Effect of Time and Temperature of Air Jet on the Mechanical and Biological Behavior of a Universal Adhesive System

2021 ◽  
Author(s):  
R Zimmer ◽  
ML Leite ◽  
CA de Souza Costa ◽  
J Hebling ◽  
G Anovazzi ◽  
...  
Keyword(s):  
Bond Strength ◽  
Morphological Changes ◽  
Adhesive System ◽  
Biological Behavior ◽  
Control Group ◽  
Cytotoxicity Test ◽  
Single Bond ◽  
Microtensile Bond Strength ◽  
Universal Adhesive ◽  
Air Jet

SUMMARY Objectives: To evaluate the influence of heat application on the degree of conversion (DC) of the 3M Single Bond Universal Adhesive System, as well as its transdentinal cytotoxicity and microtensile bond strength to dentin. Methods: Experimental groups were established according to the time and temperature of the air jet: G1: 5 seconds–25°C; G2: 10 seconds–25°C; G3: 20 seconds–25°C; G4: 5 seconds–50°C; G5: 10 seconds–50°C; G6: 20 seconds–50°C. In control group (G7), no treatment was performed. The DC was assessed using the Fourier transform infrared spectroscopy–attenuated total reflectance (FTIR–ATR) technique. For the transdentinal cytotoxicity test, dentin discs fitted in artificial pulp chambers (APC) received the application of the adhesive system and the air jets. For the microtensile bond strength, healthy molars were restored and submitted to the microtensile test after 24 hours and 6 months, respectively. Results: Significant reduction in viability of Mouse Dental Papilla Cell-23 (MDPC-23), which exhibited morphological changes, was observed in all experimental groups compared to control (p<0.05). Although all tested protocols resulted in transdentinal diffusion of 2-hydroxyethyl methacrylate (HEMA), the group G6 presented the highest degree of monomeric conversion and the lowest cytotoxic effect, with higher dentin bond strength values in comparison to group G1 (p<0.05). Conclusions: Applying an air blast at 50°C for 20 seconds increases the DC and microtensile bond strength of the 3M Single Bond Universal Adhesive System to dentin, as well as reduces the transdentinal cytotoxicity of the material to pulp cells.

scholarly journals Microtensile bond strength of a universal adhesive to deep dentin

2016 ◽  
Vol 19 (2) ◽  
pp. 104
Author(s):  
Cristina Gre ◽  
MAuro Amaral Caldeira de Andrada ◽  
Sylvio Monteiro Junior
Keyword(s):  
Bond Strength ◽  
Water Storage ◽  
Adhesive System ◽  
Single Bond ◽  
Third Molars ◽  
Microtensile Bond Strength ◽  
Universal Adhesive ◽  
The Mean ◽  
Self Etch ◽  
One Way Anova

<p><strong>Objective</strong>: This study evaluated the microtensile bond strength of a universal adhesive system applied to deep dentin under different bonding strategies. <strong>Material</strong> <strong>and Methods</strong>: Fifteen human third molars had the coronal portion removed exposing deep dentin and were assigned into 3 groups according to the adhesive system: G1(control): 2-steps totaletch (Adper Single Bond 2, 3M ESPE); G2: 1-step self-etch universal adhesive (Scotchbond Universal, 3M ESPE); G3:2 steps total-etch universal adhesive (Scotchbond Universal, 3M ESPE). Composite buildups were performed on the dentin surfaces and after water storage for 24 h, teeth were sectioned to obtain 40 bonded beams per group with sectional area of 0.9 mm2 . The specimens were submitted to the microtensile bond strength (µTBS) test until failure. Statistical analyses were computed using one-way ANOVA (p = 0.05). <strong>Results</strong>: The mean µTBS (in MPa) were G1 = 22.27, G2 = 22.85 and G3 = 20.3. After statistical analysis, no significant differences were observed among the groups. <strong>Conclusions</strong>: Universal adhesive system performed similarly to the total-etch adhesive and was not affected by the adhesion strategy.</p><p> </p><p><strong>KEYWORDS </strong></p><p>Microtensile; Adhesive system; Dentin.</p>

