scholarly journals Profil FTIR Minyak Ikan dan Lemak Babi serta Perbandingannya sebagai Dasar Penentuan Autentifikasi Halal

ALCHEMY ◽  
2020 ◽  
Vol 8 (1) ◽  
pp. 9
Author(s):  
Dewi Sinta Megawati ◽  
Begum Fauziyah ◽  
Siti Maimunah ◽  
Abdul Wafi

<p>Research has been conducted on the determination of tuna oil and lard spectra using FTIR. This research aims to determine the IR spectra profile of lard and tuna oil and to compare both spectra profiles. Profile and comparison of lard and tuna oil IR spectra useful to determine whether an ingredient or a product contaminated with lard. The fatty acid profile of lard by FTIR analysis showed a significant difference in the absorption patterns of the spectra, especially at 3010-3000, 1680- 1600, and 968-966 cm-1 wavenumbers which represented the different composition and type of fatty acids in the lard and tuna oil. The absorption patterns at 3007 and 1653 cm-1 regions (double bond C=C cis) for tuna oil showed relatively high peaks if it is compared to lard samples because of the percentage of MUFA fatty acids (oleic acid) in tuna oil was much higher. </p><p> </p><p>Telah dilakukan penelitian mengenai penentuan spektra minyak ikan tuna dan lemak babi dengan menggunakan FTIR. Penelitian ini bertujuan untuk mengetahui profil spektra IR dari lemak babi dan minyak ikan tuna serta membandingkan kedua profil spektranya. Profil dan perbandingan spektra IR lemak babi dan minyak ikan tuna dapat digunakan sebagai dasar penentuan apakah suatu bahan atau produk terkontaminasi lemak babi. Profil asam lemak babi hasil analisis FTIR menunjukkan adanya perbedaan yang cukup signifikan pada pola-pola penyerapan spektra, khususnya pada bilangan gelombang 3010-3000, 1680-1600 dan 968-966 cm-1 yang merepresentasikan perbedaan komposisi dan jenis asam lemak pada sampel lemak babi dan minyak ikan tuna. Pola serapan pada bilangan gelombang 3007 dan 1653 cm-1 (ikatan rangkap C=C cis) untuk sampel minyak ikan tuna menunjukkan puncak yang relatif tinggi jika dibandingkan dengan sampel lemak babi karena persentase asam lemak MUFA (asam oleat) pada minyak ikan tuna jauh lebih tinggi. </p>

2016 ◽  
Vol 38 (4) ◽  
Author(s):  
YANUZI MARA VARGAS CAMILO ◽  
ELI REGINA BARBOZA DE SOUZA ◽  
RONALDO VELOSO NAVES ◽  
ROSÂNGELA VERA ◽  
MUZA DO CARMO VIEIRA

ABSTRACT The present research aimed to determine the fatty acid profile in the seed oil of cagaita fruits cultivated in Goiânia, state of Goiás, in 2013 and 2014 harvests. The study was carried out with fruits produced by cagaita trees cultivated in the field of the School of Agronomy, Federal University of Goiás (EA/UFG), Goiânia, GO, where, in 1998, 440 cagaita seedlings from different municipalities in Goiás were planted. Fruits were collected from plants with 16 years of age in full production stage. Cagaita seeds show in their fatty acid profile mostly linoleic acid, oleic acid and palmitic acid. There was no variation in fatty acids content present in seeds between years 2013 and 2014, assuming that there are no external influences such as weather, foliar nutrients or soil, in the production of these oils


2021 ◽  
Vol 10 (2) ◽  
pp. 044-056
Author(s):  
Zelalem Gizachew Admassie ◽  
Jibrel Abdulkadir Eman ◽  
Sisay Awoke Endalew

