Physical Properties of Nanohybrid and Microhybrid Resin Composites Subjected to an Acidic Environment: A Laboratory Study

2020 ◽  
Vol 45 (3) ◽  
pp. E105-E113
Author(s):  
M Ferooz ◽  
R Bagheri ◽  
D Jafarpour ◽  
MF Burrow
Keyword(s):  
Lactic Acid ◽  
Color Change ◽  
Pearson Correlation ◽  
Color Stability ◽  
Time Interval ◽  
Distilled Water ◽  
Resin Composites ◽  
Acidic Environment ◽  
Hardness Tester ◽  
Storage Media

SUMMARY Background: This study investigated the hardness and color stability of five resin composites subjected to different polishing methods following immersion in distilled water or lactic acid for up to three months. Methods and Materials: Three nanohybrid, Paradigm (3M ESPE), Estelite Sigma Quick (Tokuyama), Ice (SDI), and two microhybrid, Filtek P60 and Filtek Z250, composites were examined. Disc-shaped specimens (10×1.5 mm) were prepared and immersed in distilled water for 24 hours then polished using either silicon carbide paper, the Shofu polishing system or were left unpolished (control). The CIE values and microhardness were determined using a spectrophotometer and digital Vickers hardness tester, respectively (n=10) after one, 45, and 90 days of storage in distilled water or lactic acid. Data were analyzed using analysis of variance, Tukey test, and Pearson correlation coefficient. Results: Ice exhibited the greatest color change, yet Paradigm and Filtek P60 demonstrated the least. Overall, discoloration of tested materials was multifactorial and the effect of storage media depended on the material, polishing method and time interval. The greatest hardness was obtained for Paradigm and the lowest for Estelite. Hardness was found to be significantly higher in lactic acid after 45 days (p=0.014) and even higher after 90 days (p<0.001) compared with distilled water. Conclusions: An acidic environment did not adversely affect color stability or microhardness of the resin composites. There was a significantly mild reverse correlation between hardness and color change in both storage media.

scholarly journals Color change using HSB color system of dental resin composites immersed in different common Amazon region beverages

2009 ◽  
Vol 39 (4) ◽  
pp. 961-968 ◽  
Author(s):  
Débora da Costa e Silva ◽  
Sanmya Beatriz da Silva Pereira Tiradentes ◽  
Rosana Cristina Pereira Parente ◽  
Maria Fulgência Costa Lima Bandeira
Keyword(s):  
Color Change ◽  
Color Stability ◽  
Amazon Region ◽  
Composite Resins ◽  
Distilled Water ◽  
Resin Composites ◽  
Dental Resin ◽  
Color System ◽  
Initial Color

The purpose of this study is to evaluate in vitro the color stability of composite resins when exposed to beverages with high coloring contents from the Amazon region. 240 samples from four different composite brands (Natural Look, Z350, 4Seasons and Opallis) of hue A3 were fabricated using an acrylic matrix. The samples were stored in distilled water at 37ºC for 24 hours. The initial color (T0) was registered using a Canon EOS Rebel XTi 10 mp camera, and then the samples were divided into four groups (n=15): G1 (coffee), G2 (açaí juice), G3 (energetic guaraná) and G4 (control - distilled water). The samples were exposed to solutions of DES (6hs) and RE (18hs) and placed in a double boiler under constant agitation, at 37ºC for 30 days. The samples were immersed in the coloring solutions for 15 minutes daily. After 7, 15 and 30 days, new photographic registers were made (T1, T2 and T3). The images were analyzed using Corel PHOTO-PAINT 12 software to identify the colors through the HSB system. The Kruskal-Wallis and t tests (p<0.05) demonstrated significant differences in color (hue, saturation and brightness). The results revealed that none of the tested composites showed color stability when exposed to coloring solutions, and that the Amazon region beverages (açaí juice and energetic guaraná) showed to be less coloring than coffee.

scholarly journals Influence of Different Staining Beverages on Color Stability, Surface Roughness and Microhardness of Silorane and Methacrylate-based Composite Resins