Microtensile bond strength of universal adhesive system to deep dentin

2014 ◽  
Vol 30 ◽  
pp. e144
Author(s):  
C.P. Gré ◽  
M.A.C. Andrada ◽  
S. Monteiro Júnior ◽  
D.P. Lise ◽  
C. Deucher ◽  
...  
Keyword(s):  
Bond Strength ◽  
Adhesive System ◽  
Microtensile Bond Strength ◽  
Universal Adhesive

scholarly journals The effects of different surface contaminators on the shear bond strength of a universal adhesive system to dentin: an experimental study

2021 ◽  
Vol 15 (2) ◽  
pp. 82-86
Author(s):  
Mahmoud Bahari ◽  
Siavash Savadi Oskoee ◽  
Mohammad Esmaeel Ebrahimi Chaharom ◽  
Nasim Molayi
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Adhesive System ◽  
Aluminium Chloride ◽  
Control Group ◽  
Universal Adhesive ◽  
Human Teeth ◽  
Etch And Rinse ◽  
Self Etch ◽  
Composite Samples

Background. Contamination of dentin surface is one of the common problems in restorative dentistry. The aim was to investigate the effects of different surface contaminators on the dentin shear bond strength (SBS) of universal adhesive system (UAS) applied in etch-and-rinse (ER) and self-etch (SE) strategies. Methods. One hundred forty-four maxillary anterior sound human teeth were divided into six groups based on the types of surface contaminators: no surface contaminator (control) and experimental groups contaminated with blood, saliva, aluminium chloride (ALC), ferric sulphate (FS), and caries disclosing agent (CDA). Then, each group was further subdivided into two, based on the application strategy of UAS (ER and SE). After applying the adhesive according to the manufacturer’s instructions, and bonding cylindrical composite samples, the SBS was measured. The data were analysed using two-way ANOVA, Tukey’s HSD test and t test (P<0.05). Results. The SBS in all contaminated groups, except for CDA, was significantly lower in both ER and SE strategies compared to control group (P<0.05). A comparison between the application strategies revealed that ER and SE were only significantly different in the FS contaminated group (P<0.05). Conclusion. All tested contaminators, except CDA, significantly decreased SBS of UAS in both ER and SE strategies.

scholarly journals CHX Stabilizes the Resin/demineralized Dentin Interface

2021 ◽  
Vol 32 (4) ◽  
pp. 106-115
Author(s):  
Ana Rosa Costa ◽  
Lucas Zago Naves ◽  
Franklin Garcia-Godoy ◽  
Fernanda Midori Tsuzuki ◽  
Américo Bortolazzo Correr ◽  
...  
Keyword(s):  
Bond Strength ◽  
Storage Time ◽  
Adhesive System ◽  
Control Group ◽  
Treatment Control ◽  
Microtensile Bond Strength ◽  
Pre Treatment ◽  
Acid Gel ◽  
Treatment Application ◽  
Plot Design

Abstract The aim of this study was to evaluate the effect of 2% chlorhexidine digluconate (CHX) on microtensile bond strength (µTBS) between an adhesive system and under 3 dentin conditions. For that, this study evaluated the adhesive interface at initial, after 6 months and 1 year of storage. Forty-eight human third molars were prepared and randomly divided into 3 groups, according to dentin substrates: sound dentin (Sd), caries-infected dentin (Ci) and caries-affected dentin (Ca). The groups were subdivided into two according to the dentin pre-treatment: application of 2% CHX or without pre-treatment (control). The dentin surfaces were etched with 35% phosphoric acid gel and bonded with Adper Single Bond 2 (3M ESPE) adhesive system according to manufacturer’s instructions. Subsequently, the specimens were stored in deionized water at 37°C for 24h, 6 months and 1 year. Two additional teeth were used to analyze the bonding interfaces by SEM. Data was submitted to three-way ANOVA in a split plot design and Tukey’s test (α = 0.05). The results showed that Ci decreased µTBS values when compared to Ca and Sd, regardless storages time or treatment. Stored samples for 6 months and 1 year decreased the µTBS for the control group, but no difference was found between storages time for the CHX group. As a conclusion, the 2% CHX application after etching showed improved dentin bond strength in the storage time, regardless of the substrates evaluated.

