scholarly journals Heat Treatment of Pre-hydrolyzed Silane Increases Adhesion of Phosphate Monomer-based Resin Cement to Glass Ceramic

2015 ◽  
Vol 26 (1) ◽  
pp. 44-49 ◽  
Author(s):  
Rodrigo Furtado de Carvalho ◽  
Caroline Cotes ◽  
Estevão Tomomitsu Kimpara ◽  
Fabíola Pessoa Pereira Leite
Keyword(s):  
Heat Treatment ◽  
Bond Strength ◽  
Glass Ceramic ◽  
Testing Machine ◽  
Sem Analysis ◽  
Resin Cement ◽  
Control Group ◽  
Microtensile Bond Strength ◽  
Hot Air ◽  
Ceramic Blocks

This study evaluated the influence of different forms of heat treatment on a pre-hydrolyzed silane to improve the adhesion of phosphate monomer-based (MDP) resin cement to glass ceramic. Resin and feldspathic ceramic blocks (n=48, n=6 for bond test, n=2 for microscopy) were randomly divided into 6 groups and subject to surface treatments: G1: Hydrofluoric acid (HF) 9.6% for 20 s + Silane + MDP resin cement (Panavia F); G2: HF 9.6% for 20 s + Silane + Heat Treatment (oven) + Panavia F; G3: Silane + Heat Treatment (oven) + Panavia F; G4: HF 9.6% for 20 s + Silane + Heat Treatment (hot air) + Panavia F; G5: Silane + Heat Treatment (hot air) + Panavia F; G6: Silane + Panavia F. Microtensile bond strength (MTBS) test was performed using a universal testing machine (1 mm/min). After debonding, the substrate and adherent surfaces were analyzed using stereomicroscope and scanning electron microscope (SEM) to categorize the failure types. Data were analyzed statistically using two-way test ANOVA and Tukey's test (=0.05). Heat treatment of the silane containing MDP, with prior etching with HF (G2: 13.15±0.89a; G4: 12.58±1.03a) presented significantly higher bond strength values than the control group (G1: 9.16±0.64b). The groups without prior etching (G3: 10.47±0.70b; G5: 9.47±0.32b) showed statistically similar bond strength values between them and the control group (G1). The silane application without prior etching and heat treatment resulted in the lowest mean bond strength (G6: 8.05±0.37c). SEM analysis showed predominantly adhesive failures and EDS analysis showed common elements of spectra (Si, Na, Al, K, O, C) characterizing the microstructure of the glass-ceramic studied. Heat treatment of the pre-hydrolyzed silane containing MDP in an oven at 100 °C for 2 min or with hot air application at 50±5 ºC for 1 min, was effective in increasing the bond strength values between the ceramic and resin cement containing MDP.

Effects of Surface Treatments, Thermocycling, and Cyclic Loading on the Bond Strength of a Resin Cement Bonded to a Lithium Disilicate Glass Ceramic

2013 ◽  
Vol 38 (2) ◽  
pp. 208-217 ◽  
Author(s):  
GB Guarda ◽  
AB Correr ◽  
LS Gonçalves ◽  
AR Costa ◽  
GA Borges ◽  
...  
Keyword(s):  
Bond Strength ◽  
Glass Ceramic ◽  
Hydrofluoric Acid ◽  
Lithium Disilicate ◽  
Surface Treatments ◽  
Resin Cement ◽  
Control Group ◽  
Ceramic Surface ◽  
Microtensile Bond Strength ◽  
Ceramic Blocks