2014 ◽  
Vol 15 (3) ◽  
pp. 319-325 ◽  
Author(s):  
Oguz Suleyman Özdemir ◽  
Emel Karaman ◽  
Duygu Tuncer ◽  
Esra Firat ◽  
Sevilay Karahan
Keyword(s):  
Surface Roughness ◽  
Statistical Analysis ◽  
Aluminum Oxide ◽  
Vickers Hardness ◽  
Color Change ◽  
Color Stability ◽  
Composite Resins ◽  
Distilled Water ◽  
Resin Composites ◽  
Water Control

ABSTRACT Aim To investigate the influence of different staining beverages on color stability, surface roughness and microhardness of silorane and methacrylate-based composite resins. Materials and methods Three different composite resins (Filtek Silorane, Filtek P60, Filtek Supreme XT) were tested. Thirty cylindrical specimens (10 × 2 mm) per material were prepared and polished with a series of aluminum-oxide polishing disks. Each group was then randomly subdivided into three groups according to the test beverages: distilled water (control), cola and coffee. The samples were immersed into different beverages for 15 days. Color, surface roughness and microhardness values were measured by a spectrophotometer, prophylometer and Vickers hardness device respectively, at baseline and after 15 days. The data were subjected to statistical analysis. Results Immersion in coffee resulted in a significant discoloration for all the composites tested, although the color change was lower in Filtek Silorane than that of MBCs (p < 0.05). All the composites tested showed similar surface roughness changes after immersion in different beverages (p > 0.05). Besides coffee caused more roughness change than others. Immersion in coffee caused highest microhardness change in Filtek Supreme XT (p < 0.05). Conclusion Cola and coffee altered, to some degree, the color, surface roughness and/or microhardness of the tested resin composites, depending on the characteristics of the materials. How to cite this article Karaman E, Tuncer D, Firat E, Ozdemir OS, Karahan S. Influence of Different Staining Beverages on Color Stability, Surface Roughness and Microhardness of Silorane and Methacrylate-based Composite Resins. J Contemp Dent Pract 2014;15(3):319-325.

scholarly journals Evaluation of color stability of different temporary restorative materials

2015 ◽  
Vol 44 (5) ◽  
pp. 262-267 ◽  
Author(s):  
José Vitor Quinelli Mazaro ◽  
Luiz Miguel Minani ◽  
Adriana Cristina Zavanelli ◽  
Caroline Cantieri de Mello ◽  
Cleidiel Aparecido Araújo Lemos
Keyword(s):  
Storage Time ◽  
Color Change ◽  
Artificial Saliva ◽  
Color Stability ◽  
Time Interval ◽  
Acrylic Resins ◽  
Significant Difference ◽  
Restorative Materials ◽  
Before And After ◽  
Level Of Significance

AbstractIntroductionTemporary restorative materials are widely used, however, little is know about their color stability.Objectiveto evaluate the color stability of the following temporary restorative materials: acrylic and bis-acrylic resins after immersion in pigmenting solutions for different periods of storage.Material and methodFour materials were tested (Dêncor/Clássico, Protemp 4/3M ESPE; Structur 2 SC/Voco; Luxatemp AM Plus/DMG) and 30 test specimens (15 mm in diameter and 2 mm thick) per material were fabricated. They were divided according to the storage medium (artificial saliva, saliva + cola type soda, and saliva + coffee) and storage time intervals (2, 5, 7 and 15 days). Color measurements were made before and after immersions, with use of a spectrophotometer, by means of the CIE L*a*b* system. The data were analyzed by the analysis of variance and the Tukey Test, at a level of significance of 5%.ResultAcrylic resin presented greater color stability in comparison with bis-acrylic resins (p<0.001). When bis-acrylic resins were compared no significant difference was observed between the resins Structur and Luxatemp (p=0.767). As regards solutions tested, coffee showed the highest color change values (p<0.001), and the longer the storage time interval, the greater was the color change in all the temporary restorative materials analyzed (p<0.001).ConclusionAcrylic resin presented greater color stability in comparison with bis-acrylic resins (p<0.001). Coffee caused the greatest color change, and immersion time was determinant in color stability of the temporary materials analyzed.

