scholarly journals Process Optimization for the Synthesis of Silver (AgNPs), Iron Oxide (α-Fe2O3NPs) and Core-Shell (Ag-Fe2O3CNPs) Nanoparticles Using the Aqueous Extract of Alstonia Scholaris: A Greener Approach

2018 ◽  
Vol 12 (1) ◽  
pp. 29-39 ◽  
Author(s):  
Navinchandra G. Shimpi ◽  
Mujahid Khan ◽  
Sharda Shirole ◽  
Shriram Sonawane
Keyword(s):  
Fourier Transform ◽  
Iron Oxide ◽  
Aqueous Extract ◽  
Core Shell ◽  
Shell Nanoparticles ◽  
Alstonia Scholaris ◽  
Transmission Electron ◽  
Infra Red ◽  
High Level ◽  
Core Shell Nanoparticles

Objective:The present study is deals with the green synthesis of silver (AgNPs), iron oxide (α-Fe2O3NPs) and core-shell (Ag-α-Fe2O3CNPs) nanoparticles using the aqueous extract ofAlstonia scholariswithout any catalyst, template or surfactant or any intermediate under ultrasound cavitation technique. The purpose was to facilitate the high level of dispersion with increase in rate of reaction. Further AgNPs and α-Fe2O3NPs were used to synthesis Ag-Fe2O3CNPs in aqueous extract ofAlstonia scholarisunder controlled ultrasound cavitation technique.Methods:The size of AgNPs and Ag-Fe2O3CNPs can be tuned by optimizing various reaction parameters. UV-visible, X-ray diffraction spectroscopy (XRD), Transmission electron microscopy (TEM), Field emission scanning electron microscope (FE-SEM) and Fourier transform infra-red spectroscopy has been used for the characterization of silver and core shell Ag@Fe2O3nanoparticles. TEM images clearly show the formation of core shell nanoparticles with spherical morphology.Result:Fourier transform infra-red spectroscopy analysis revealed that carbohydrate, polyphenols, and protein molecules were involved in the synthesis and capping of silver, iron oxide and Ag@Fe2O3CNPs.

Iron Oxide-Gold Core-Shell Nanoparticles as Multimodal Imaging Contrast Agent

2013 ◽  
Vol 13 (6) ◽  
pp. 2341-2347 ◽  
Author(s):  
Luca Menichetti ◽  
Leonardo Manzoni ◽  
Luigi Paduano ◽  
A. Flori ◽  
Claudia Kusmic ◽  
...  
Keyword(s):  
Iron Oxide ◽  
Contrast Agent ◽  
Multimodal Imaging ◽  
Core Shell ◽  
Shell Nanoparticles ◽  
Gold Core ◽  
Core Shell Nanoparticles ◽  
Imaging Contrast Agent

Monodisperse Fe3O4/Fe Core/Shell Nanoparticles with Enhanced Magnetic Property

2011 ◽  
Vol 306-307 ◽  
pp. 410-415
Author(s):  
Li Sun ◽  
Fu Tian Liu ◽  
Qi Hui Jiang ◽  
Xiu Xiu Chen ◽  
Ping Yang
Keyword(s):  
Average Diameter ◽  
Chemical Precipitation ◽  
Precipitation Method ◽  
Core Shell ◽  
X Ray Diffraction ◽  
Shell Nanoparticles ◽  
X Ray ◽  
Transmission Electron ◽  
Shell Particles ◽  
Core Shell Nanoparticles

Core/shell type nanoparticles with an average diameter of 20nm were synthesized by chemical precipitation method. Firstly, Monodisperse Fe3O4 nanoparticles were synthesized by solvethermal method. FeSO4ž7H2O and NaBH4 were respectively dissolved in distilled water, then moderated Fe3O4 particles and surfactant(PVP) were ultrasonic dispersed into the FeSO4ž7H2O solution. The resulting solution was stirred 2 h at room temperature. Fe could be deposited on the surface of monodispersed Fe3O4 nanoparticles to form core-shell particles. The particles were characterized by using various experimental techniques, such as transmission electron microscopy (TEM), X-ray diffraction (XRD), AGM and DTA. The results suggest that the saturation magnetization of the nanocomposites is 100 emu/g. The composition of the samples show monodisperse and the sides of the core/shell nanoparticles are 20-30nm. It is noted that the formation of Fe3O4/Fe nanocomposites magnetite nanoparticles possess superparamagnetic property.

Nanoporous and nanostructured materials made out of clusters for environmental applications

2005 ◽  
Vol 876 ◽  
Author(s):  
Jiji Antony ◽  
Joseph Nutting ◽  
Donald R. Baer ◽  
You Qiang
Keyword(s):  
Iron Oxide ◽  
Chemical Reactivity ◽  
Building Blocks ◽  
High Rate ◽  
Core Shell ◽  
Shell Nanoparticles ◽  
Nanoporous Films ◽  
Iron Iron ◽  
Iron Oxide Core ◽  
Core Shell Nanoparticles

AbstractThe nanoporous materials prepared from iron-iron oxide core-shell nanoparticles are of great interest due to their enhanced possibilities for distribution in the environment, a high rate of chemical reactivity and also the possibility to enhance environmentally friendly reaction paths. However, production of these nanoparticle porous materials by conventional methods is difficult. Therefore, we use a cluster deposition system, which prepares the iron nanoclusters and iron-iron oxide core shell nanoclusters at room temperature. The nanoporous films are synthesized by using the nanoclusters as building blocks. These films are characterized using Transmission Electron Microscopy (TEM), Atomic Force Microscopy (AFM), and the Brunauer-Emmett-Teller (BET) method for surface area determination.

scholarly journals Dye-doped biodegradable nanoparticle SiO2 coating on zinc- and iron-oxide nanoparticles to improve biocompatibility and for in vivo imaging studies

Nanoscale ◽  
2020 ◽  
Vol 12 (10) ◽  
pp. 6164-6175 ◽  
Author(s):  
Elena Navarro-Palomares ◽  
Paula González-Saiz ◽  
Carlos Renero-Lecuna ◽  
Rosa Martín-Rodríguez ◽  
Fernando Aguado ◽  
...  
Keyword(s):  
Iron Oxide ◽  
In Vivo Imaging ◽  
Oxide Nanoparticles ◽  
Core Shell ◽  
Imaging Studies ◽  
Sio2 Coating ◽  
Shell Nanoparticles ◽  
Nano Medicine ◽  
Core Shell Nanoparticles

Core–shell nanoparticles provide two fold functionality in nano medicine: reduction of nanotoxicity and improving as a tool for imaging and therapy.

PEG-Iron Oxide Core-Shell Nanoparticles: In situ Synthesis and In vitro Biocompatibility Evaluation for Potential T2-MRI Applications

2020 ◽  
Vol 10 (4) ◽  
pp. 1107-1120
Author(s):  
Karina Almeida Barcelos ◽  
Marli Luiza Tebaldi ◽  
Eryvaldo Socrates Tabosa do Egito ◽  
Nádia Miriceia Leão ◽  
Daniel Cristian Ferreira Soares
Keyword(s):  
Iron Oxide ◽  
In Situ Synthesis ◽  
Core Shell ◽  
Shell Nanoparticles ◽  
In Vitro Biocompatibility ◽  
Iron Oxide Core ◽  
Core Shell Nanoparticles ◽  
T2 Mri
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