SUMMARY Objectives The aim of this present study was to investigate the effect of two surface treatments, fatigue and thermocycling, on the microtensile bond strength of a newly introduced lithium disilicate glass ceramic (IPS e.max Press, Ivoclar Vivadent) and a dual-cured resin cement. Methods A total of 18 ceramic blocks (10 mm long × 7 mm wide × 3.0 mm thick) were fabricated and divided into six groups (n=3): groups 1, 2, and 3—air particle abraded for five seconds with 50-μm aluminum oxide particles; groups 4, 5, and 6—acid etched with 10% hydrofluoric acid for 20 seconds. A silane coupling agent was applied onto all specimens and allowed to dry for five seconds, and the ceramic blocks were bonded to a block of composite Tetric N-Ceram (Ivoclar Vivadent) with RelyX ARC (3M ESPE) resin cement and placed under a 500-g static load for two minutes. The cement excess was removed with a disposable microbrush, and four periods of light activation for 40 seconds each were performed at right angles using an LED curing unit (UltraLume LED 5, Ultradent) with a final 40 second light exposure from the top surface. All of the specimens were stored in distilled water at 37°C for 24 hours. Groups 2 and 5 were submitted to 3,000 thermal cycles between 5°C and 55°C, and groups 3 and 6 were submitted to a fatigue test of 100,000 cycles at 2 Hz. Specimens were sectioned perpendicular to the bonding area to obtain beams with a cross-sectional area of 1 mm2 (30 beams per group) and submitted to a microtensile bond strength test in a testing machine (EZ Test) at a crosshead speed of 0.5 mm/min. Data were submitted to analysis of variance and Tukey post hoc test (p≤0.05). Results The microtensile bond strength values (MPa) were 26.9 ± 6.9, 22.2 ± 7.8, and 21.2 ± 9.1 for groups 1–3 and 35.0 ± 9.6, 24.3 ± 8.9, and 23.9 ± 6.3 for groups 4–6. For the control group, fatigue testing and thermocycling produced a predominance of adhesive failures. Fatigue and thermocycling significantly decreased the microtensile bond strength for both ceramic surface treatments when compared with the control groups. Etching with 10% hydrofluoric acid significantly increased the microtensile bond strength for the control group.

scholarly journals Can the silane heat treatment influence the bond durability between resin cements and a dental ceramic?

2020 ◽  
Vol 68 ◽  
Author(s):  
Ronaldo Luís Almeida de CARVALHO ◽  
Jean Soares MIRANDA ◽  
Rodrigo Furtado de CARVALHO ◽  
Michelly Rocha DUARTE ◽  
Estevão Tomomitsu KIMPARA ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Bond Strength ◽  
Resin Cement ◽  
Microtensile Bond Strength ◽  
Resin Cements ◽  
Luting Agents ◽  
All Ceramic ◽  
Cad Cam ◽  
Ceramic Blocks ◽  
Bond Durability

ABSTRACT Objective Evaluate the influence of silane heat treatment in bond durability between two resin cements and CAD/CAM feldspathic ceramic. Methods 40 feldspathic ceramic blocks were obtained, and were duplicated in microhybrid composite. All ceramic blocks were etched with 10% hydrofluoric acid for 20 s and received application of silane agent. The blocks were randomizedinto eight groups (n=5) according to the surface treatments and luting agents: P- Panavia F; PAg- Panavia F + Aging; HP- Heat Treatment + Panavia F; HPAg- Heat Treatment + Panavia F + Aging; R- RelyX ARC; Rag- RelyX ARC + Aging; HR- Heat Treatment + RelyX ARC; HRAg- Heat Treatment + RelyX ARC + Aging. The heat treatment was performed in furnace at 100 °C for 2 min. All blocks were cemented and cut to obtain samples with adhesive area of 1 mm2. Aging was performed with 10000 thermal cycles. The samples were subjected to microtensile bond strength test. Results The three-way ANOVA test revealed a significant interaction between cement versus heat treatment (p=0.001) and heat treatment versus thermal cycling (p=0.001) indicating that there was a change in bond strength due to surface treatment and aging. Conclusion Therefore, the heat treatment of the silane at 100 ºC for 2 minutes obtained higher values of bond strength between the resin cement and a feldspathic ceramicafter aging.

scholarly journals A área da superfície adesiva no ensaio de microtração afeta a resistência de união entre uma cerâmica feldspática e um cimento resinoso?

