scholarly journals Оптические и фотолюминесцентные свойства тонкопленочной структуры ZnO-ЦТСЛ в ультрафиолетовом и видимом диапазонах спектра

2019 ◽  
Vol 127 (12) ◽  
pp. 986
Author(s):  
Л.В. Григорьев ◽  
Я.Б. Егорова ◽  
Н.А. Быков ◽  
А.А. Семенов ◽  
А.А. Никитин

The results of a study of the structural, optical, and photoluminescent properties of the thin-film structure ZnO/ferroelectric ceramics PLZT are presented. The results of X-ray diffraction analysis of a zinc oxide film synthesized on a PLZT substrate and on a quartz substrate are presented. The transmission spectra, reflection spectra, absorption spectra, and spectral dependence of the photoluminescence of the thin-film structure of ZnO- PLZT and the structure of ZnO-SiO2 in the ultraviolet and visible spectral ranges are presented.

2014 ◽  
Vol 83 (12) ◽  
Author(s):  
M A Shcherbina ◽  
S N Chvalun ◽  
Sergey Anatol'evich Ponomarenko ◽  
Mikhail Valentinovich Kovalchuk

2022 ◽  
Vol 130 (2) ◽  
pp. 242
Author(s):  
Л.В. Григорьев ◽  
А.А. Семенов ◽  
А.В. Михайлов

Presents the results of the study of the structural, optical and photo luminescent properties of the thin films ZnO on LiNbO3 substrate. The results of X-ray structural analysis of a zinc oxide film synthesized on a single-crystal LiTaO3 substrate and on a KU-1 quartz substrate are presented. Present the transmission spectra, reflection spectra and the spectral dependence of zinc oxide thin films on substrate LiTaO3 and the structure of ZnO-SiO2 in the ultraviolet and visible spectral ranges.


2001 ◽  
Vol 664 ◽  
Author(s):  
A. C. Dillon ◽  
L. Gedvillas ◽  
D. L. Williamson ◽  
J. Thiesen ◽  
J. D. Perkins ◽  
...  

ABSTRACTThe structure of thin film SiN, deposited by the hot wire chemical vapor deposition (HWCVD) technique using SiH4 and NH3 gas mixtures, has been examined as a function of the amount of H2 dilution of the gas mixture. For NH3/SiH4 gas ratios > 0.5/1, all films are a-SiN:H. While H2 dilution does not change the basic film structure, in that the films are amorphous with all dilutions, H2 dilution does increase the efficiency of NH3 dissociation in the gas phase, and causes a further reduction in the already small amount of N-H bonding in a-SiN:H films deposited by HWCVD. For NH3/SiH4 gas ratios typically <0.5/1 and with high H2 dilution, the first deposition of µc-SiN is demonstrated. X-ray diffraction (XRD) measurements demonstrate that the structure of these films consists of silicon crystallites embedded in an a-SiN:H matrix. An upper limit for N incorporation with the preservation of microcrystallinity was found, beyond which the films again became amorphous. The existence of this limit is explained in terms of structural disorder in the a-SiN:H tissue brought about by N incorporation.


2004 ◽  
Vol 146 (3) ◽  
pp. 243-250 ◽  
Author(s):  
P. Ostoja ◽  
P. Maccagnani ◽  
M. Gazzano ◽  
M. Cavallini ◽  
J.C. Kengne ◽  
...  

1991 ◽  
Vol 113 (1) ◽  
pp. 58-62 ◽  
Author(s):  
Yoshiki Oshida ◽  
P. C. Chen

A five-layered (Cu/Cr/Kapton® /Cr/Cu) metallic thin film structure was subjected to a completely reversed bending fatigue cycling with a wide ranges of applied strain amplitudes from 0.25 percent to about 30 percent. A new model for determination of the number of cycles to fatigue failure NF was proposed for single-crack and multi-crack formations. Within a strain amplitude ranging from 1 to 10 percent, a Manson-Coffin’s relationship was recognized for both the number of cycles to crack initiation NC and NF with exponents of 0.39 and 0.51, respectively. Selected fatigued test samples were further subjected to X-ray diffraction line analysis for dislocation density (ρ) calculation, which was related to the number of fatigue cycles N and strain amplitude (Δ εT) in an empirical formula. It was also found that dislocation densities accumulated up to both Nc and NF were related to applied strain amplitudes. Consequently, if applied strain amplitude is known and progressive change in dislocation density is measured, one can predict the remaining fatigue life as well as fatigue cycles which were already consumed.