scholarly journals Color Stability and Gloss of Esthetic Restorative Materials after Chemical Challenges

2019 ◽  
Vol 30 (1) ◽  
pp. 52-57 ◽  
Author(s):  
Eduardo Haruki Ozera ◽  
Fernanda Miori Pascon ◽  
Américo Bortolazzo Correr ◽  
Regina Maria Puppin-Rontani ◽  
Aline Rogéria de Castilho ◽  
...  
Keyword(s):  
Color Change ◽  
Artificial Saliva ◽  
Color Stability ◽  
Initial Surface ◽  
Resin Composites ◽  
Cranberry Juice ◽  
Color Changes ◽  
Restorative Materials ◽  
Post Hoc ◽  
Acidic Beverages

Abstract This study evaluated gloss and color changes of esthetic restorative materials subjected to different acidic beverages. Specimens of resin composites (Z350XT (Z350), IPS Empress Direct (ED), Charisma Diamond (CD)) were prepared and the initial surface gloss and color (ΔE) were measured (n=10). Then, the specimens were immersed in 4 mL of each of the different beverages (cranberry juice; Coca-Cola; coffee or artificial saliva) during 15 min, 3x/day for 14 days and new gloss and color readings were obtained. Color change was evaluated with the ΔE formula and gloss change values were obtained by the formula: (final gloss - initial gloss). Data was submitted to two-way ANOVA followed by Tukey’s post hoc test (a=0.05). CD showed the lowest color change among resin composites. The highest ΔE values were obtained after immersion in coffee and cranberry juice. Coffee promoted the highest gloss change (worst gloss retention), followed by cranberry juice, Coca-cola and artificial saliva (p<0.05). The type of beverage significantly influenced the gloss of resin composites. Coca-cola reduced gloss of the three resin composites in a similar manner. Coffee affected the ED gloss more than that of Z350 and CD, while cranberry juice affected Z350 more than ED and CD. Saliva had a more pronounced effect on the gloss retention of CD than ED. The beverages used in this study influenced the optical surface properties of the composites studied.

scholarly journals The effect of a bleaching agent on the pigment removal and the bond strength of bulk-fill resin composites: an in vitro study

2018 ◽  
Vol 47 (5) ◽  
pp. 298-304
Author(s):  
Caroline de Farias CHARAMBA ◽  
Renally Bezerra Wanderley LIMA ◽  
Sônia Saeger MEIRELES ◽  
Rosângela Marques DUARTE ◽  
Ana Karina Maciel ANDRADE
Keyword(s):  
Bond Strength ◽  
Color Change ◽  
Resin Composite ◽  
Distilled Water ◽  
Filling Material ◽  
Resin Composites ◽  
Bleaching Agent ◽  
Microtensile Testing ◽  
Before And After

Abstract Introduction In order to simplify the technique, reduce the time required for direct adhesive restorations, bulk-fill resin composites have been developed be applied in bulk placement up to 4 mm increments. Objective Evaluating the color change (ΔE) and the microtensile bond strength (μTBS) of bulk fill resin composites (BFRC) to dentin after the immersion in regular beverages and the application of bleaching systems. Method Forty-five human molar teeth were randomly distributed in three groups according to the filling material (n=15): Filtek Bulk Fill, Tetric N Ceram Bulk Fill and Filtek Z100. The restored teeth were immersed in coffee, wine and distilled water (n=5) for 72 hours. The color parameters were measured using a spectrophotometer, having as basis the CIE L*a*b*, before and after tooth staining and application of bleaching processes. Subsequently, the teeth were sectioned to obtain the specimens for the microtensile testing. The ΔE values were analyzed applying the Kruskal-Wallis and the Wilcoxon tests, and the μTBS values were analyzed applying the ANOVA and the Bonferroni tests (p<0.05). Result There were no significant differences in the ∆E values when comparing the BFRCs to the conventional resin composite (CRC) in most of the experimental groups. The ∆E values did not present significant differences before and after the application of bleaching processes for all the tested resin composites. The BFRCs presented higher μTBS values than the CRC after exposure to distilled water, wine and bleaching agent. Conclusion The studied BFRCs presented similar color stability to the CRC. The BFRCs presented higher bond strength to the dentin than the CTC in most of the evaluated conditions. The bleaching agent was not effective in whitening the stained restored teeth.

