INVESTIGATION OF HOT ISOSTATIC PRESSING AND HEAT TREATMENT EFFECT ON STRUCTURE AND MECHANICAL PROPERTIES OF 3D-PRINTED SAMPLES MADE FROM VT6-PS GRADE MATERIAL

2021 ◽  
pp. 22-30
Author(s):  
A.I. Vasilev ◽  
◽  
P.V. Panin ◽  
S.V. Putyrskiy ◽  
A.M. Rogalev ◽  
...  

Presents the results of the investigation of the influence of hot isostatic pressing and heat treatment on the structure and mechanical properties during tension of synthesized workpieces obtained by selective laser alloying from a metal-powder composition of VT6 alloy. The blanks were subjected to heat treatment at various temperatures in the state after synthesis, as well after HIP. The influence of different heat treatment modes was assessed by the results of tensile tests and structural researches.

Materials ◽  
2020 ◽  
Vol 13 (17) ◽  
pp. 3805 ◽  
Author(s):  
Janusz Kluczyński ◽  
Lucjan Śnieżek ◽  
Krzysztof Grzelak ◽  
Artur Oziębło ◽  
Krzysztof Perkowski ◽  
...  

In this study, we analyzed the mechanical properties of selectively laser melted (SLM) steel obtained via different modifications during and after the manufacturing process. The aim was to determine the effects of precipitation heat treatment on the mechanical properties of elements additively manufactured using three different process parameters. Some samples were additionally obtained using hot isostatic pressing (HIP), while some were treated using two different types of heat treatment and a combination of those two processes. From each manufactured sample, a part of the material was taken for structural analysis including residual stress analysis and microstructural investigations. In the second part of the research, the mechanical properties were studied to define the scleronomic hardness of the samples. Finally, tensile tests were conducted using a digital image correlation (DIC) test and fracture analysis. The treated samples were found to be significantly elongated, thus indicating the advantages of using precipitation heat treatment. Additionally, precipitation heat treatment was found to increase the porosity of samples, which was the opposite compared to HIP-treated samples.


Metals ◽  
2020 ◽  
Vol 10 (6) ◽  
pp. 753 ◽  
Author(s):  
Kanwal Chadha ◽  
Yuan Tian ◽  
John Spray ◽  
Clodualdo Aranas

In this work, the microstructural features and mechanical properties of an additively manufactured 316L stainless steel have been determined. Three types of samples were characterized: (i) as printed (AP), (ii) annealing heat treated (AHT), and (iii) hot isostatic pressed and annealing heat treated (HIP + AHT). Microstructural analysis reveals that the AP sample formed melt pool boundaries with nano-scale cellular structures. These structures disappeared after annealing heat treatment and hot isostatic pressing. The AP and AHT samples have similar grain morphologies; however, the latter has a lower dislocation density and contains precipitates. Conversely, the HIP + AHT sample displays polygon-shaped grains with twin structures; a completely different morphology compared to the first two samples. Optical micrography reveals that the application of hot isostatic pressing reduces the porosity generated after laser processing. The tensile strengths of all the samples are comparable (about 600 MPa); however, the elongation of the HIP + AHT sample (48%) was superior to that of other two samples. The enhanced ductility of the HIP + AHT sample, however, resulted in lower yield strength. Based on these findings, annealing heat treatment after hot isostatic pressing was found to improve the ductility of as-printed 316L stainless steel by as much as 130%, without sacrificing tensile strength, but the sample may have a reduced (40%) yield strength. The tensile strength determined here has been shown to be higher than that of the hot isostatic pressed, additively manufactured 316L stainless steel available from the literature.


Materials ◽  
2021 ◽  
Vol 14 (20) ◽  
pp. 6140
Author(s):  
Evgenii Borisov ◽  
Igor Polozov ◽  
Kirill Starikov ◽  
Anatoly Popovich ◽  
Vadim Sufiiarov

Multimaterial additive manufacturing is an attractive way of producing parts with improved functional properties by combining materials with different properties within a single part. Pure Ti provides a high ductility and an improved corrosion resistance, while the Ti64 alloy has a higher strength. The combination of these alloys within a single part using additive manufacturing can be used to produce advanced multimaterial components. This work explores the multimaterial Laser Powder Bed Fusion (L-PBF) of Ti/Ti64 graded material. The microstructure and mechanical properties of Ti/Ti64-graded samples fabricated by L-PBF with different geometries of the graded zones, as well as different effects of heat treatment and hot isostatic pressing on the microstructure of the bimetallic Ti/Ti64 samples, were investigated. The transition zone microstructure has a distinct character and does not undergo significant changes during heat treatment and hot isostatic pressing. The tensile tests of Ti/Ti64 samples showed that when the Ti64 zones were located along the sample, the ratio of cross-sections has a greater influence on the mechanical properties than their shape and location. The presented results of the investigation of the graded Ti/Ti64 samples allow tailoring properties for the possible applications of multimaterial parts.


2020 ◽  
Vol 9 (1) ◽  
pp. 580-595 ◽  
Author(s):  
Yali Zhang ◽  
Xiaosong Jiang ◽  
Hongliang Sun ◽  
Zhenyi Shao

AbstractIn this study, nonequiatomic Co28.5Cr21.5Fe20Ni26Mo4 medium-entropy alloys (MEAs) were prepared using hot isostatic pressing. The effect of annealing heat treatment on microstructure and mechanical properties of MEAs was investigated. The results showed that the microstructure of as-sintered alloys was mainly composed of the face-centered cubic (FCC) phase and μ phase. The presence of the μ phase could improve the compressive strength of Co28.5Cr21.5Fe20Ni26Mo4 MEAs. Meanwhile, the ductile FCC phase matrix could effectively suppress the propagation of cracks to improve its ductility. Hence, as-sintered MEAs possessed excellent compression properties, and the average compressive strength value was 2,606 MPa when the strain was 50%. Compared with as-sintered MEAs, the phase composition of as-annealed MEAs did not change. The micro-hardness of annealed MEAs was stable compared to as-sintered MEAs (342 HV), and its fluctuation was about ±30 HV. The compressive strength of the annealed MEAs did not alter greatly, and the maximum fluctuation value was only about 6.5%. Hence, Co28.5Cr21.5Fe20Ni26Mo4 MEAs had excellent thermal stability.


Metals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 884
Author(s):  
A-Ra Jo ◽  
Ji-Seob An ◽  
Sun-Hyung Kim ◽  
Myeong-Sik Jeong ◽  
Young-Hoon Moon ◽  
...  

Tungsten carbide-cobalt (WC-Co) alloys have various mechanical properties according to their Co content and manufacturing method. High-strength materials such as WC-Co alloys are usually manufactured using various sintering methods. In this study, WC-Co was compared according to the Co content and manufacturing method using the sinter-hot isostatic pressing process. Furthermore, an additional test was performed to investigate the effect of post-hot isostatic pressing (HIP) treatment on the mechanical properties. To compare tensile strength, threaded end and shoulder end specimens are generally applied in axial tensile testing with hard metals. However, it is extremely difficult to shape WC-Co by machining. A tensile testing jig for a shoulder end specimen is, therefore, proposed. Tensile tests were conducted using the proposed jig, and microstructure, hardness, and impact tests were carried out to compare the mechanical properties. The microstructure evolution was obtained by decreasing the Co content and applying the HIP treatment, resulting in changes in Young’s modulus and strength. The results indicated that the proposed jig of the axial tensile test could be applied to the extremely hard WC-Co, and the mechanical properties of WC-Co could be modified by the Co content and HIP treatment control.


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