2018 ◽  
Vol 1 (1) ◽  
Author(s):  
Luiz Felipe Valandro ◽  
Mutlu Özcan ◽  
Regina Amaral ◽  
Sheila Pestana Passos ◽  
Marco Antonio Bottino
Keyword(s):  
Bond Strength ◽  
Surface Area ◽  
Glass Ceramic ◽  
Pearson Correlation ◽  
Testing Machine ◽  
Resin Cement ◽  
Microtensile Bond Strength ◽  
Correlation Test ◽  
Surface Areas ◽  
Pearson Correlation Test

Purpose: To evaluate the effect of the bonded surface area on the bond strength of a resin cement to a glass ceramic. Methods: Surfaces of 12 glass ceramic blocks (6x6x4mm3) were conditioned with 10% hydrofluoric acid and silanizated. The conditioned blocks were placed inside a silicone mold and the dual-cure resin cement was applied on the treated surface. Specimens were stored sectioned for obtaining samples with different bonded surface areas: Gr1 - 0.7mm x 0.7mm (0.5mm²), Gr2 - 1mm x 1mm (1mm²), Gr3 - 1.4mm x 1.4mm (2mm²). The non-trimmed beam samples were submitted to the microtensile bond strength test in a universal testing machine (cross-head speed: 1 mm/min). Data were statistically analyzed (ANOVA and Tukey’s test;; Pearson Correlation test). Results: The microtensile bond strength results were significantly affected by the bonded surface area (p<.0001). The highest bond strength (MPa) was of the Gr1 (26.3±8.2a), followed by Gr2 (20.8±6.5b) and Gr3 (16.1±5.7c). The Pearson correlation test revealed that there is an inverse correlation between bonded surface area and microtensile bond strength results (r=-0.5234; p<0.0001). Conclusion: The lowest bonded surface areas provided the highest values of bond strength.

Effect of Hydrofluoric Acid Concentration and Etching Time on Bond Strength to Lithium Disilicate Glass Ceramic

2017 ◽  
Vol 42 (6) ◽  
pp. 606-615 ◽  
Author(s):  
J Puppin-Rontani ◽  
D Sundfeld ◽  
AR Costa ◽  
AB Correr ◽  
RM Puppin-Rontani ◽  
...  
Keyword(s):  
Bond Strength ◽  
Glass Ceramic ◽  
Hydrofluoric Acid ◽  
Surface Characterization ◽  
Testing Machine ◽  
Lithium Disilicate ◽  
Resin Cement ◽  
Etching Time ◽  
Failure Data ◽  
Ceramic Blocks

SUMMARY The aim of this study was to evaluate the influence of different concentrations of hydrofluoric acid (HF) associated with varied etching times on the microshear bond strength (μSBS) of a resin cement to a lithium disilicate glass ceramic. Two hundred seventy-five ceramic blocks (IPS e.max Press [EMX], Ivoclar Vivadent), measuring 8 mm × 3 mm thickness, were randomly distributed into five groups according to the HF concentrations (n=50): 1%, 2.5%, 5%, 7.5%, and 10%. Further random distribution into subgroups was performed according to the following etching times (n=10): 20, 40, 60, 120, and 20 + 20 seconds. After etching, all blocks were treated with a silane coupling agent followed by a thin layer of an unfilled resin. Three resin cement cylinders (∅︀=1 mm) were made on each EMX surface, which was then stored in deionized water at 37°C for 24 hours before testing. The μSBS was in a universal testing machine at a crosshead speed of 1 mm/min until failure. Data were submitted to two-way analysis of variance, and multiple comparisons were performed using the Tukey post hoc test (α=0.05). One representative EMX sample was etched according to the description of each subgroup and evaluated using scanning electron microscopy for surface characterization. The HF concentrations of 5%, 7.5%, and 10% provided significantly higher μSBS values than 1% and 2.5% (p&lt;0.05), regardless of the etching times. For 1% and 2.5% HF, the etching times from 40 to 120 seconds increased the μSBS values compared with 20 seconds (p&lt;0.05), but etching periods did not differ within the 5%, 7.5%, and 10% HF groups (p&gt;0.05). The effect of re-etching was more evident for 1% and 2.5% HF (p&lt;0.05). Different HF concentrations/etching times directly influenced the bond strength and surface morphology of EMX.

scholarly journals Effect of Surface Treatments on the Bond Strength to Turkom-Cera All-ceramic Material