Effect of Tooth-Whitening Procedures on Stained Composite Resins

2019 ◽  
Vol 44 (1) ◽  
pp. 65-75 ◽  
Author(s):  
JW Reinhardt ◽  
MM Balbierz ◽  
CM Schultz ◽  
B Simetich ◽  
MW Beatty
Keyword(s):  
Red Wine ◽  
Composite Resin ◽  
Color Change ◽  
Composite Resins ◽  
The Other ◽  
Time Interval ◽  
Distilled Water ◽  
Water Control ◽  
Tooth Whitening ◽  
Final Composite

SUMMARY In this laboratory study, a composite resin was stained to a visibly discernible level using both coffee and red wine over 14 days (change was considered clinically noticeable and significant when ΔEab*≥2.7). Color change was measured at one, three, seven, and 14 days of staining. Although the nature of color change was different for the two staining solutions, the overall degree of staining (ΔEab*) rendered by either coffee or wine at each time interval was not significantly different (p≥0.05). Four whitening protocols were applied to stained composites. Treatment included applications of distilled water (control), Crest Pro-Health [HD] toothpaste, Crest Whitestrips, Opalescence PF bleach (15%), and application of a fine pumice polishing (Preppies). HD toothpaste and Whitestrips were applied daily for 21 days, Opalescence was applied daily for 10 days, and polishing was applied once. Each of the whitening products, applied in a manner simulating at-home or in-office treatment, was effective in producing color improvements (lightening) over controls (p&lt;0.05), but none of the four treatments produced lightening that was significantly different from the other treatments (p≥0.05). A comparison of final composite color with that measured at baseline showed that Opalescence returned composite color to an acceptable level following exposure to both staining solutions (ΔEab*&lt;2.7), Whitestrips returned color close to baseline for wine-stained composites, and HD paste and polishing permitted residual stain to remain (ΔEab*≥2.7).

scholarly journals Effect of Brushing Time and Dentifrice Abrasiveness on Color Change and Surface Roughness of Resin Composites

2015 ◽  
Vol 26 (5) ◽  
pp. 507-513 ◽  
Author(s):  
Lourenço de Moraes Rego Roselino ◽  
Michelle Alexandra Chinelatti ◽  
Carla Cecilia Alandia-Román ◽  
Fernanda de Carvalho Panzeri Pires-de-Souza
Keyword(s):  
Surface Roughness ◽  
Healthy Individual ◽  
Repeated Measures ◽  
Color Change ◽  
Resin Composite ◽  
Color Stability ◽  
Resin Composites ◽  
Repeated Measures Anova ◽  
Bonferroni Test ◽  
Initial Color