The Effect of Etching Time to Durability of Dentin Adhesives

2007 ◽  
Vol 361-363 ◽  
pp. 869-872
Author(s):  
J.R. Kim ◽  
M.R. Jung ◽  
Sang Jin Park ◽  
K.K. Choi
Keyword(s):  
Bond Strength ◽  
Etching Time ◽  
Control Group ◽  
Single Bond ◽  
Microtensile Bond Strength ◽  
Dentin Adhesives ◽  
Significant Difference ◽  
One Step ◽  
Bonding Systems ◽  
Total Etching

The purpose of this study was to evaluate the effect of different etching times on microtensile bond strength(μTBS) to dentin both initial and after thermocycling with 3 different types of total-etching adhesives. Fifty four teeth were divided into 18 groups according to 3 etching times(5, 15, 25sec), 3 types of adhesives(Scotchbond Multipurpose(SM), Single Bond(SB), One-Step(OS)), and thermocycling(0, 2,000cycles). Following the bonding procedure, the specimens were bonded using Z250 composite. Half of them were not thermocycled (control group) and the others were subjected to 2,000 thermocycle (experimental group) and processed for microtensile bond strength testing. The microtensile bond strength(MPa) by different etching time(5, 15, 25s) was 37.7±9.1, 34.3±10.9 and 30.5±7.5 using Scotchbond Multipurpose(SM), 34.6±10.1, 33.8±7.6, 35.3±9.9 using single bond(SB) and 34.3±7.6, 31.3±8.5, 35.8±11.0 using one step(OS). After 2000 thermocycling the specimens, the microtensile bond strength(MPa) was decreased for all dentin bonding systems tested. But when specimens were bonded with OS, there is no significant difference between microtensile bond strength of the groups with the different etching times(5, 15, 25s) (28.2±7.8a , 29.1±8.6a and 28.2±9.4a). And the microtensile bond strength of the groups using SM, SB was decreased significantly when the etchant was applied for 25 sec(p<0.05). After all, the adhesive durability for dentin could be affected by type of solvents in adhesive and etching time. Especially, extended etching time may deteriorate dentin bond strength when ethanol-based adhesive was used

scholarly journals Effect of Metalloproteinase Inhibitors on the Microtensile Bond Strength of Composite Resin to Er:YAG Laser-Irradiated Dentin

2016 ◽  
Vol 27 (4) ◽  
pp. 442-445 ◽  
Author(s):  
Beatriz Carlos Correa ◽  
Rodrigo Galo ◽  
Camila Scatena ◽  
Maria Cristina Borsatto ◽  
Aloísio Oro Spazzin ◽  
...  
Keyword(s):  
Bond Strength ◽  
Composite Resin ◽  
Er:Yag Laser ◽  
Testing Machine ◽  
Adhesive System ◽  
Fracture Pattern ◽  
Chemical Degradation ◽  
Control Group ◽  
Microtensile Bond Strength ◽  
Cross Sectional

Abstract This study evaluated the effect of matrix metalloproteinase (MMP) inhibitors - 2% (CHX) and sodium fluoride (NaF) (5000 ppm) - on microtensile bond strength (μTBS) of composite resin to Er:YAG laser-irradiated dentin after chemical degradation of the bond interface. The occlusal surface of forty sound human molars was removed exposing the dentin surface (n=10), which was polished, irradiated with Er:YAG laser, acid etched and dried. Twenty specimens were rewetted with 2% CHX (control group) and 20 were rewetted with NaF (5000 ppm). The adhesive system was applied and a 4-mm-high plateau of light-cured composite resin was built up. Resin-dentin sticks were obtained with a rectangular cross-sectional area (0.8-1 mm2) and were either stored in water at 37 ?#61616;C for 24 h or submitted to chemical degradation. For chemical degradation, they were immersed in 10% NaOCl aqueous solution for 5 h and rinsed in water for 1 h. The sticks were submitted to microtensile test in a mechanical testing machine at 0.5 mm/min until failure. Fracture pattern was analyzed using SEM. μTBS values were calculated in MPa and submitted to analysis of variance ANOVA (α=0.05). The variance analysis showed that the 'MMP inhibitor' and 'degradation' factors (p=0.214 and p=0.093, respectively) and interaction between the factors were not statistically significant (p=0.143). Mixed failure predominated in all groups. In conclusion, the 2% CHX and NaF 5000 ppm presented similar μTBS of composite resin to laser-irradiated dentin before and after chemical degradation

Does Bonding Approach Influence the Bond Strength of Universal Adhesive to Dentin of Primary Teeth?

