Controllable synthesis of palladium nanoparticles via a simple sonoelectrochemical method

2003 ◽  
Vol 18 (6) ◽  
pp. 1399-1404 ◽  
Author(s):  
Xiao-Feng Qiu ◽  
Jin-Zhong Xu ◽  
Jian-Ming Zhu ◽  
Jun-Jie Zhu ◽  
Shu Xu ◽  
...  
Keyword(s):  
Growth Mechanism ◽  
Current Density ◽  
Palladium Nanoparticles ◽  
Room Temperature ◽  
Controllable Synthesis ◽  
Highly Dispersed ◽  
Ultrasonic Intensity ◽  
Palladium Particles ◽  
Shape And Size

A simple pulse sonoelectrochemical technique was used to synthesize highly dispersed spherical palladium particles and a dendritic Pd superstructure in the presence of cethyltrimethylammonium bromide (CTAB) at room temperature. The shape and size of spherical nanocrystalline Pd can be controlled by varying current density, the interval between two continuous ultrasonic pulses, ultrasonic intensity, and the concentration of CTAB. The possible growth mechanism of dendritic-structured Pd is discussed.

scholarly journals A Process for Hydrogen Production from the Catalytic Decomposition of Formic Acid over Iridium—Palladium Nanoparticles

Materials ◽  
2021 ◽  
Vol 14 (12) ◽  
pp. 3258
Author(s):  
Hamed M. Alshammari ◽  
Mohammad Hayal Alotaibi ◽  
Obaid F. Aldosari ◽  
Abdulellah S. Alsolami ◽  
Nuha A. Alotaibi ◽  
...  
Keyword(s):  
Hydrogen Production ◽  
Formic Acid ◽  
Activated Charcoal ◽  
Palladium Nanoparticles ◽  
Room Temperature ◽  
Catalytic Decomposition ◽  
Conversion Yield ◽  
Production Of Hydrogen ◽  
Commercial Applications

The present study investigates a process for the selective production of hydrogen from the catalytic decomposition of formic acid in the presence of iridium and iridium–palladium nanoparticles under various conditions. It was found that a loading of 1 wt.% of 2% palladium in the presence of 1% iridium over activated charcoal led to a 43% conversion of formic acid to hydrogen at room temperature after 4 h. Increasing the temperature to 60 °C led to further decomposition and an improvement in conversion yield to 63%. Dilution of formic acid from 0.5 to 0.2 M improved the decomposition, reaching conversion to 81%. The reported process could potentially be used in commercial applications.

Morphology Evolution and Luminescence Properties of YF3: Sm Nano-/Microcrystals

2012 ◽  
Vol 463-464 ◽  
pp. 112-118
Author(s):  
Feng Tao ◽  
Geng Zhu ◽  
Zhi Jun Wang ◽  
Feng Pan ◽  
Yu Feng Sun ◽  
...  
Keyword(s):  
Hydrothermal Method ◽  
Growth Mechanism ◽  
Room Temperature ◽  
Red Light ◽  
Environmentally Friendly ◽  
Morphology Evolution ◽  
Flat Panel Display ◽  
Flat Panel ◽  
Display Devices ◽  
Potential Applications

Abstract. Recently, there has been increasting interest in the doping of nano-/microcrystal hosts with Sm3+. However, very few examples of Sm3+doped YF3-based nanophosphors have been reported. In this paper, a variety of uniform YF3:Sm nano-/microcrystals have been successfully prepared by a facile, effective, and environmentally friendly hydrothermal method. The morphology evolution process has been investigated by quenching the reaction at different time. Based on the results, a possible growth mechanism is presented in detail. The as-obtained YF3:Sm nano-/microcrystals show strong yellow and red light emissions under room temperature, which is quite different from those reported previously and might find potential applications in fields such as light phosphor powers and advanced flat panel display devices.

scholarly journals Skyrmion flow near room temperature in an ultralow current density

2012 ◽  
Vol 3 (1) ◽  
Author(s):  
X.Z. Yu ◽  
N. Kanazawa ◽  
W.Z. Zhang ◽  
T. Nagai ◽  
T. Hara ◽  
...  
Keyword(s):  
Current Density ◽  
Room Temperature

scholarly journals Correction: Growth mechanism of ceria nanorods by precipitation at room temperature and morphology-dependent photocatalytic performance

CrystEngComm ◽  
2017 ◽  
Vol 19 (36) ◽  
pp. 5492-5492
Author(s):  
Zhao Liu ◽  
Xiaojing Li ◽  
Mohannad Mayyas ◽  
Pramod Koshy ◽  
Judy N. Hart ◽  
...  
Keyword(s):  
Growth Mechanism ◽  
Room Temperature ◽  
Photocatalytic Performance

Correction for ‘Growth mechanism of ceria nanorods by precipitation at room temperature and morphology-dependent photocatalytic performance’ by Zhao Liu et al., CrystEngComm, 2017, 19, 4766–4776.

On the growth mechanism of UV laser deposited a-C:H from CH2I2 at room temperature

2001 ◽  
Vol 172 (3-4) ◽  
pp. 200-206 ◽  
Author(s):  
Mikael Lindstam ◽  
Mats Boman ◽  
Klaus Piglmayer
Keyword(s):  
Growth Mechanism ◽  
Room Temperature ◽  
Uv Laser

An easily prepared palladium-hydrogel nanocomposite catalyst for C–C coupling reactions

2014 ◽  
Vol 2 (44) ◽  
pp. 18952-18958 ◽  
Author(s):  
Mitasree Maity ◽  
Uday Maitra
Keyword(s):  
Palladium Nanoparticles ◽  
Room Temperature ◽  
Coupling Reaction ◽  
Coupling Reactions ◽  
Sodium Cyanoborohydride ◽  
Efficient Catalyst ◽  
Suzuki Coupling Reaction ◽  
Reaction In Water ◽  
Hydrogel Nanocomposite

Palladium nanoparticles were efficiently prepared in situ by sodium cyanoborohydride reduction of Pd(ii) at room temperature using calcium-cholate hydrogel fibers as templates. The PdNPs self-organize on the gel fibers, which supports the controlled growth as well as stabilization of PdNPs. The hybrid xerogel was used as an efficient catalyst for the Suzuki coupling reaction in water.

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