Evaluation of the Effect of Cold Plasma Treatment on the Microshear Bond Strength of Composite Resin Restorations to Dentin using Different Adhesive Systems and the Effect of Thermocycling

Introduction: Currently, non-thermal plasma is used to modify the enamel and dentin surfaces to improve the bonding surface to dental composite resins. Non-thermal plasma creates a hydrophilic surface, decreases the contact angle, and improves the bonding quality. The present study aimed to evaluate the microshear bond strength (µSBS) of composite resins to dentin using different adhesive systems. Materials and Methods: Bovine incisor teeth were randomly assigned to three groups of G-Premio, Clearfil SE Bond, and Adper Single Bond adhesive groups after preparation. Each group was divided into two subgroups in terms of argon plasma surface preparation, and each subgroup was divided into two groups in terms of thermocycling (n=12). The microshear bond strength of the samples was determined using a universal testing machine. Three-way ANOVA was used to analyze the effect of the adhesive, plasma preparation, and thermocycling. Post hoc Tukey tests were used for two-by-two comparisons of µSBS. Statistical significance was set at P <0.05. Results: The results of the µSBS test showed that the application of plasma resulted in a significant increase in the mean µSBS in the G-Premio group, with no significant increase in the Clearfil SE bond and Adper Single groups. The effect of thermocycling after plasma application was significant only in the Adper Single group. Conclusion: The application of plasma might increase the bond strength of composite resins to dentin. However, further studies are necessary.

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Microshear Bond Strength of Different Adhesive Systems to Dentin

Frontiers in Dentistry ◽

10.18502/fid.v16i4.2085 ◽

2019 ◽

Author(s):

Sara Valizadeh ◽

Aida Moradi ◽

Mansooreh Mirazei ◽

Hooman Amiri ◽

Mohammad Javad Kharazifard

Keyword(s):

Bond Strength ◽

Testing Machine ◽

Single Bond ◽

Adhesive Systems ◽

Etch And Rinse ◽

Significant Difference ◽

Microshear Bond Strength ◽

Self Etch ◽

Composite Cylinders

Objectives: The aim of this study was to compare the microshear bond strength (µSBS) of various adhesive systems to dentin. Materials and Methods: In this in vitro experimental study, 60 sound human third molars were divided into four groups. Dentin discs were prepared of middle-third dentin measuring 4 mm in diameter and 2 mm in thickness. Dentin surfaces were bonded with one of the four types of adhesives: (A) Single Bond (3M ESPE), Scotchbond Universal (3M ESPE) in etch and rinse (B) and self-etch (C) modes and (D) Clearfil SE Bond (Kuraray Noritake Dental). After the application of adhesive systems according to the manufacturers’ instructions, composite cylinders (Vit-l-escence) were bonded to dentin surfaces. The μSBS test was performed using a universal testing machine at a crosshead speed of 1 mm/min. Data were analyzed with one-way ANOVA and Tukey’s test (α=0.05). Results: The µSBS was the highest in self-etch Scotchbond Universal (15.8±6.08 MPa) followed by Clearfil SE Bond (15.24±4.6 MPa), etch and rinse Scotchbond Universal (11.68±4.07MPa) and Single Bond (11.24±3.74 MPa). A significant difference was only found between Single Bond and etch and rinse Scotchbond Universal groups (P=0.04). Conclusion: Based on the results of this study, application of Scotchbond Universal in self-etch mode provides a reliable bond to dentin.

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Microshear Bond Strength of Different Adhesive Systems to Dentin

Frontiers in Dentistry ◽

10.18502/fid.v14i4.2085 ◽

2019 ◽

Author(s):

Sara Valizadeh ◽

Aida Moradi ◽

Mansooreh Mirazei ◽

Hooman Amiri ◽

Mohammad Javad Kharazifard

Keyword(s):

Bond Strength ◽

Testing Machine ◽

Single Bond ◽

Adhesive Systems ◽

Etch And Rinse ◽

Significant Difference ◽

Microshear Bond Strength ◽

Self Etch ◽

Composite Cylinders

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Non-thermal plasma increase bond strength of zirconia to a resin cement

Brazilian Dental Science ◽

10.14295/bds.2018.v21i2.1562 ◽

2018 ◽

Vol 21 (2) ◽

pp. 210 ◽

Cited By ~ 3

Author(s):

Beatriz Togoro Ferreira Da Silva ◽

Lívia Tosi Trevelin ◽

Fernanda De Sá Teixeira ◽

Maria Cecília Salvadori ◽

Paulo Francisco Cesar ◽

...