2017 ◽  
Vol 41 (3) ◽  
pp. 214-218 ◽  
Author(s):  
Tathiane Larissa Lenzi ◽  
Fabio Zovico Maxnuck Soares ◽  
Rachel de Oliveira Rocha
Keyword(s):  
Bond Strength ◽  
Adhesive System ◽  
Primary Tooth ◽  
Adhesive Systems ◽  
Microtensile Bond Strength ◽  
Universal Adhesive ◽  
Etch And Rinse ◽  
Tooth Dentin ◽  
Self Etch ◽  
One Way Anova

Objective: To evaluate the effect of bonding strategy on microtensile bond strength (μTBS) of a new universal adhesive system to primary tooth dentin. Study design: Flat dentin surfaces from 25 primary molars were assigned to 5 groups according to the adhesive and bonding approach: Adper Single Bond 2 (two-step etch-and-rinse adhesive) and Clearfil SE Bond (two-step self-etch system), as controls; Scotchbond Universal Adhesive–self-etch, dry or wet-bonding etch-and-rinse strategies. Composite buildups were constructed and the teeth were sectioned to obtain bonded sticks (0.8 mm2) to be tested under tension at 1mm/min. The μTBS means were analyzed by one-way ANOVA and Tukey's tests (α = 0.05). Failure mode was evaluated using a stereomicroscope (400×). Results: Universal adhesive applied following both dry and wet-bonding etch-and-rinse strategies showed similar bond strength compared with control adhesive systems. Self-etch approach resulted in the lowest μTBS values. For all groups, adhesive/mixed failure prevailed. The percentage of premature debonded specimens was higher when the universal adhesive was used as self-etch mode. Conclusion: The universal adhesive does not share the same versatility of being used in the etch-and-rinse and self-etch approaches; however, the use of the new adhesive following either wet or dry-bonding may be a suitable option as alternative to two-step etch-and-rinse adhesive protocol.

scholarly journals Bond strength of orthodontic brackets to polymethylmethacrylate: effect of the surface treatment and adhesive system

2021 ◽  
Vol 62 (1) ◽  
Author(s):  
Rita Cardoso ◽  
◽  
Joana Godinho ◽  
Luís Jardim ◽  
◽  
...  
Keyword(s):  
Bond Strength ◽  
Aluminum Oxide ◽  
Surface Treatment ◽  
Failure Mode ◽  
Shear Bond Strength ◽  
Adhesive System ◽  
Orthodontic Brackets ◽  
Control Group ◽  
Universal Adhesive ◽  
Machine Failure

Objectives: To evaluate the influence of the surface treatment and adhesive system on the shear bond strength and the failure mode of orthodontic brackets bonded to polymethylmethacrylate surfaces. Methods: Ninety metal brackets (n=15) were bonded to aged discs of polymethylmethacrylate SR Ivocron subjected to three surface conditions (no treatment; sandblasting with 50-μm aluminum oxide; roughening with a tungsten bur), using two combinations of adhesives (methylmethacrylate monomer + Transbond XT Primer; Scotchbond Universal Adhesive) followed by the composite Transbond XT. In the control group, metal brackets were bonded with Transbond XT to 15 human mandibular incisors. The specimens were thermocycled, stored in distilled water (37ºC, 7 days), and tested in shear, using an Instron universal machine. Failure mode was classified according to the adhesive remnant index using a stereomicroscope. The data were analyzed with an analysis of variance and posthoc tests (p<0.05). Results: Significant differences were found between the bracket bond strength to polymethylmethacrylate with different surface treatments (p<0.001). Sandblasting with aluminum oxide was superior to tungsten bur roughening. The adhesive system did not significantly influence the shear bond strength nor the failure mode (p=0.8415). All experimental groups showed lower bond strengths than the control group (p=0.1566). Conclusions: Mechanical surface treatment significantly influenced the bracket’s bond strength to polymethylmethacrylate. Sandblasting with aluminum oxide was the most effective mechanical treatment. The weakest adhesive link was found at the acrylic-adhesive interface. Orthodontic bonding to polymethylmethacrylate was weaker than bonding to enamel, regardless of the surface treatment and the adhesive used.

