scholarly journals A novel surfactant-assisted dilute phosphoric acid plus steam explosion pretreatment of poplar wood for fermentable sugar production

Author(s):  
Denghui Tong ◽  
Peng Zhan ◽  
Weifeng Zhang ◽  
Yongcai Zhou ◽  
Yilei Huang ◽  
...  

Abstract Pretreatment is an indispensable process in lignocellulosic bioethanol production. In this work, a surfactant agent JFC was introduced into the dilute phosphoric acid plus steam explosion pretreatment scheme for fermentable sugar production using poplar as substrate. Four crucial factors (phosphoric acid concentration, surfactant concentration, pressure, and residence time) affecting the pretreatment efficiency were optimized using the single factor tests. The optimal parameters obtained were as follows: 1:2.5 solid/liquid rate, 2 h pre-soaking time, 1.5 %(v/v) JFC-M + 2.0 wt% phosphoric acid, 2.0 MPa pressure, and 120 s residence time, resulting in a maximum cellulose recovery rate of 86.33 % and enzymatic saccharification rate of 84.62 %, which was 38.97 % higher than that of control. The morphological and structural characteristics of samples before and after pretreatment, were characterized by the scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier transform infrared (FTIR) method. The addition of JFC-M was of a notable influence in overcoming biomass recalcitrance and boosting cellulose digestion, showing great application potentials in biomass conversion process.

Author(s):  
Johanna Olsson ◽  
Michael Persson ◽  
Mats Galbe ◽  
Ola Wallberg ◽  
Ann-Sofi Jönsson

AbstractEfficient fractionation of lignocellulosic biomass is an important step toward the replacement of fossil-based products. However, the utilisation of all of the components in biomass requires various fractionation techniques. One promising process configuration is to apply steam explosion for the recovery of hemicelluloses and a subsequent hydrotropic extraction step for the delignification of the remaining solids. In this work, the influence of residence time, temperature and biomass loading on lignin recovery from birch using sodium xylene sulphonate as a hydrotrope was investigated. Our results show that residence time, temperature and biomass loading correlate positively with lignin extraction, but the effects of these parameters were limited. Furthermore, when steam explosion was implemented as the initial step, hydrotropic extraction could be performed even at room temperature, yielding a lignin extraction of 50%. Also, hydrothermal degradation of the material was necessary for efficient delignification with sodium xylene sulphonate, regardless of whether it occurs during steam explosion pretreatment or is achieved at high temperatures during the hydrotropic extraction.


2020 ◽  
Vol 148 ◽  
pp. 112279 ◽  
Author(s):  
C. Padilla-Rascón ◽  
E. Ruiz ◽  
I. Romero ◽  
E. Castro ◽  
J.M. Oliva ◽  
...  

RSC Advances ◽  
2016 ◽  
Vol 6 (80) ◽  
pp. 76848-76854 ◽  
Author(s):  
Sujun Wang ◽  
Xianhong Ouyang ◽  
Wenya Wang ◽  
Qipeng Yuan ◽  
Aixia Yan

As an emerging method for lignocellulose pretreatment, the ultrasound-assisted Fenton reaction is not well developed in comparison to the dilute acid-catalysed steam explosion.


2010 ◽  
Vol 113-116 ◽  
pp. 525-528 ◽  
Author(s):  
Xu Tao Wang ◽  
Li Sha Liu

The research on biomass conversion technology has attracted great attention of the world along with the shortage of fossil energy resources. But the effect and efficiency of the pretreatment technique now used in biomass conversion are not so perfect. Using new steam explosion technique as a pretreatment process of biomass conversion has been reported rarely. The mechanism of steam explosion and its application effect in biomass conversion and utilization were introduced and analyzed respectively in this paper. The result showed that the semi-cellulose of steam exploded corn stalk degraded greatly to 7.57% from 25.4%, and a little cellulose and lignin degraded in this process. The saccharification rate of steam exploded green reserved corn stalk was 33.4% under the condition 2.0Mpa, 120s. It’s 1.33 times higher than the unexploded. According to the result of experimentation, the steam explosion technique should be a good pretreatment method for biomass conversion.


2012 ◽  
Vol 06 ◽  
pp. 745-750
Author(s):  
AI ASAKAWA ◽  
CHIZURU SASAKI ◽  
CHIKAKO ASADA ◽  
YOSHITOSHI NAKAMURA

Waste Shiitake (Lentinula edodes) mushroom medium, a lignocellulosic aglicultural residue, was evaluated as a fermentable substrate. 87% of the fermentable sugars remained in the waste mushroom medium. The sugar yield of the waste mushroom medium (46.3%) was higher than that of raw mushroom medium (20.3%) after 48 h of enzymatic saccharification by Meicelase because L. edodes changed wood structure. These results indicated that the waste mushroom medium is a suitable substrate for fermentation. Next, the efficient ethanol production using steam explosion pretreatment was studied. After 30 h of simultaneous saccharification and fermentation (SSF) using Meicelase and Saccharomyces cerevisiae AM12, 20.0 g/L ethanol was produced from 100 g/L water-insoluble residue of the waste mushroom medium treated at a steam pressure of 20 atm and a steaming time of 5 min. This corresponded to an ethanol yield of 77.0% of the theoretical, i.e. 14.7 g of ethanol obtained from 100 g of waste mushroom medium.


2013 ◽  
Vol 94 (8) ◽  
pp. 1607-1613 ◽  
Author(s):  
Amir Daraei Garmakhany ◽  
Mahdi Kashaninejad ◽  
Mehran Aalami ◽  
Yahya Maghsoudlou ◽  
Mortza Khomieri ◽  
...  

2013 ◽  
Vol 2013 ◽  
pp. 1-5 ◽  
Author(s):  
Anna Šutka ◽  
Silvija Kukle ◽  
Janis Gravitis ◽  
Laima Grave

Microfibrillated cellulose was extracted from hemp fibres using steam explosion pretreatment and high-intensity ultrasonic treatment (HIUS). The acquired results after steam explosion treatment and water and alkali treatments are discussed and interpreted by Fourier transform infrared spectroscopy (FTIR). Scanning electron microscopy (SEM) was used to examine the microstructure of hemp fibres before and after each treatment. A fibre size analyser was used to analyse the dimensions of the untreated and treated cellulose fibrils. SEM observations show that the sizes of the different treated fibrils have a diameter range of several micrometres, but after HIUS treatment fibres are separate from microfibrils, nanofibres, and their agglomerates.


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