Keyword(s):

Surface Roughness ◽

Surface Energy ◽

Bond Strength ◽

Surface Treatment ◽

Thermal Plasma ◽

Oxygen Plasma ◽

Resin Cement ◽

Suitable Alternative ◽

Non Thermal Plasma ◽

Microshear Bond Strength

Objective: This study investigated the influence of different surface treatments on zirconia surface energy, roughness and microshear bond strength. Material and Methods: Forty eight slices of Yttria-stabilized tetragonal zirconia polycrystal (Y-TZP- VITA In-Ceram® YZ for inLab®) (6.4 x 3.2 x 1.6 mm) were divided into 3 groups according to the surface treatment (n = 16): YTZP_control -untreated; YTZP_plasma -surface treatment with non-thermal oxygen plasma; YTZP_primer - coating with ceramic primer. Surface energy (n = 6) was measured with a goniometer; and surface roughness (n = 10) was analyzed with a 3D profilometer were performed over zirconia surface. On the same specimens of surface roughness, on the treated zirconia's surface, resin cement (PANAVIA V5 - Kuraray Noritake Dental) was built up by inserting the resin cement into Tygon tubes (1 mm of internal diameter X 1 mm length). After 24 h storage, microshear test was assessed. Data were analyzed by one-way ANOVA and Tukey post-hoc test (p < 0.05). Results: Non-thermal oxygen plasma treated specimens exhibited higher statistically significant surface energy (p = 0.00) and bond strength (p = 0.00) when compared to control and primer groups. Roughness test (p = 0.897) could not detect statistical difference among the tested groups. Conclusion: Non-thermal oxygen plasma should be a suitable alternative for zirconia surface treatment prior to luting hence it improved microshear bond strength and provided higher surface energy without affecting surface roughness. Keywords Adhesion; Non-thermal plasma; Surface treatment.

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Effect of Fluoride and Simplified Adhesive Systems on the Bond Strength of Primary Molars and Incisors

Brazilian Dental Journal ◽

10.1590/0103-6440201300160 ◽

2015 ◽

Vol 26 (4) ◽

pp. 368-373

Author(s):

Leily Macedo Firoozmand ◽

Lawanne Ellen Carvalho Noleto ◽

Isabella Azevedo Gomes ◽

José Roberto de Oliveira Bauer ◽

Meire Coelho Ferreira

Keyword(s):

Bond Strength ◽

Testing Machine ◽

Group Analysis ◽

Adhesive System ◽

Composite Resins ◽

Primary Molars ◽

Adhesive Systems ◽

Etch And Rinse ◽

Prior Application

The aim of this study was evaluate in vitro the influence of simplified adhesive systems (etch-and-rinse and self-etching) and 1.23% acidulated phosphate fluoride (APF) on the microshear bond strength (μ-SBS) of composite resins on primary molars and incisors. Forty primary molars and forty incisors vestibular enamel was treated with either the self-etching Clearfil SE Bond (CSE, Kuraray) or etch-and-rinse Adper Single Bond 2 (SB2, 3M/ESPE) adhesive system. Each group was subdivided based on the prior treatment of the enamel with or without the topical application of 1.23% APF. Thereafter, matrices were positioned and filled with composite resin and light cured. After storage in distilled water at 37±1°C for 24 h, the specimens were submitted to μ-SBS in a universal testing machine. Kruskal-Wallis and Mann-Whitney tests (p<0.05) showed that the prior application of 1.23% APF led to a significant reduction in bond strength. The type of adhesive exerted no significant influence bond strength. In the inter-group analysis, however, significantly bond strength reduction was found for the incisors when CSE was employed with APF. Adhesive failure was the most common type of fracture. The bond strength was affected by the prior application of 1.23% APF and type of tooth.

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Effect of cpp-acp on the bond strength of silorane and methacrylate based restorative systems

Journal of Research in Dentistry ◽

10.19177/jrd.v1e1201364-71 ◽

2013 ◽

Vol 1 (1) ◽

pp. 64

Author(s):

Bruno de Castro Ferreira Barreto ◽

Anderson Catelan ◽

Marina Baptista Aleixo ◽

Gisele Rodrigues Silva ◽

Tathy Aparecida Xavier ◽

...