2016 ◽  
Vol 17 (11) ◽  
pp. 920-925 ◽  
Author(s):  
Bandar MA Al-Makramani ◽  
Fuad A Al-Sanabani ◽  
Abdul AA Razak ◽  
Mohamed I Abu-Hassan ◽  
Ibrahim Z AL-Shami ◽  
...  
Keyword(s):  
Bond Strength ◽  
Ceramic Material ◽  
Failure Modes ◽  
Testing Machine ◽  
Surface Treatments ◽  
Resin Cement ◽  
Control Group ◽  
Significant Difference ◽  
All Ceramic ◽  
Effect Of Surface

ABSTRACT Aim The aim of this study was to evaluate the effect of surface treatments on shear bond strength (SBS) of Turkom-Cera (Turkom-Ceramic (M) Sdn. Bhd., Puchong, Malaysia) all-ceramic material cemented with resin cement Panavia-F (Kuraray Medical Inc., Okayama, Japan). Materials and methods Forty Turkom-Cera ceramic disks (10 mm × 3 mm) were prepared and randomly divided into four groups. The disks were wet ground to 1000-grit and subjected to four surface treatments: (1) No treatment (Control), (2) sandblasting, (3) silane application, and (4) sandblasting + silane. The four groups of 10 specimens each were bonded with Panavia-F resin cement according to manufacturer's recommendations. The SBS was determined using the universal testing machine (Instron) at 0.5 mm/min crosshead speed. Failure modes were recorded and a qualitative micromorphologic examination of different surface treatments was performed. The data were analyzed using the one-way analysis of variance (ANOVA) and Tukey honestly significant difference (HSD) tests. Results The SBS of the control, sandblasting, silane, and sandblasting + silane groups were: 10.8 ± 1.5, 16.4 ± 3.4, 16.2 ± 2.5, and 19.1 ± 2.4 MPa respectively. According to the Tukey HSD test, only the mean SBS of the control group was significantly different from the other three groups. There was no significant difference between sandblasting, silane, and sandblasting + silane groups. Conclusion In this study, the three surface treatments used improved the bond strength of resin cement to Turkom-Cera disks. Clinical significance The surface treatments used in this study appeared to be suitable methods for the cementation of glass infiltrated all-ceramic restorations. How to cite this article Razak AAA, Abu-Hassan MI, AL-Makramani BMA, AL-Sanabani FA, AL-Shami IZ, Almansour HM. Effect of Surface Treatments on the Bond Strength to Turkom-Cera All-Ceramic Material. J Contemp Dent Pract 2016;17(11):920-925.

scholarly journals Influence of curing mode of resin luting cements on bond strength to dentin

2017 ◽  
Vol 15 (4) ◽  
pp. 258
Author(s):  
Marcelo Giannini ◽  
Andreia Assis Carvalho ◽  
Ariovaldo Stefani ◽  
Wladimir Franco de Sá Barbosa ◽  
Lawrence Gonzaga Lopes
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Resin Cement ◽  
Control Group ◽  
Resin Cements ◽  
Luting Cements ◽  
Halogen Light ◽  
Significant Difference ◽  
Tooth Surfaces ◽  
Light Curing

Self-adhesive, dual-polymerizing resin cements require no treatment to the prepared tooth surfaces before cementation. Aim: The aim of this study was to evaluate the influence of curing mode on bond strength (BS) of three cementing systems to bovine dentin. Methods: The buccal enamel surfaces of 50 bovine incisors were removed to expose dentin and to flat the surface. The teeth were divided into five groups (n=10), which consisted of two resin cements (Multilink and Clearfil SA Cement) that were tested in dual- (halogen light for 40 s) and self-cured modes, and a control (RelyX ARC). Two cylinders of resin cements (1.0 mm X 0.75 mm) were prepared on each bonded dentin surface. After 24h at 37oC, resin cylinders were subjected to micro-shear testing in a universal testing machine (4411/Instron - 0.5 mm/min). Data were statistically analyzed by two-way ANOVA, Tukey and Dunnett`s test (5%). Results: Multilink showed higher BS than those observed on Clearfil SA. Light-curing resulted in higher BS for both Multilink and Clearfil SA. When Multilink was light-cured, no significant difference on BS was demonstrated between it and RelyX ARC. Conclusions: The highest BS values were obtained in control group and light-cured Multilink resin cement.