scholarly journals Bond strength of universal adhesive applied to dry and wet dentin

2020 ◽  
Vol 19 ◽  
pp. e201662
Author(s):  
Maria Luísa de Alencar e Silva Leite ◽  
Caroline de Farias Charamba ◽  
Renally Bezerra Wanderley e Lima ◽  
Sônia Saeger Meireles ◽  
Rosângela Marques Duarte ◽  
...  
Keyword(s):  
Bond Strength ◽  
Storage Time ◽  
Resin Composite ◽  
Adhesive System ◽  
Microtensile Bond Strength ◽  
Universal Adhesive ◽  
Bonding Quality ◽  
Etch And Rinse ◽  
Significant Difference ◽  
One Year

Aim: This study evaluated the influence of dentin wettability on the immediate and extended microtensile bond strength (mTBS) of a universal adhesive system used in the etch-and-rinse strategy. Methods: Twenty human third molars were selected and divided into four groups according to the adhesive system and dentin wettability. The mTBS values of each group were registered 24 h and one year after adhesive system application and resin composite block build-up (n=30). Data were analyzed by the t-test (p<0.05). Results: When both adhesive systems were compared, there was no statistically significant difference when they were applied following wet bonding (p>0.05). However, the dry bonding reduced μTBS values of the Adper Single Bond 2 adhesive (p<0.05). Regarding storage time, both groups presented similar μTBS values at 24 h and one year (p>0.05). Conclusions: Therefore, the Scotchbond Universal Adhesive can be applied to dry or wet dentin without compromising the etch-and-rinse bonding quality and the durability of the restorations.

scholarly journals Evaluation of Microtensile Bond Strength of Universal Self-etch Adhesive System to Wet and Dry Dentin

2020 ◽  
Vol 8 (D) ◽  
pp. 77-81
Author(s):  
Mohamed Ahmed Wakwak ◽  
Eslam Hassan Gabr ◽  
Ahmed Mohamed Elmarakby
Keyword(s):  
Bond Strength ◽  
Adhesive System ◽  
Solvent Free ◽  
Microtensile Bond Strength ◽  
Universal Adhesive ◽  
Significance Level ◽  
Significant Difference ◽  
One Step ◽  
Storage Times ◽  
Self Etch

BACKGROUND: The durability of dentin-resin interfaces with the universal adhesive system is a crucial characteristic with chemical interactions between the exposed collagen and the adhesive monomers, but it is still compromised with wet and dry mode. AIM: The present study evaluated the effect of dentin wetness and solvents containing of one-step self-etch adhesives on the microtensile bond strength (μTBS) of dentin at different storage times. METHODS: Occlusal dentin of 54 extracted human molars was exposed. Each adhesive agent was applied according to manufacturer instructions to wet and dry dentin surfaces. Composite resin was incrementally built up. Bond strengths to dentin were determined using the μTBS test after water storage for 24 h, 1 month, and 6 months. One-way ANOVA was used to compare between more than two non-related samples. The significance level was set at p ≤ 0.05. RESULTS: Dryness of dentin increases the μTBS with solvent-containing adhesives while decrease the μTBS with solvent-free adhesive. There was an increase in microtensile bond strength values in the case of ethanol water-based self-etch adhesive over time. No statistically significant difference was found among different storage times regarding μTBS for solvent-free adhesive, while a statistically significant difference was found among different storage times in μTBS for solvent-containing adhesives. CONCLUSION: Universal adhesive systems improve the durability and stability of dentin bond strength.

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