The Yield Stress of the Fully-Lamellar Microstructure

1996 ◽  
Vol 460 ◽  
Author(s):  
Y. Q. Sun

ABSTRACTThis paper is an inquiry into the relationship between the yield stress and the two length parameters in the fully-lamellar polycrystalline microstructure, the grain-size dCB and the lamellar thickness dLM. Deformation in the multilayer structure is assumed to proceed by dislocations propagating in the formation of a succession of mutually interacting pileups, blocked at the lamellar interfaces and piled-up ultimately against the grain boundary. An important case suggested is a yield stress independent of the grain size, sensitive only to the lamellar spacing.

2004 ◽  
Vol 842 ◽  
Author(s):  
Jean-Pierre Chevalier ◽  
Mélanie Lamirand ◽  
Jean-Louis Bonnentien

ABSTRACTTi-Al-Cr ternary and Ti-Al-Cr-Nb quaternary alloys have been studied as a function of initial purity and added interstitial content. Using strict clean processing together with either ultra high purity or commercial purity alloys, the effects of interstitial elements (essentially O, but also C and N) on microstructure and hardness, yield stress and fracture strain have been studied for both fully lamellar microstructures and duplex microstructures. The results are clear and similar trends are observed : as long as they do not precipitate, these stabilise the lamellar microstructure and affect the kinetics of the α-γ phase tranformation, leading to a higher than equilibrium value for the α2 phase for continuous cooling. Both the lamellar spacing and the α2 phase fraction correlate with increased hardness and yield stress, and also with decreasing fracture strain. The effects are significant.


2010 ◽  
Vol 638-642 ◽  
pp. 1934-1939 ◽  
Author(s):  
Y.B. Chun ◽  
S.H. Ahn ◽  
D.H. Shin ◽  
S.K. Hwang

Recent advances in the severe plastic deformation technique have shown that effective refinement of the microstructure can be achieved in pure metals as well as in alloys. Among the various methods of severe plastic deformation, equal channel angular pressing has been the subject of numerous research works. Since the grain refining effect of this technique appears to reach a peak at a level of approximately 200 nm further microstructural changes are sought—deformation at a cryogenic temperature being one of the candidate routes. In the present study, we opted to combine equal channel angular pressing and low temperature plastic deformation to refine the microstructure of commercially pure V. The starting microstructure consisted of equiaxed grains with an average size of 100 micrometers. This microstructure was refined to a 200 nm thick lamellar microstructure by 8 passes of equal channel angular pressing at 350°C. The lamellar thickness was further reduced to 140 nm upon subsequent cryogenic rolling, which resulted in room temperature yield strength of 768 MPa. In the specimens, recrystallization annealed at 850°C, the grain size reached 1000 nm or larger, and the yield strength obeyed the Hall-Petch relationship with that grain size. The tensile elongation value, which was low and insensitive to the grain size in the as-deformed state, increased significantly up to 43% with the recrystallization annealing.


Author(s):  
H. Saari ◽  
S. Bulmer ◽  
D. Y. Seo ◽  
P. Au

The microstructures and creep properties at 760 °C and 276 MPa of three powder metallurgy TiAl alloys (Ti-48Al-2Cr-2Nb, Ti-48Al-2Cr-2Nb+0.5W, and Ti-48Al-2Cr-2Nb+1W (atomic percent)) are presented. The results indicate that the addition of W to the base composition, the use of a solution heat treatment combined with controlled cooling (to generate a fully lamellar microstructure), and the use of an aging heat treatment (to generate precipitate particles at the lamellar interfaces) improve creep properties dramatically. The solution heat treated and aged Ti-48Al-2Cr-2Nb+1W alloy has a time to 0.5% strain of 8.3 hours, a time to 1% strain of 46.4 hours, and a creep life of 412 hours with a rupture ductility of 16.9%.


2004 ◽  
Vol 449-452 ◽  
pp. 25-30 ◽  
Author(s):  
Xin Hua Wu ◽  
D. Hu ◽  
M.H. Loretto

The IRC has carried out a major research programme over the last ten or so years aimed at developing the processing and optimisation of TiAl-based alloys. This work has covered melting, the production of shaped castings, powder processing and a range of thermomechanical processing routes in parallel with alloy development. In this paper the work aimed at understanding the factors that influence the properties of thermo-mechanically processed and cast samples of TiAl-based alloys will be reviewed. It is shown that the use of boron to control the grain size of castings leads to limited ductility in the stronger and more highly alloyed TiAl alloys because ribbon-like borides up to 200µm in length can be formed. It is also shown that although a fully lamellar microstructure offers a good balance of properties their plastic anisotropy leads to pre-yield fracture and to reduced fatigue life. It is clear that grain size control is essential if an acceptable balance of properties is to be obtained but that if casting is to be used grain refinement via boron addition is not totally satisfactory. A simple heat treatment can be used to refine the microstructure of cast boron-free alloys, which leads to ductility comparable with that in wrought samples and the associated convoluted microstructure should also eliminate pre-yield cracking.