scholarly journals Effect of Nd:YAG Laser with/without Graphite Coating on Bonding of Lithium Disilicate Glass-Ceramic to Human Dentin

2021 ◽  
Vol 2021 ◽  
pp. 1-7
Author(s):  
Amjad Abu Hasna ◽  
Stephanie Semmelmann ◽  
Fernanda Alves Feitosa ◽  
Danilo De Souza Andrade ◽  
Franklin R Tay ◽  
...  
Keyword(s):  
Bond Strength ◽  
Glass Ceramic ◽  
Nd:Yag Laser ◽  
Testing Machine ◽  
Glass Ceramics ◽  
Lithium Disilicate ◽  
Resin Cement ◽  
Cylindrical Shape ◽  
Universal Testing ◽  
Human Dentin

This study evaluated the effect of different surface treatments on the tensile bond strength between lithium disilicate glass-ceramics, resin cement, and dentin. Fifty truncated cone-shape glass-ceramics were divided into five groups (n = 10): G1, control: 10% hydrofluoric acid (HF); G2, Nd:YAG laser + silane; G3, Sil + Nd:YAG laser; G4, graphite + Nd:YAG laser + Sil; and G5, graphite + Sil + Nd:YAG laser. Fifty human third-molars were cut to cylindrical shape and polished to standardize the bonding surfaces. The glass-ceramic specimens were bonded to dentin with a dual-cured resin cement and stored in distilled water for 24 h at 37ºC. Tensile testing was performed on a universal testing machine (10 Kgf load cell at 1 mm/min) until failure. The bond strength values (mean ± SD) in MPa were G1 (9.4 ± 2.3), G2 (9.7 ± 2.0), G3 (6.7 ± 1.9), G4 (4.6 ± 1.1), and G5 (1.2 ± 0.3). Nd:YAG laser and HF improve the bond strength between lithium disilicate glass-ceramics, resin cement, and dentin. The application of a graphite layer prior to Nd:YAG laser irradiation negatively affects this bonding and presented inferior results.

scholarly journals Effect of Provisional Cements on Shear Bond Strength of Porcelain Laminate Veneers

2011 ◽  
Vol 05 (04) ◽  
pp. 373-379 ◽  
Author(s):  
Subutay Han Altintas ◽  
Onjen Tak ◽  
Asli Secilmis ◽  
Aslihan Usumez
Keyword(s):  
Bond Strength ◽  
Calcium Hydroxide ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Acrylic Resin ◽  
Resin Cement ◽  
Control Group ◽  
Molar Teeth ◽  
Laminate Veneers ◽  
Selection Of

ABSTRACTObjectives: The purpose of this study was to evaluate the effect of three provisional cements and two cleaning techniques on the final bond strength of porcelain laminate veneers. Methods: The occlusal third of the crowns of forty molar teeth were sectioned and embedded in autopolymerizing acrylic resin. Dentin surfaces were polished and specimens were randomly divided into four groups (n=10). Provisional restorations were fabricated and two provisional restorations were cemented onto each tooth. Restorations were fixed with one of three different provisional cements: eugenol-free provisional cement (Cavex), calcium hydroxide (Dycal), and light-cured provisional cement (Tempond Clear). Provisional restorations were removed with either a dental explorer and air-water spray, or a cleaning bur (Opticlean). In the control group, provisional restorations were not used on the surfaces of specimens. IPS Empress 2 ceramic discs were luted with a dual-cured resin cement (Panavia F). Shear bond strength was measured using a universal testing machine. Data were statistically analyzed by ANOVA, Tukey’s HSD and Dunnett tests. Surfaces were examined by scanning electronic microscopy. Results: Significant differences were found between the control group and both the light-cured provisional cement groups and the eugenol-free provisional cement-cleaning bur group (P<.05). Groups that had received light-cured provisional cement showed the lowest bond strength values. Conclusions: Selection of the provisional cement is an important factor in the ultimate bond strength of the final restoration. Calcium hydroxide provisional cement and cleaning with a dental explorer are advisable. (Eur J Dent 2011;5:373-379)

scholarly journals Influence of Air Abrasion and Sonic Technique on Microtensile Bond Strength of One-Step Self-Etch Adhesive on Human Dentin