Keyword(s):

Bond Strength ◽

Hybrid Composites ◽

Resin Composite ◽

Testing Machine ◽

Adhesive Systems ◽

Universal Testing ◽

Significant Difference ◽

S Matrix ◽

Casein Phosphopeptide ◽

Microshear Bond Strength

This study evaluated the influence of the previous application of casein phosphopeptide amorphous calcium phosphate (CPP-ACP) on the bond strength of two restorative systems to dentin. Self-etching adhesive systems Clearfil SE Bond (Kuraray) and FiltekTM LS System Adhesive (3M ESPE) were used in combination with two micro-hybrid composites FiltekTM Z250 (3M ESPE) and FiltekTM LS (3M ESPE), respectively. Twenty-eight sound human third molars had the occlusal surface worn until the total exposure of dentin and were randomly divided into 4 groups (n = 7): G1 (Clearfil + Z250), G2 (CPP-ACP + Clearfil + Z250), G3 (LS system) and G4 (CPP-ACP + LS system). The application of the paste containing CPP-ACP was held in the dentin of G2 and G4 prior to adhesive protocol, which followed the manufacturer's recommendations. Two cylinders of a single increment of resin composite were built on each dentin surface using tygon`s matrix with 1.26 mm of diameter x 1 mm high and light-cured with LED Bluephase 16i (Vivadent) apparatus. Microshear bond strength test was conducted in a universal testing machine (EZ Test, Shimadzu) with a speed of 0.5 mm/min. The data were subjected to two-way ANOVA test with a significance of 5%. There was no significant difference on bond strength between restorative systems with or without the previous use of a CPP-ACP paste. It was concluded that the application of CPP-ACP in the dentin prior to adhesive protocol did not influence the bond strength of the restorative systems tested.

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Effect of dentinal surface preparation on bond strength of self-etching adhesive systems

Brazilian Oral Research ◽

10.1590/s1806-83242006000100010 ◽

2006 ◽

Vol 20 (1) ◽

pp. 52-58 ◽

Cited By ~ 4

Author(s):

Patrícia Itocazo Rocha ◽

Alessandra Bühler Borges ◽

José Roberto Rodrigues ◽

César Augusto Galvão Arrais ◽

Marcelo Giannini

Keyword(s):

Bond Strength ◽

High Speed ◽

Testing Machine ◽

Surface Preparation ◽

Surface Treatments ◽

Cross Sectional Area ◽

Sectional Area ◽

Adhesive Systems ◽

Cross Sectional ◽

Low Speed

The aim of this study was to evaluate the effects of dentin surface treatments on the tensile bond strength (TBS) of the self-etching primer Clearfil SE Bond (CSE) and the one-step self-etching One-Up Bond F (OUB). The exposed flat dentin surfaces of twenty-four sound third molars were prepared with diamond bur at high-speed, carbide bur at low-speed or wet ground with #600 grit SiC paper. The adhesive systems were applied to the dentin surfaces and light-cured according to the manufacturers' instructions. A 6-mm high composite crown was incrementally built-up and each increment was light-cured for 40 seconds. After being stored in water (37°C/24 h), the samples were serially sectioned parallel to the long axis, forming beams (n = 20) with a cross-sectional area of approximately 0.8 mm². The specimens were tested in a Universal Testing Machine at 0.5 mm/min. The cross-sectional area was measured and the results (MPa) were analyzed by two-way ANOVA and Tukey Test (p < 0.05). Overall, the groups treated with CSE exhibited the highest TBS for all surface treatments. Dentin surfaces prepared with carbide bur at low speed reduced TBS in the CSE group; however, OUB was not affected by surface treatments. The effect of surface abrasive methods on TBS was material-dependent.