Abstract: Dentifrice abrasiveness and brushing time may increase color change (∆E) and surface roughness (∆Ra) of resin composites. This study aimed to evaluate the effect of mechanical brushing time of dentifrices with different abrasiveness on ∆E and ∆Ra of nanofilled (Z350, 3M ESPE) and nanohybrid (Tetric N-Ceram, Ivoclar Vivadent) resin composites. Sixteen specimens (12 mm diameter x 2 mm thick) were fabricated using a white Teflon matrix of each resin composite and a ceramic (IPS e.max Ceram, Ivoclar Vivadent), used as control. After initial color readouts on white backgrounds (Spectrophotometer PCB 6807, Byk Gardner), with D65 standard illuminant, and surface roughness (Rugosimeter Surfcorder SE 1700, Kosalab) with cut-off=0.8 mm and speed=0.25 mm/s, specimens were assigned (n=8) according to the abrasiveness of the dentifrices: RDA* 68 (Colgate) and RDA* 180 (Colgate Total Plus Whitening). Specimens were submitted to mechanical brushing (58,400 cycles) and after every 14,600 cycles (1 year of brushing by a healthy individual), new color and surface roughness readouts were taken. Color stability was calculated by CIEDE2000. Data were analyzed by 3-way repeated measures ANOVA and Bonferroni test (p<0.05), and demonstrated that the dentifrice abrasiveness (p=0.02) and brushing time (p<0.0001) affected the ∆E of nanofilled resin composite. There was no difference on surface roughness of materials (p=0.6752) or brushing time (p=0.7997). In conclusion, the longer the brushing time and dentifrice abrasiveness, the greater the color change of the nanofilled resin composite. The surface roughness was not influenced by dentifrice abrasiveness.

scholarly journals Effect of Staining Solutions on the Color Stability of Conventional and Bulk Fill Nanohybrid Resin Composites: A Spectrophotometric Analysis

2017 ◽  
Vol 2 (1) ◽  
pp. 1-5 ◽  
Author(s):  
Jayaprakash Thumu ◽  
Anirudh Kadiyala ◽  
Indira Priyadarshini Bollu ◽  
Srinidhi Vishnu Ballullaya ◽  
Srihari Devalla
Keyword(s):  
Color Change ◽  
Color Stability ◽  
Spectrophotometric Analysis ◽  
Resin Composites ◽  
Water Control ◽  
Group Iii ◽  
Color Changes ◽  
Group I ◽  
Immersion Period ◽  
Friedman's Test

ABSTRACT Aim This study is aimed to evaluate the effect of staining solutions on the color stability of bulk fill and conventional nanohybrid resin composites (RCs) when subjected to various immersion periods. Materials and methods A total of 120 cylindrical Teflon molds (4 × 4 mm) were obtained and divided into four groups of 30 each. Molds of groups I and II were filled with Tetric N Ceram Bulk Fill (Ivoclar Vivadent, Schaan, Liechtenstein) and Filtek Bulk Fill (3M ESPE, St. Paul, MN, USA). Molds of groups III and IV were filled with Tetric N Ceram (Ivoclar Vivadent) and Filtek Z250 XTE (3M ESPE) incremental fill RC. Photo-activation was performed and specimens were incubated. Spectrophotometer analysis was done according to Commission Internationale d'Eclairage Lab color scale. After taking the baseline measurements, 10 samples from each group were immersed in distilled water (control, subgroup a), tea (subgroup b), and coffee (subgroup c) respectively, for 1, 7, and 30 days. The color values of each specimen were remeasured and color change value (E*ab) was calculated after 1, 7, and 30 days. Data were analyzed by Friedman's test and Mann–Whitney U-test; p < 0.05 is considered to be statistically significant. Results Group III specimens showed perceptible color changes at 30-day immersion period in coffee and tea. In group I specimens, color changes were perceptible at 7- and 30-day immersion periods in coffee and only 30-day immersion period in tea. Groups II and IV specimens showed perceptible color changes after all immersion periods in coffee and after 30 days in tea. Conclusion It can be concluded that Tetric N Ceram has less color change than the other nanohybrid RCs investigated when immersed in coffee and tea after various immersion periods. How to cite this article Thumu J, Kadiyala A, Bollu IP, Ballullaya SV, Devalla S. Effect of Staining Solutions on the Color Stability of Conventional and Bulk Fill Nanohybrid Resin Composites: A Spectrophotometric Analysis. J Oper Dent Endod 2017;2(1):1-5.

scholarly journals In Vitro Evaluation of Physical and Mechanical Properties of Light-Curing Resin Cement: A Comparative Study