2015 ◽  
Vol 2015 ◽  
pp. 1-6 ◽  
Author(s):  
Baraba Anja ◽  
Dukić Walter ◽  
Chieffi Nicoletta ◽  
Ferrari Marco ◽  
Sonja Pezelj Ribarić ◽  
...  
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Control Group ◽  
Air Abrasion ◽  
Microtensile Bond Strength ◽  
Dentin Surface ◽  
Significant Difference ◽  
Human Dentin ◽  
One Step ◽  
Self Etch

The purpose of thisin vitrostudy was to evaluate the microtensile bond strength of one-step self-etch adhesive to human dentin surface modified with air abrasion and sonic technique and to assess the morphological characteristics of the pretreated dentin surface. The occlusal enamel was removed to obtain a flat dentin surface for thirty-six human molar teeth. The teeth were randomly divided into three experimental groups (n= 12 per group), according to the pretreatment of the dentin: (1) control group, (2) air abrasion group, and (3) sonic preparation group. Microtensile bond strength test was performed on a universal testing machine. Two specimens from each experimental group were subjected to SEM examination. There was no statistically significant difference in bond strength between the three experimental groups (P> 0.05). Mean microtensile bond strength (MPa) values were 35.3 ± 12.8 for control group, 35.8 ± 13.5 for air abrasion group, and 37.7 ± 12.0 for sonic preparation group. The use of air abrasion and sonic preparation with one-step self-etch adhesive does not appear to enhance or impair microtensile bond strength in dentin.

scholarly journals Bond Strength of Overdenture Locator Posts Cemented with Seven Luting Agents

2013 ◽  
Vol 14 (4) ◽  
pp. 675-680
Author(s):  
Khalil Aleisa
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Mean Value ◽  
Resin Cement ◽  
Control Group ◽  
Resin Cements ◽  
Human Teeth ◽  
Luting Agents ◽  
Relyx Unicem ◽  
Significant Difference

ABSTRACT Statement of the problem Post retention is crucial factor in restoration survival. Posts are commonly failed due to loss of retention. It is unknown which luting agents would provide the maximum bond strength for Locator overdenture posts. Aim The aim of this study was to evaluate the bond retentive strengths of Locator overdenture posts cemented with 7 luting agents. Materials and methods One hundred and five single rooted human teeth were decoronated and randomly assigned to 7 groups (n = 15). Post spaces were prepared with Locator post drills to the depth of 6 mm. The Locator posts were cemented with Variolink II, RelyX ARC, Multilink N, RelyX Unicem, ParaCore, or MultiCore Flow resin luting agents. Zinc phosphate cement was served as control group. Specimens were stored in water at 37°C for 24 hours. Each specimen was loaded in tension in an Instron universal testing machine. The maximum force required to dislodge each Locator post was recorded. Means and standard deviations were calculated and data were statistically analyzed with one-way analysis of variance (ANOVA). Results The highest mean bond strength value for Locator posts was recorded for MultiCore® Flow group (mean = 550.1 N), while the lowest mean value was for RelyX Unicem™ resin cement group (mean = 216.8 N). A statistically significant difference in mean locator overdenture post bond strength was observed between the 7 cement types (p < 0.0001). ParaCore™ and MultiCore® Flow groups had significantly higher bond strength than all other groups, but they were not differed from each other. Conclusion Bond strength of Locator overdenture posts were influenced by the type of luting agents. MultiCore Flow and ParaCore resin cements offered the greatest retention. Clinical significance The type of luting agents had a significant effect on the retention of Locator posts. The use of Core buildup resin cements as luting agent with Locator post demonstrated the greatest retention. How to cite this article Aleisa K. Bond Strength of Overdenture Locator Posts Cemented with Seven Luting Agents. J Contemp Dent Pract 2013;14(4):675-680.

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