Yu. Panchenko ◽  
...  

We investigated the phase composition, plastic deformation and fracture micromechanisms of Fe-(25-26)Cr-(5-12)Mn-0.15C-0.55N (wt. %) high-nitrogen chromium-manganese steel. Obtained by the method of electron-beam 3D-printing (additive manufacturing) and subjected to a heat treatment (at a temperature of 1150°C following by quenching). To establish the effect of the electron-beam 3D-printing process on the phase composition, microstructure and mechanical properties of high-nitrogen steel, a comparison was made with the data for Fe-21Cr-22Mn-0.15C-0.53N austenitic steel (wt. %) obtained by traditional methods (casting and heat treatment) and used as a raw material for additive manufacturing. It was experimentally established that in the specimens obtained by additive manufacturing method, depletion of the steel composition by manganese in the electron-beam 3D-printing and post-built heat treatment contributes to the formation of a macroscopically and microscopically inhomogeneous two-phase structure. In the steel specimens, macroscopic regions of irregular shape with large ferrite grains or a two-phase austenite-ferrite structure (microscopic inhomogeneity) were observed. Despite the change in the concentration of the basic elements (chromium and manganese) in additive manufacturing, a high concentration of interstitial atoms (nitrogen and carbon) remains in steel. This contributes to the macroscopically heterogeneous distribution of interstitial atoms in the specimens - the formation of a supersaturated interstitial solid solution in the austenitic regions due to the low solubility of nitrogen and carbon in the ferrite regions. This inhomogeneous heterophase (ferrite-austenite) structure has high strength properties, good ductility and work hardening, which are close to those of the specimens of the initial high-nitrogen austenitic steel used as the raw material for additive manufacturing.


2015 ◽  
Vol 37 (1) ◽  
pp. 21-26 ◽  
Author(s):  
I. V. Karpets’ ◽  
O. M. Myslyvchenko ◽  
M. O. Krapivka ◽  
V. F. Gorban’ ◽  
O. S. Makarenko ◽  
...  

2021 ◽  
pp. 22-30
Author(s):  
S. A Barannikova ◽  
A. M Nikonova ◽  
S. V Kolosov

This work deals with studying staging and macroscopic strain localization in austenitic stainless steel 12Kh18N9T within a temperature range of 143 K < T < 420 K. The visualization and evolution of macroscopic localized plastic deformation bands at different stages of work hardening were carried out by the method of the double-exposure speckle photography (DESP), which allows registering displacement fields with a high accuracy by tracing changes on the surface of the material under study and then comparing the specklograms recorded during uniaxial tension. The shape of the tensile curves σ(ε) undergoes a significant change with a decreasing temperature due to the γ-α'-phase transformation induced by plastic deformation. The processing of the deformation curves of the steel samples made it possible to distinguish the following stages of strain hardening, i.e. the stage of linear hardening and jerky flow stage. A comparative analysis of the design diagrams (with the introduction of additional parameters of the Ludwigson equation) and experimental diagrams of tension of steel 12Kh18N9T for different temperatures is carried out. The analysis of local strains distributions showed that at the stage of linear work hardening, a mobile system of plastic strain localization centers is observed. The temperature dependence of the parameters of plastic deformation localization at the stages of linear work hardening has been established. Unlike the linear hardening, the jerky flow possesses the propagation of single plastic strain fronts that occur one after another through the sample due to the γ-α' phase transition and the Portevin-Le Chatelier effect. It was found that at the jerky flow stage, which is the final stage before the destruction of the sample, the centers of deformation localization do not merge, leading to the neck formation.


2021 ◽  
Vol 2144 (1) ◽  
pp. 012004
Author(s):  
P V Panin ◽  
I A Bogachev ◽  
E A Lukina

Abstract Chemical composition, structure, and technological properties have been investigated for metal powder compositions (MPCs) of a new six-component TiAl-based alloy with Gd microadditions: Ti-31.0Al-2.5V-2.5Nb-2.5Cr-0.4Gd, wt.% (Ti-44.5Al-2V-1Nb-2Cr-0.1Gd, at.%). Three MPCs fractions (10–63, 40–100, 80–120 μm) were produced by electrode induction melting and inert gas atomization technique and targeted for the additive synthesis of parts. It is shown that the chemical composition of the MPCs for the main elements corresponds to that of the electrode. In contrast, a 1.5-fold increase of the oxygen content in the MPCs was observed, which is being the result of natural oxidation of powder particles upon air environment due to developed specific surface. It has been determined that the phase composition of the MPCs (γ+α(α2)+β) differs from the equilibrium phase composition of the electrode (γ+α2)+β0/B2) and corresponds to a rapidly quenched metastable state, which indicates high solidification rates in the atomization process, exceeding critical cooling rates of the alloy. The technological properties, specifically the powder flowability, were found to be improved for 40–100 and 80–120 μm fractions, making them applicable for additive synthesis of parts from the studied alloy by selective electron-beam melting method


2021 ◽  
Vol 2103 (1) ◽  
pp. 012075
Author(s):  
AA Dmitrievskiy ◽  
DG Zhigacheva ◽  
VM Vasyukov ◽  
PN Ovchinnikov

Abstract In this work, the phase composition (relative fractions of monoclinic m-ZrO2, tetragonal t-ZrO2, and cubic c-ZrO2 phases) and mechanical properties (hardness, fracture toughness, compressive strength) of alumina toughened zirconia (ATZ) ceramics, with an addition of silica were investigated. Calcium oxide was used as a stabilizer for the zirconia tetragonal phase. It was shown that CaO-ATZ+SiO2 ceramics demonstrate increased resistance to low-temperature degradation. The plasticity signs at room temperature were found due to the SiO2 addition to CaO-ATZ ceramics. A yield plateau appears in the uniaxial compression diagram at 5 mol. % SiO2 concentration. It is hypothesized that discovered plasticity is due to the increased t→m transformability.


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