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Interfacial Fracture Toughness Comparison of Three Indirect Resin Composites to Dentin and Polyether Ether Ketone Polymer

European Journal of Dentistry ◽

10.1055/s-0040-1713309 ◽

2020 ◽

Vol 14 (03) ◽

pp. 456-461

Author(s):

Rayhaneh Khalesi ◽

Mahdi Abbasi ◽

Zahra Shahidi ◽

Masoumeh Hasani Tabatabaei ◽

Zohreh Moradi

Keyword(s):

Fracture Toughness ◽

Bond Strength ◽

Testing Machine ◽

Composite Resins ◽

High Wear Resistance ◽

Luting Cements ◽

Anterior Teeth ◽

Polyether Ether Ketone ◽

Ether Ketone

Abstract Objectives Advances in laboratory composites and their high wear resistance and fracture toughness have resulted in their growing popularity and increasing use for dental restorations. This study sought to assess the fracture toughness of three indirect composites bonded to dental substrate and polyether ether ketone (PEEK) polymer. Materials and Methods This in vitro study was conducted on two groups of dental and polymer substrates. Each substrate was bonded to three indirect composite resins. Sixty blocks (3 × 3 × 12 mm) were made of sound bovine anterior teeth and PEEK polymer. Sixty blocks (3 × 3 × 12 mm) were fabricated of CRIOS (Coltene, Germany), high impact polymer composite (HIPC; Bredent, Germany), and GRADIA (Indirect; GC, Japan) composite resins. Composites were bonded to dentin using Panavia F 2.0 (Kuraray, Japan). For bonding to PEEK, Combo.lign (Bredent) and Visio.Link (Bredent) luting cements were used. In all samples, a single-edge notch was created by a no. 11 surgical blade at the interface. The samples were subjected to 3,500 thermal cycles, and their fracture toughness was measured in a universal testing machine (Zwick/Roell, Germany) by application of four-point flexural load. Statistical Analysis Data were analyzed using one-way analysis of variance, Kruskal–Wallis. Results The fracture toughness of CRIOS–PEEK interface was significantly higher than HIPC–PEEK. The fracture toughness of GRADIA–PEEK was not significantly different from that of HIPC and CRIOS. The fracture toughness of GRADIA–dentin was significantly higher than HIPC–dentin. Conclusion Considering the limitations of this study, GRADIA has the highest bond strength to dentin, while CRIOS shows the highest bond strength to PEEK.

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Efficacy of Fiber Post Bonding To Root Dentin after Different Obturation Techniques and Cementation Timings: In Vitro Study

Open Access Macedonian Journal of Medical Sciences ◽

10.3889/oamjms.2018.343 ◽

2018 ◽

Vol 6 (9) ◽

pp. 1707-1711

Author(s):

Rami M. Atia ◽

Nada Omar ◽

Haidy Nabil ◽

Yousra Aly

Keyword(s):

Bond Strength ◽

Statistical Significance ◽

Testing Machine ◽

In Vitro Study ◽

Resin Cement ◽

Vitro Study ◽

Endodontically Treated Teeth ◽

Root Dentin ◽

Push Out

OBJECTIVE: The aim of this in vitro study was to assess the effect of obturation technique and cementation timings on the bonding of fibre-reinforced posts to the root canal walls. METHODS: Twenty extracted teeth were randomly allocated to two groups according to the obturation technique and cementation timing. Central incisors with single canals were used after being decoronated. Every extracted tooth of the {vertical compaction group} (VC) group (n = 10) had been obturated using the {E & Q plus obturation system} with posts cemented in the same day; The other (CO) conventional group (n = 10) teeth were obturated using the conventional lateral compaction technique and posts cemented after one week. “SF“ Fiber posts were used after bonding and cementation using Rely X ARC resin cement with all the endodontically treated teeth. The push-out test was performed in a universal testing machine. Data were analysed by 2 way analysis of variance with Statistical significance was set to 0.05. RESULTS: Heat softened gutta percha group showed more push out the bond strength of the bonded posts than the conventional obturation group (p < 0.05). In the middle region, there was no statistical significance between the two groups while there was significance in the coronal and apical thirds. CONCLUSION: The vertical compaction technique and early cementation improved the bond strength of the resin posts in comparison to the conventional obturation technique with late cementation.

