The Metal - Oxide Composite [Fe0.2Co0.8]0.8[Fe2.38Co0.62O4]: Hrtem and EDX Characterization

1994 ◽  
Vol 346 ◽  
Author(s):  
J. C Yamegni Noubeyo ◽  
A. Malats I Riera ◽  
J. Werckmann ◽  
G. Pourroy ◽  
G. Ehret ◽  
...  

ABSTRACTThe new metal-ferrite composite [Fe0.2Co0.8]0.8[Fe2.38Co0.62O4] is obtained by precipitation of ferrous and cobalt chloride in KOH. Further heating under vacuum above 400°C shows a cationic exchange between metal and spinel leading to a new composite made up of cobalt metal and cobalt doped magnetite.HTERM and EDX observations have been carried out on both composites, i.e., before and after vacuum annealing, We show that cationic exchange occurs mainly in crystals made up of spinel, CoO and amorphous nanoparticles.

Coatings ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 221
Author(s):  
Mariya Aleksandrova ◽  
Ivailo Pandiev

This paper presents impedance measurements of ferroelectric structures involving lead-free oxide and polymer-oxide composite coatings for sensing and energy harvesting applications. Three different ferroelectric materials grown by conventional microfabrication technologies on solid or flexible substrates are investigated for their basic resonant characteristics. Equivalent electrical circuit models are applied to all cases to explain the electrical behavior of the structures, according to the materials type and thickness. The analytical results show good agreement with the experiments carried out on a basic types of excited thin-film piezoelectric transducers. Additionally, temperature and frequency dependences of the dielectric permittivity and losses are measured for the polymer-oxide composite device in relation with the surface morphology before and after introduction of the polymer to the functional film.


Author(s):  
Govindhasamy Murugadoss ◽  
Narthana Kandhasamy ◽  
Manavalan Rajesh Kumar ◽  
Abdullah K. Alanazi ◽  
Firoz Khan ◽  
...  

1992 ◽  
Vol 279 ◽  
Author(s):  
K. K. Bourdelle ◽  
D. O. Boerma

ABSTRACTNi foils and samples consisting of bilayers of Ni or Fe on Al, Ti or Si were implanted at room temperature with 15N+ ions to fluences of around 1×l017 N/cm2. The concentration depth profiles of 15N were determined with nuclear reaction analysis before and after vacuum annealing. It was found that the penetrability for N atoms of the surface and the solid/solid interface plays an important role in the N redistribution during implantation or annealing. The formation of a nitride layer or nitride clusters in Ni and Fe was deduced. Parameters for N migration determined for the metals under investigation are discussed in terms of models.


2017 ◽  
Vol 703 ◽  
pp. 461-465 ◽  
Author(s):  
Hao Yang ◽  
Huajun Qiu ◽  
Jun-Qiang Wang ◽  
Juntao Huo ◽  
Xinmin Wang ◽  
...  

Author(s):  
Adrian Nur ◽  
Jundi Rofi’uddien ◽  
Muhammad Abdul Basir ◽  
Nazriati Nazriati ◽  
Fauziatul Fajaroh

<p>The metal oxide composite is used to the microelectronic circuit, piezoelectric, fuel cell, sensor, catalyst, coating for preventing corrosion, and solar cell. The ZnO/CuO is one of the metal oxide composites. The combination of ZnO and CuO is the potential composite used to the catalyst and the anti-bacterial agent. The method used in this research was the electrochemical method in the acetate acid solution. The acetate acid solution used in this research is cheaper than the succinite acid used in the previous research. The electrochemical method has advantages due the easy to control and cheap. The composite resulted was analyzed by the XRD and the FTIR. The aims of this analysis are to know the crystallite phase, structure, and the functional groups of the particle resulted. The analysis showed that the ZnO-CuO composite can be resulted by the electrochemical method.</p>


2022 ◽  
pp. 89-109
Author(s):  
Zainab Ibrahim Elkahlout ◽  
Abdulrahman Mohmmed AlAhzm ◽  
Maan Omar Alejli ◽  
Fatima Zayed AlMaadeed ◽  
Deepalekshmi Ponnamma ◽  
...  

Sensors ◽  
2019 ◽  
Vol 19 (23) ◽  
pp. 5190 ◽  
Author(s):  
Miriam Alvarado ◽  
Silvia De La Flor ◽  
Eduard Llobet ◽  
Alfonso Romero ◽  
José Luis Ramírez

Many sensors are developed over flexible substrates to be used as wearables, which does not guarantee that they will actually withstand being bent. This work evaluates the gas sensing performance of metal oxide devices of three different types, before and after having undergone automated, repetitive bending tests. These tests were aimed at demonstrating that the fabricated sensors were actually flexible, which cannot be taken for granted beforehand. The active layer in these sensors consisted of WO3 nanowires (NWs) grown directly over a Kapton foil by means of the aerosol-assisted chemical vapor deposition. Their response to different H2 concentrations was measured at first. Then, they were cyclically bent, and finally, their response to H2 was measured again. Sensors based on pristine WO3-NWs over Ag electrodes and on Pd-decorated NWs over Au electrodes maintained their performance after having been bent. Ag electrodes covered with Pd-decorated NWs became fragile and lost their usefulness. To summarize, two different types of truly flexible metal oxide gas sensor were fabricated, whereas a third one was not flexible, despite being grown over a flexible substrate following the same method. Finally, we recommend that one standard bending test procedure should be established to clearly determine the flexibility of a sensor considering its intended application.


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