The fatty acids, cholesterol compositions and the ratio between unsaturated and saturated fatty acids are important parameters for the determination of the nutritional value of certain oils. Most oils sold in our markets are claimed they are cholesterol- free and their fatty acid profile is unknown. To determine the cholesterol and fatty acid profile of commercially sold vegetable oils in three places, twelve oil samples were analyzed for their cholesterol and fatty acid compositions. Cholesterol was detected in most sample oils except in nigger seed and peanut oils. Locally produced Sunflower oil has significantly (p < 0.05) highest cholesterol concentration (24.31±0.85) while Modjo oil has the least concentration (0.78± 0.16 mg/l). High saturated fatty acids were found in palm oil (43.87) with predominant presence of palmitic acid. Oleic acid (C16:0) is the predominant one in sunflower oil. Hamaressa and Modjo oils contained 46.12%, 16.7% Erucic acid (C20:1) respectively. Linoleic acid (C18:2 6c) was predominant in soybean oils (52.45–59.54%), corn oil (61.73%) and sunflower oil (43.54%). The highest percentage composition of alpha-linolenic acid was found in Hamaressa oil (1.27%) followed by Modjo oil (0.5%). Sesame, peanut and sunflower ( high oleic acid) oils were found to be better for salad and cooking purposes than other oils due to lower saturated and higher monounsaturated fatty acid contents. In general, the research output disclosed the quantity of cholesterol detected in sample oils contradicts the label of cholesterol claimed by most of the producers and marketers.


2012 ◽  
Vol 32 (2) ◽  
pp. 234-238 ◽  
Author(s):  
Marli da Silva Santos ◽  
Obdulio Gomes Miguel ◽  
Carmen Lúcia Oliveira Petkowicz ◽  
Lys Mary Bileski Cândido

This study aimed to evaluate the antioxidant potential and fatty acid profile of gabiroba (Campomanesia xanthocarpa Berg) seeds. In order to obtain the extract, the seeds were dried, crushed, and subjected to sequential extraction by maceration and percolation in a modified soxhlet extractor using solvent polarity gradient composed of hexane, chloroform, ethyl acetate, and alcohol, respectively. The extraction time was six hours. The ethanol extract showed the highest antioxidant potential, given by the EC50 value and the amount of total phenolic compounds. High amounts of unsaturated fatty acids were found in the oil studied, especially the oleic acid.


1987 ◽  
Vol 33 (12) ◽  
pp. 1116-1120 ◽  
Author(s):  
Panchanon Chattopadhyay ◽  
Santu Kumar Banerjee ◽  
Kalyani Sen ◽  
Parul Chakrabarti

Conidial lipids of the wild-type (V35) Aspergillus niger and its unsaturated fatty acid auxotroph (UFA2) were compared. The wild type contained lower levels (7.6%) of phospholipids and higher levels (28.4%) of glycolipids than the mutant (16.5 and 22.2%, respectively). Oleic (33.4%), linoleic (22.5%), palmitic (12.8%), stearic (7.4%), and linolenic (6.2%) were the main fatty acids of the wild type (V35). The mutant grew only in the presence of unsaturated fatty acid having at least one Δ9cis double bond, and its conidial fatty acid profile was influenced by the exogenous acid. Analyses of the fatty acids of UFA2 grown in the presence of different fatty acid supplements support the original view that the mutant is defective in Δ9-desaturase activity.


Author(s):  
D. B. Kiin-Kabari ◽  
P. S. Umunna ◽  
S. Y. Giami

African elemi (Canarium schweinfurthii) fruit pulp oil was extracted and refined which yielded 39.5% oil. It was characterized for its physical, chemical, phytochemical properties and fatty acid profile in comparison with palm kernel oil (PKO). The result for physical properties revealed that there was no significant difference in the density, refractive index, and flash point of the oils. African elemi fruit pulp oil (AEO) had significantly (p>0.05) higher slip melting point and viscosity while significantly (p<0.05) lower smoke point and fire point. Chemical properties of the oils such as iodine, acid value, unsaponifiable matter and free fatty acids were significantly (p>0.05) higher in AEO with the values of 76.79 g/100 g, 0.94 mg KOH/g, 1.32 and 0.58%, respectively and significantly (p<0.05) lower in saponification and peroxide values, 155.47 mg KOH/g and 1.06 meq/kg, respectively compared to the values obtained for the PKO. Saturated fatty acid profile of AEO had the values of 9.44, 32.24 and 2.63% for myristic (C14:0), stearic acid (C18:0) and palmitic acid (C16:0) while PKO had the values of 48.00, 16.20, 2.50 and 8.40% for lauric (C12:0), myristic (C14:0), stearic acid (C18:0) and palmitic acid (C16:0), respectively. The monounsaturated fatty acids were oleic acid (C18:1) 30.24% for AEO and 15.0% for PKO making oleic acid the highest occurring monounsaturated fatty acids present in AEO. Thus, lauric acid (C12:0) and linoleic (C18:2) was not dictated in AEO while gadoleic (C20:1) was not dictated in PKO. Flavonoids, tannins, saponins, phytates and alkaloids had the values of 0.29, 0.33, 0.13, 0.13 and 0.74% for AEO and 0.32, 0.12, 0.24, 0.11 and 0.07% for PKO, respectively and all were within the acceptable limit of 3% for food products with respect to the phytochemical properties of the oils. The result for solid fat content - temperature profile revealed that PKO and AEO completely melted at 35 °C and 45 °C, respectively.