2002 ◽  
Vol 753 ◽  
Author(s):  
T. Takasugi ◽  
T. Tsuyumu ◽  
Y. Kaneno ◽  
H. Inoue

ABSTRACTThe TiAl-based (Ti-46Al-7Nb-1.5Cr (at%)) intermetallic alloy was tensile tested in vacuum and air as a function of temperature to investigate microstructural effect on the moisture-induced embrittlement. The reduction in tensile strength (or elongation) due to testing in air diminishes as testing temperature increases. From the fracture strength (or elongation)-temperature curves, it was found that the near gamma grain microstructure was most resistant, and the dual-phase microstructure most susceptible to moisture-induced embrittlement. Also, the moisture-induced embrittlement of the TiAl-based intermetallic alloy with fully lamellar microstructure depends on the lamellar spacing, and reduced with decreasing lamellar spacing.


2014 ◽  
Vol 922 ◽  
pp. 372-375
Author(s):  
Sho Kobayashi ◽  
Tomo Kawakatsu ◽  
Yorinobu Takigawa ◽  
Tokuteru Uesugi ◽  
Kenji Higashi

A relationship between yield stress and grain size was examined in FSP-ed and annealed 5N-Al (99.9996% purity) in order to reveal the relationship on materials with equal chemical composition, because the large positive deviations of yield stress from the Hall–Petch relation obtained by plots with coarse grain size were reported in the fine grain sizes with SPD processed and we focused on amount of impurities during SPD processing about this phenomenon. The purity of FSP-ed samples on this study were 99.9988% Al (Fe +8at.ppm). Annealing this sample at various temperatures, the relationship between yield stress and grain sizes was obtained on materials with equal chemical composition. However, the yield stress of sample as FSP-ed is higher than that following Hall-Petch relation obtained by subsequently annealed samples plots. As a result, the positive deviation is occurred by factors other than the impurities.


2021 ◽  
Vol 7 ◽  
Author(s):  
Hariprasath Ganesan ◽  
Ingo Scheider ◽  
Christian J. Cyron

γ-titanium aluminide (TiAl) alloys with fully lamellar microstructure possess excellent properties for high-temperature applications. Such fully lamellar microstructure has interfaces at different length scales. The separation behavior of the lamellae at these interfaces is crucial for the mechanical properties of the whole material. Unfortunately, quantifying it by experiments is difficult. Therefore, we use molecular dynamics (MD) simulations to this end. Specifically, we study the high-temperature separation behavior under tensile loading of the four different kinds of lamellar interfaces appearing in TiAl, namely, the γ/α2, γ/γPT, γ/γTT, and γ/γRB interfaces. In our simulations, we use two different atomistic interface models, a defect-free (Type-1) model and a model with preexisting voids (Type-2). Clearly, the latter is more physical but studying the former also helps to understand the role of defects. Our simulation results show that among the four interfaces studied, the γ/α2 interface possesses the highest yield strength, followed by the γ/γPT, γ/γTT, and γ/γRB interfaces. For Type-1 models, our simulations reveal failure at the interface for all γ/γ interfaces but not for the γ/α2 interface. By contrast, for Type-2 models, we observe for all the four interfaces failure at the interface. Our atomistic simulations provide important data to define the parameters of traction–separation laws and cohesive zone models, which can be used in the framework of continuum mechanical modeling of TiAl. Temperature-dependent model parameters were identified, and the complete traction–separation behavior was established, in which interface elasticity, interface plasticity, and interface damage could be distinguished. By carefully eliminating the contribution of bulk deformation from the interface behavior, we were able to quantify the contribution of interface plasticity and interface damage, which can also be related to the dislocation evolution and void nucleation in the atomistic simulations.


2010 ◽  
Vol 24 (15n16) ◽  
pp. 2279-2284
Author(s):  
WEI ZHANG ◽  
YUE MA ◽  
SHENGKAI GONG

Microstructure stability in fully lamellar (FL) structure TiAl based intermatellics have been studied. The experiment results have shown that the smaller the lamellar spacing is, the more instable the lamellar structure is. The distinct lamellar spheroidization occurs at 1150°C holding for 24h. This phenomena may be caused by lamellar coarsening and decomposition. The linear residual β phase distributed in the Ti -47 A 1-2 Cr -2 Nb alloy may prevent lamellar spheroidization and improves the stability of lamellar structure significantly.


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