Mechanical Property Determination for Supported Polymer Films using Double Bending Beams

1986 ◽  
Vol 76 ◽  
Author(s):  
B. J. Han ◽  
H. M. Tong ◽  
K. Saenger ◽  
Carl C. Gryte

ABSTRACTA double-bending-beam technique has been developed to determine the mechanical properties (e.g., the elastic stiffness parameter and the in-plane coefficient of thermal expansion) of thin polymer films during thermal cycling. The mechanical properties of poly(methyl methacrylate) and a polyimide have been determined from the combined stress-temperature relationships of identical polymer films coated on two rigid beams (each with a distinctly different Young's modulus and coefficient of thermal expansion). The measured mechanical properties were found to agree with data obtained using conventional techniques. The double-bending-beam technique can be applied to a wide variety of dry and wet processing situations involving thin polymer films.

1998 ◽  
Vol 511 ◽  
Author(s):  
K. S. Patel ◽  
Sue Ann bidstrup-Allen ◽  
P. A. Kohl ◽  
T. C. HODGE

ABSTRACTPolymer thin films (less than 20 ltm) are widely used as coatings and inter-level dielectrics in microelectronic applications. In multi-layer structures, stresses generated in the films due to interaction with adjacent layers and solvent evaporation induced shrinkage, cause the polymer chains to orient in the plane of the film resulting in anisotropic film properties. Characterization of properties in all directions is essential for accurate electrical and mechanical design and modeling.A new technique has been developed to measure, in-situ, the through-plane (z) properties of thin polymer films. A parallel plate capacitor device and an interdigitated electrode structure were used as sensors to detect changes in dielectric constant and thickness of thin polymer films under thermal or mechanical loading. The through-plane compression modulus and coefficient of thermal expansion were calculated and results are reported for benzocyclobutene (BCB) films.


2001 ◽  
Vol 34 (9) ◽  
pp. 3041-3045 ◽  
Author(s):  
Darrin J. Pochan ◽  
Eric K. Lin ◽  
Sushil K. Satija ◽  
Wen-li Wu

2021 ◽  
Vol 887 ◽  
pp. 79-84
Author(s):  
Marat N. Niyazov ◽  
Anatoliy I. Kupchishin ◽  
Buvkhan G. Taipova

The study of the deformation characteristics of thin polymer films has established 2 stages of increasing strain with increasing stress: the first stage in the elastic region is slow linear; the second stage is sharply exponential. The dependence of deformation (ε) on stress (σ) in polytetrafluoroethylene at various exposure doses has been experimentally investigated. Irradiation of the fluoroplastic films under study with electrons doses of 1, 3, 5, 7, and 10 kGy leads to significant changes in their mechanical properties, while the samples lose their plasticity and begin to break at a lower strain, which is associated with the formation of nanodefects in the structure of the material. A significant decrease in elongation is observed compared with unirradiated material. The reason for this is the degradation of the main chains of the fluoroplastic. With an increase in the absorbed dose, the Young's modulus increases exponentially, which is associated with a decrease in the distance between atoms in the structure of the sample. The resulting effect can be used in industry. The curves obtained for both non-irradiated and irradiated material are satisfactorily described in the exponential model.


Langmuir ◽  
2009 ◽  
Vol 25 (9) ◽  
pp. 5091-5097 ◽  
Author(s):  
D. Silbernagl ◽  
H. Sturm ◽  
B. Cappella*

Langmuir ◽  
2009 ◽  
Vol 25 (17) ◽  
pp. 9938-9946 ◽  
Author(s):  
Camila A. Rezende ◽  
Lay-Theng Lee ◽  
Fernando Galembeck

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