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Effect of Different Protocols in Preconditioning With EDTA in Sclerotic Dentin and Enamel Before Universal Adhesives Applied in Self-etch Mode

Operative Dentistry ◽

10.2341/16-014-l ◽

2017 ◽

Vol 42 (3) ◽

pp. 284-296 ◽

Cited By ~ 3

Author(s):

EC Martini ◽

SO Parreiras ◽

MF Gutierrez ◽

AD Loguercio ◽

A Reis

Keyword(s):

Bond Strength ◽

Adhesive Systems ◽

Microtensile Bond Strength ◽

Universal Adhesive ◽

Etching Pattern ◽

Bonding Performance ◽

Universal Adhesives ◽

Microshear Bond Strength ◽

Self Etch ◽

Main Factor

SUMMARY Objectives: The aim of this study was to investigate the effect of different protocols of 17% ethylene diamine tetra-acetic acid (EDTA) conditioning on the etching pattern and immediate bond strength of universal adhesives to enamel and sclerotic dentin. Methods and Materials: Forty bovine teeth with sclerotic dentin and 20 human third molars were randomly divided into eight groups resulting from the combination of the main factors surface treatment (none, two-minute EDTA conditioning manual application, 30-second EDTA manual application, 30-second EDTA sonic application) and adhesives systems (Scotchbond Universal Adhesive [SBU] and Prime & Bond Elect [PBE]). Resin-dentin and enamel-dentin bond specimens were prepared and tested under the microtensile bond strength (μTBS) and microshear bond strength (μSBS) tests, respectively. The etching pattern produced on the unground enamel and the sclerotic dentin surfaces under the different protocols and adhesive systems was evaluated under scanning electron microscopy. Results: For enamel, only the main factor adhesive was significant (p<0.0001), with SBU showing the highest μSBS. In sclerotic dentin, the lowest mean was observed for the group without EDTA application and the highest mean in the group with EDTA application with the sonic device for 30 seconds. Regardless of the EDTA protocol, the highest means of μTBS were observed for SBU (p<0.05). Conclusions: EDTA conditioning improves the bonding performance of universal adhesives in the self-etch mode on sclerotic dentin, mainly when applied for 30 seconds with the aid of a sonic device. EDTA pretreatment also improves the retentive etching pattern of enamel, but it does not result in higher enamel bond strength.

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Effect of Tannic Acid on Bond Strength of Etch and Rinse and Self-etch Adhesive Systems in Dentin of Primary Teeth

The Journal of Contemporary Dental Practice ◽

10.5005/jp-journals-10024-1984 ◽

2017 ◽

Vol 18 (1) ◽

pp. 34-38

Author(s):

Mojtaba Abdollahi ◽

Masoumeh Ebrahimi ◽

Alireza Sarraf Shirazi ◽

Faraneh Abdolhoseinpour

Keyword(s):

Bond Strength ◽

Tannic Acid ◽

Primary Teeth ◽

Testing Machine ◽

T Test ◽

Adhesive Systems ◽

Primary Molar ◽

Etch And Rinse ◽

Self Etch

ABSTRACT Introduction One of the possible mechanisms for the gradual destruction of bond strength in dentin-resin interface, could be due to the demineralized unstable collagen matrix. Use of protease inhibitors, such as tannic acid (TA) could prevent destruction of collagen fibers. The aim of this study was to compare the TA effect on bond strength of etch and rinse and self-etch adhesive systems in the dentin of primary teeth. Materials and methods This in vitro study was done on 40 extracted primary molar teeth. The teeth were sectioned in the mesiodistal direction, and enamel of buccal and lingual surfaces was removed. Samples were randomly divided into four groups: Single bond (SB) + TA, SB, Clearfil SE Bond (CSB) + TA, and CSB. Then, Z250 and Clearfil AP-X composites were cured on the surfaces of SB and CSB groups respectively. After that, all samples were divided into aging and non-aging groups. For 3 months, samples were placed under 1,000 thermal cycles in aging group. Subsequently, the shear bond strengths of all groups were measured by the International testing machine, and failure mode was evaluated by an optical stereomicroscope. Data were analyzed with paired t-test and independent t-test. Results Tannic acid induced a significant reduction in the immediate bond strength of adhesive SB. Meanwhile, TA had no significant effect on shear bond strength of the CSB system. Conclusion Based on our findings, use of TA is not recommended with SB and CSB adhesives on primary teeth. Clinical significance Tannic acid may not be considered in resin restorations of primary teeth. How to cite this article Ebrahimi M, Sarraf Shirazi A, Abdolhoseinpour F, Abdollahi M. Effect of Tannic Acid on Bond Strength of Etch and Rinse and Self-etch Adhesive Systems in Dentin of Primary Teeth. J Contemp Dent Pract 2017;18(1):34-38.

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