2020 ◽  
Vol 16 ◽  
pp. 317-324 ◽  
Author(s):  
Atsunori Mori ◽  
Keisuke Fujita ◽  
Chihiro Kubota ◽  
Toyoko Suzuki ◽  
Kentaro Okano ◽  
...  

Differently substituted thiophene–thiophene-alternating copolymers were formally synthesized employing a halo-bithiophene as a monomer. Nickel-catalyzed polymerization of bithiophene with substituents at the 3-position, including alkyl-, fluoroalkyl-, or oligosiloxane-containing groups, afforded the corresponding copolymers in good to excellent yield. The solubility test in organic solvents was performed to reveal that several copolymers showed a superior solubility. X-ray diffraction analysis of the thin film of the alternating copolymers composed of methyl and branched oligosiloxane substituents was also performed, and the results suggested the formation of a dual-layered film structure.


Author(s):  
Ayu Uswatu Lissa Sapta Setyadi ◽  
Yofentina Iriani ◽  
Fahru Nurosyid

<p class="AbstractEnglish"><strong>Abstra</strong><strong>ct</strong><strong>:</strong><strong> </strong>Preparation of Barium Titanate thin film (BaTiO3) has been done on Quartz substrate using sol gel method with spin coating technique. A thin film BaTiO3 wase made with a mole variation of 0.4 mol and 0.8 mol at a rotation speed of 3000 rpm. The samples were annealed at 400 ° C with 30 minutes stand-up time and at 900 ° C with 2 hours stand-up time and a heating rate of 5 ° C per minute. Characterization of optical properties samples was performed using UV-Vis spectrometers and characterization of microstructure samples using X-Ray Diffraction (XRD). The particle size was calculated by Scherer's formula. Based on the results of the analysis it was found that mole variation of the solution influenced the absorbance value, intensity, crystality level and BaTiO3 thin film particle size. The greater mole of BaTiO<sub>3</sub> solution the higher then absorbance value. The fewer then number of layers the greater then diffraction peak intensity. More number of layers the greater the level of crystallinity and particle size.</p><p class="KeywordsEngish"> </p><p class="AbstrakIndonesia"><strong>Abstra</strong><strong>k: </strong>Pembuatan lapisan tipis Barium Titanat (BaTiO<sub>3</sub>) telah dilakukan  diatas substrat Quartz menggunakan metode sol gel dengan teknik spin coating. Lapisan tipis BaTiO<sub>3 </sub>dibuat dengan variasi mol  0.4 mol dan  0.8 mol pada kecepatan putar 3000 rpm. Sampel diannealing  pada suhu 400<sup>o</sup>C dengan waktu tahan 30 menit  dan pada suhu 900<sup>o</sup>C dengan waktu tahan 2 jam dan kenaikan suhunya 5<sup>o</sup>C per menit. Karakterisasi sifat optik sampel dilakukan  menggunakan spektrometer UV-Vis dan karakterisasi struktrur mikro sampel menggunakan X-Ray Diffraction (XRD).Ukuran partikel dihitung dengan formula Scherer. Berdasarkan hasil analisis didapat bahwa variasi mol larutan mempengaruhi  mempengaruhi nilai absorbansi, intensitas, tingkat kekristalan dan ukuran partikel lapisan tipis BaTiO<sub>3</sub>. Semakin besar mol larutan BaTiO<sub>3 </sub>maka semakin tinggi nilai absorbansinya. Semakin sedikit jumlah lapisan maka intensitas puncak difraksi semakin besar. Semakin banyak jumlah lapisan maka semakin besar pula tingkat kekristalan dan ukuran partikel<em>. </em></p>


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