Thickness dependence of microstructure and critical current density of Yba2Cu3O7−δ on rolling-assisted biaxially textured substrates

2003 ◽  
Vol 18 (5) ◽  
pp. 1109-1122 ◽  
Author(s):  
K. J. Leonard ◽  
A. Goyal ◽  
D. M. Kroeger ◽  
J. W. Jones ◽  
S. Kang ◽  
...  

The change in microstructure associated with the decrease in critical current density (Jc) of Yba2Cu3O7−δ (YBCO) films with increasing thickness was examined. Samples of pulse laser deposited YBCO films varying in thickness from 0.19 to 3.0 μm on rolling-assisted biaxially textured substrates with an architecture of CeO2/YSZ/CeO2/Ni were prepared by tripod polishing for cross-sectional electron microscopy. More randomly oriented grains in the upper portion of the YBCO film surface were observed with increasing film thickness, resulting in less cube texture. In addition, increases in mismatch across the boundaries of the c-axis grains with increasing time during deposition, along with the development of BaCeO3 and Y2BaCuO5 phases at the YBCO/CeO2 interface, contributed to the degradation of film properties. Surface outgrowths of the YBCO film were examined as well as the defect structures and second-phase formations within the films.

2001 ◽  
Vol 689 ◽  
Author(s):  
S. Sathyamurthy ◽  
M. Paranthaman ◽  
B. W. Kang ◽  
H. Y. Zhai ◽  
T. Aytug ◽  
...  

Sol-gel processing of La2Zr2O7 (LZO) buffer layers on biaxially textured Ni-3 at.% W alloy substrates using a continuous reel-to-reel dip-coating unit has been studied. The epitaxial LZO films obtained have a strong cube texture and uniform microstructure. The effect of increasing the annealing speed on the texture, microstructure and the carbon content retained in the film were studied. On top of the LZO films, epitaxial layers of Yttria Stabilized Zirconia (YSZ) and Ceria (CeO2) were deposited using rf sputtering, and YBa2Cu3Ox (YBCO) films were then deposited using Pulsed Laser Deposition (PLD). A critical current density (Jc) of 1.9 MA/cm2 at 77K and self-field and 0.34 MA/cm2 at 77K and 0.5T have been obtained on these films. These values are comparable to those obtained on YBCO films deposited on all-vacuum deposited buffer layers, and are the highest ever obtained using solution seed layers. The use of all-solution buffers for coated conductor processing has also been explored. A critical current density of 1.1 MA/cm2 at 77 K and self-field was obtained on YBCO films grown be PLD on LZO buffered nickel substrates.


2002 ◽  
Vol 17 (7) ◽  
pp. 1750-1757 ◽  
Author(s):  
B. W. Kang ◽  
A. Goyal ◽  
D. F. Lee ◽  
J. E. Mathis ◽  
E. D. Specht ◽  
...  

We investigated the dependence of critical current density (Jc) on thickness of Yba2Cu3O7−δ (YBCO) films grown by pulsed laser deposition on (100) SrTiO3 (STO) and on rolling-assisted biaxially textured substrates (RABiTS). The thickness of YBCO films varied from 0.19 to 3 μm. The highest Jcs of 5.3 and 2.6 MA/cm2 at 77 K, self-field were obtained for 0.19-μm YBCO films on STO and RABiTS, respectively. Jc was found to decrease exponentially with YBCO thickness on both substrates. However, the results suggest different mechanisms are responsible for the Jc reduction in the two cases. On STO, growth of a-axis grains within c-axis films and broadening of the in-plane texture were observed in thick films. On RABiTS, degradation in cube texture as well as development of a porous surface morphology were found to correlate with film thickness.


2017 ◽  
Vol 5 (1) ◽  
pp. 69
Author(s):  
Soh Deawha ◽  
N. Korobova ◽  
Park Jungcheul

<p>High temperature superconducting (HTS) thick films deposited on metal Ag wire were prepared with YBCO and BSCCO powders by electrophoretic deposition method. I<sub>2</sub> was used as additives for surface charge of YBCO and BSCCO particles. When 2-3 wt.% BaF<sub>2</sub> was added in the YBCO suspension, the pores and cracks of film surface were decreased and film density could be increased. In case of YBCO films, the critical current density (J<sub>c</sub>) was calculated at the value of 1458 A/cm<sup>2</sup> (77 K, 0 K) by 4 point prove method. BSCCO films had less cracks than YBCO films, and the critical current density (J<sub>c</sub>) was obtained more than 10<sup>4</sup> A/cm<sup>2</sup>.</p>


1995 ◽  
Vol 09 (07) ◽  
pp. 439-443 ◽  
Author(s):  
JUN-HUI JIA ◽  
ZHEN-ZHONG QI

Thin films of YBCO with or without Nb added were prepared on (100) ZrO 2 single crystalline substrate by dc magnetron sputtering method. A phase of YBa 2 NbO 6 was found to form not only in the target materials of YBCO but also in the sputtered thin films. The second phase of YBa 2 NbO 6 in the superconducting films destroyed a match relation between the lattice of YBCO and the lattice of ZrO 2 substrate. The measurements of critical current density J c under magnetic field (H // c axis, up to 5T) showed that the J c in Nb-added YBCO films reduced more apparently than that in YBCO films. It is concluded that the existence of second phase of YBa 2 NbO 6 in superconducting phase does not play a rule of flux pinning.


2005 ◽  
Vol 426-431 ◽  
pp. 1108-1112 ◽  
Author(s):  
P. Mele ◽  
K. Matsumoto ◽  
T. Horide ◽  
O. Miura ◽  
A. Ichinose ◽  
...  

2011 ◽  
Vol 24 (10) ◽  
pp. 105020 ◽  
Author(s):  
I A Golovchanskiy ◽  
A V Pan ◽  
O V Shcherbakova ◽  
S A Fedoseev ◽  
S X Dou

1999 ◽  
Vol 9 (2) ◽  
pp. 1531-1534 ◽  
Author(s):  
J.A. Smith ◽  
M.J. Cima ◽  
N. Sonnenberg

2000 ◽  
Vol 341-348 ◽  
pp. 1177-1178 ◽  
Author(s):  
G. Ghigo ◽  
A. Chiodoni ◽  
R. Gerbaldo ◽  
L. Gozzelino ◽  
F. Laviano ◽  
...  

1994 ◽  
Vol 235-240 ◽  
pp. 627-628 ◽  
Author(s):  
M. Pernet ◽  
D. Chateigner ◽  
P. Germi ◽  
C Dubourdieu ◽  
O. Thomas ◽  
...  

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