2020 ◽  
Vol 14 (01) ◽  
pp. 152-156
Author(s):  
Luís Felipe Espíndola-Castro ◽  
Oscar Felipe Fonseca de Brito ◽  
Larissa Gabrielle Assis Araújo ◽  
Izabella Luiza Aragão Santos ◽  
Gabriela Queiroz De Melo Monteiro
Keyword(s):  
Color Change ◽  
Surface Hardness ◽  
Color Stability ◽  
Resin Cement ◽  
The Other ◽  
Distilled Water ◽  
Water Control ◽  
Mean Values ◽  
Significance Level

Abstract Objective The aim of study was to evaluate in vitro the surface hardness, sorption, solubility, and color stability of three light-cured resin cements, namely RelyX Veneer (RLX), Variolink Veneer (VLK), and All Cem Veneer (ACV). Materials and Methods Cylindrical samples (15 × 1 mm) were made for each group using a metallic mold (n = 10). Vickers microhardness test was performed, and average hardness was calculated from three indentations (300 gf/15s) per sample. The sorption and solubility of the materials were evaluated according to ISO 4049:2009 based on three samples weighing: initial (m 1), after immersion in distilled water for 7 days (m 2), and final (after removal of all moisture [m 3]). The color change was observed using a digital spectrophotometer, at three different time points, baseline, 1 day, and 1 week of immersion in coffee and distilled water (control). Statistical Analysis Shapiro–Wilk test was used to analyze the normality of the data, and groups were compared using Kruskal–Wallis and Mann–Whitney tests. A significance level of 5% was used. Results RLX showed the highest microhardness mean values (36.96 VHN), but higher sorption (23.2 µg/mm3) and solubility (2.40 µg/mm3), with statistically significant differences with the other groups. For color stability, higher ∆E was observed for the samples immersed in coffee (p = 0.009). The VLK resin cement presented statistically significant differences from the other groups, with higher color changes in coffee at 1 day (15.14) and after 1 week (23.65). Conclusion RLX resin cement showed better hardness results. All materials tested performed satisfactorily for sorption and solubility according to ISO 4049:2009. All materials showed high-staining values after 1 week of immersion in coffee.

scholarly journals Color Stability of the Bulk-Fill Composite Resins with Different Thickness in Response to Coffee/Water Immersion

2016 ◽  
Vol 2016 ◽  
pp. 1-5 ◽  
Author(s):  
Sayna Shamszadeh ◽  
Seyedeh Mahsa Sheikh-Al-Eslamian ◽  
Elham Hasani ◽  
Ahmad Najafi Abrandabadi ◽  
Narges Panahandeh
Keyword(s):  
Composite Resin ◽  
Color Change ◽  
Imaging System ◽  
Water Immersion ◽  
Color Space ◽  
Color Stability ◽  
Composite Resins ◽  
Distilled Water ◽  
Color Changes ◽  
Post Hoc

We aimed to evaluate the color stability of bulk-fill and conventional composite resin with respect to thickness and storage media. Twenty specimens of a conventional composite resin (6 mm diameter and 2 mm thick) and 40 specimens of the bulk-fill Tetric EvoCeram composite resin at two different thicknesses (6 mm diameter and 2 mm thick or 4 mm thick,n=20) were prepared. The specimens were stored in distilled water during the study period (28 d). Half of the specimens were remained in distilled water and the other half were immersed in coffee solution 20 min/d and kept in distilled water between the cycles. Color changes (ΔE) were measured using the CIEL⁎a⁎b⁎color space and a digital imaging system at 1, 7, 14, and 28 days of storage. Data were analyzed using Two-way ANOVA and Tukey’s HSD post hoc test (P<0.05). Composite resins showed significant increase in color changes by time (bulk-fill > conventional;P<0.001). Coffee exhibited significantly more staining susceptibility than that of distilled water (P<0.001). There was greater color changes with increasing the increment thickness, which was significant at 14 (P<0.001) and 28 d (P<0.01). Color change of bulk-fill composite resin was greater than that of the conventional one after coffee staining and is also a function of increment thicknesses.

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