2019 ◽  
Vol 13 (4) ◽  
Author(s):  
E. Ghanbari Shendia ◽  
D. Sivri Ozaya ◽  
M. Ozkayab

In this study, a Mobile Olive Oil Processing Unit (TEM Oliomio 500-2GV, Italy) was designed and used for cold press extra virgin olive oil (EVOO) production at optimum conditions. Local olive varieties “Beylik, Tavşan Yüreği, Uslu and Saurani in Antalya, Manisa, and Hatay provinces of Turkey were investigated in the present study. EVOO was stored before and after paper filtration. Generally, no significant change was observed in fatty acid composition during 60 days of storing and filtration had no detectable effect, but there was significant difference among EVOOs which was obtained from different cultivars. Results of this study showed that fatty acid profile of EVOOs was good method for classification of Turkish olive oils. Beylik and Tavşan Yüreği had higher oleic acid content than other cultivars. Saurani EVOO had the highest content of palmitic acid and stearic acid. The highest amount of linoleic acid was detected in EVOO of Uslu (Manisa) with the range of 12.06-12.09%. Olive oil samples were classified as EVOO according to International olive council (IOC) regulations. Turkish virgin olive oils characterized by low linoleic and palmitic, and high oleic acid contents.


Author(s):  
Mısra Bakan ◽  
Elif Ayşe Erdoğan Eliuz ◽  
Deniz Ayas

In this study, seasonal changes in the lipid and fatty acid profiles of S. lessepsianus caught from the Mersin Bay were investigated. The total lipid levels of S. lessepsianus were found to be 2.94%, 7.19%, 2.45%, 0.83%, in spring, summer, autumn and winter season, respectively. Major fatty acids in S. lessepsianus were palmitic acid, stearic acid, oleic acid, palmitoleic acid, eicosapentaenoic acid (EPA) and docosahexaenoic acid (DHA) in all seasons. The highest values of palmitic, palmitoleic and EPA were determined as 22.97%, 3.80% and 4.22% in spring, respectively. The highest values of stearic and oleic acid were determined as 15.93% and 7.84% in autumn, respectively. The highest value of DHA were also determined as 31.91% in winter season. The EPA level from polyunsaturated fatty acids was found in the range of 2.54-4.22% (23.09-195.62 mg/100g). The highest level of DHA were observed in the winter season and its levels changed in the range of 19.83-31.81% and was calculated as 201.29-1301.73 mg/100g. In addition, the highest level of the Σn3, Σn6, and Σn9 were calculated in the summer season as 1516.39, 114.88, 399.77 mg/100g, respectively. This report showed that fat and fatty acid profiles of S. lessepsianus are quite influenced by seasonal factors.


2011 ◽  
Vol 40 (3) ◽  
pp. 463-468 ◽  
Author(s):  
Rodrigo Yutaka Dichoff Kasai ◽  
Ana Lúcia Salaro ◽  
Jener Alexandre Sampaio Zuanon ◽  
Céphora Maria Sabarense ◽  
Mateus Moraes Tavares ◽  
...  

The objective of this work was to evaluate suplemenation of vitamin C during feed training of giant trahira fingerlings. An experiment was established in a complete random design with seven treatments (0.0, 17.5, 52.5, 87.5, 122.5, 175.0 and 350.0 mg vitamin C/kg diet) and four repetitions. Giant trahira fingerlings (2.8 ± 0.2 cm) were distributed in 6-L aquaria at the density of 6 fish/L. A basal diet was formulated with 44.0% of crude protein and vitamin C and bovine heart were added in it daily. After 20 days, biometry of fish for evaluation of weight and length gains, rates of survival and cannibalism and uniformity of final length and for macroscopic observations of clinical signs of deficiency or excess of vitamin was carried out. After biometry evaluation, ten fish from each tested diet were collected for analysis of the fatty acid profile which was compared to profile of fish at the same life stage fed forage fish collected from breeding fishponds. Data on growth performance and fatty acid profiles were submitted to analyses of polynomial regression and uniformity of the final length was evaluated by the Bartlett test. There was a significant difference only for uniformity in final length and fatty acid profile of the carcass. Supplementation with 52.5 mg vitamin C/kg diet provided a greater uniformity of the final length of the fish. Fish from breeding fishponds presented lower concentration of PUFA (polyunsaturated fatty acids) and higher concentration of saturated fatty acids compared to fish trained to accept dry diets.


2019 ◽  
Vol 3 (2) ◽  
Author(s):  
J. Slaughter ◽  
T. Peckman ◽  
K. Burdick ◽  
Z. Callahan ◽  
B. Wiegand

ObjectivesThe objective of this study was to evaluate the effect of dietary inclusion of high oleic soybean meal and oil on broiler performance and lipid quality.Materials and MethodsMale Ross 308 broiler chicks (n = 160) were sorted by weight and randomly assigned to one of two treatments containing 10 replicate pens with 8 broilers each. Treatment groups consisted of a control corn-soy diet that included commodity soybean meal and oil (CON) and a corn-soy diet containing high oleic soybean meal and oil (HO). Broilers received, ad libitum, a two-phase diet consisting of starter (d0–21) containing 5% oil and grower (d21–42) containing 3% oil. Pen weight (PW) and feed intake (FI) were recorded on Days 0, 21, and 42 and used to calculate feed to gain ratio (F:G). Broilers were slaughtered on d42, after which carcasses were weighed and fabricated. Weights of fabricated parts were recorded for carcass yield. Samples of breast and thigh meat were taken for fatty acid profile analysis, which was conducted using a modified version of methods by Folch et al. (1957) and Morrison and Smith (1964). To measure lipid oxidation, boneless, skinless breast halves chosen randomly from each pen were placed on Styrofoam trays and overwrapped with oxygen permeable, polyvinyl chloride and placed in retail storage (4°C) and used for collection of thiobarbituric acid reactive substances (TBARS) on Day 1, 3, and 5 of storage. Data was analyzed using PROC GLM procedure in SAS, with level of significance set at P < 0.05.ResultsCON pens had a greater (P < 0.002) change in weight (23480.61 g. vs. 21829.39 g.), however, the CON treatment had an increase in FI (P < 0.0003) compared to the HO treatment (29841.74 g. vs. 27405.68 g). Thus, there was no significant difference (P = 0.22) in F:G between treatments. While there was no difference (P = 0.39; P = 0.71) in percent carcass yield or breast yield, the CON treatment had a higher (P = 0.01) percent thigh yield compared to the HO treatment (16.36% vs. 15.86%). Results of lipid oxidation showed there was an effect of day (P < 0.0001), but no treatment or interaction effects were observed. Diet changed (P < 0.0001) the proportion of saturated fatty acids (SFA), monounsaturated fatty acids (MUFA), and polyunsaturated fatty acids (PUFA) in breast and thigh meat. HO treatment increased the proportion of MUFA and decreased the proportion of PUFA and SFA in both breast and thigh meat. Both breast and thigh samples from the HO treatment had increased (P < 0.0001) proportions of oleic acid (C18:1) and decreased proportions of linoleic acid (C18:2) compared to the control. Inclusion of HO soybean meal and oil in broiler diets resulted in increased uptake of MUFA (C18:1) and decreased PUFA (C18:2) in both breast and thigh meat, while having no impact on broiler feed efficiency.ConclusionPull through effect of HO acid seen in fatty acid analysis of broiler meat shows the ability to serve as a mechanism to increase oleic acid inclusion in human diets. Oleic acid needs are potentially related to omega-3 fatty acid needs which are shown to have health benefits related to cardiac health in humans among other things. Studies have shown that increases in oleic acid in diets can lead to an increase in omega-3 fatty acids.


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