scholarly journals Quality control of substances by electromagnetic sensing in a waveguide

Relevance. The problems of remote non-destructive determination and control of quality indicators of a wide variety of material environments, in particular, household and food products, are relevant practically for all areas of the national economy, science and technology. The relevance of scientific research in the field of dielectrometry in the microwave range is also due to the needs for the development of high technologies in medicine and health care, the national economy in real time. The aim of this work is to develop the method of microwave waveguide dielectrometry based on the application of the theory of multilayer plane-layered dielectric structures to the determination of the complex dielectric constant of a substance from the values ​​of the standing wave ratio of the samples under study in a waveguide at two close frequencies. Materials and methods. The research is based on well-studied phenomena of interference of electromagnetic waves on multilayer plane-layered dielectric structures. By using a mathematical model of the phenomenon of interference of a plane electromagnetic wave on a three-layer dielectric structure, the ambiguity of determining the complex dielectric constant of a substance by the classical method of waveguide dielectrometry in the microwave range by measuring the standing wave ratio of a dielectric sample placed in the waveguide and the phase angle of the reflection coefficient is overcome. Results. A method is proposed for ensuring the unambiguity of determining the complex dielectric constant of a substance in waveguide dielectrometry on the basis of the theory of multilayer plane-layered dielectric structures. The method leads to an explicit expression for the complex reflection coefficient of an electromagnetic wave from the investigated dielectric sample placed in a rectangular waveguide. The complex dielectric constant of a substance is determined from the values ​​of the standing wave ratio at two close frequencies in the microwave range. By the found value of the dielectric constant and the tangent of the dielectric loss angle, the quality parameter of the substance is determined by comparing and optimizing two objective functions, including the arrays of reference values ​​of the complex dielectric constant obtained in the course of measurements and compiled in advance, and by comparing and optimizing the third objective function, previous functions. As an example of an indicator of the quality of a substance, the specific heat of combustion of coal was determined. Conclusions. The proposed method for determining the complex dielectric constant and quality indicators of dielectric materials in the microwave frequency range has been tested in the case of various types of coals, its efficiency has been proven and the reliability of the results has been proven. The method and the devices and software implemented on its basis are promising for non-destructive express control of dielectric materials and media.

1961 ◽  
Vol 39 (3) ◽  
pp. 526-534 ◽  
Author(s):  
B. D. Ripley ◽  
R. McIntosh

The complex dielectric constants of three compositions of trimethylpentane and nitrobenzene have been measured as a function of temperature for a range near the consolute temperature. The frequency employed was 3300 Mc/sec. The experimental procedure involved the study of the standing wave established in a coaxial line. The chemical systems showed maxima in both the real and imaginary parts of the complex dielectric constant at temperatures above those at which phase separation occurs. The finding of Semenchenko and Azimov is thus confirmed. A discussion of the validity of applying thermodynamic formulae to dielectrics showing loss is given and some qualitative remarks are offered concerning the change of the systems as they are cooled. These remarks are based upon the effect of the applied field upon the entropy of the solutions.


2020 ◽  
Vol 86 (2) ◽  
pp. 37-43
Author(s):  
A. I. Kaz’min ◽  
P. A. Fedyunin

The development of modern engineering is inextricably linked with the development of the new types of multilayer dielectric materials. Existing radio wave methods for monitoring interlayer defects in such materials exhibit low accuracy in reconstructing the geometric parameters of defects. The results of studying extended interlayer defects in the three-layer coating consisting of polymethyl methacrylate, F-4D PTFE, and semi-hard rubber by the method of surface electromagnetic waves are presented. The method is based on the solution of inverse problems in the reconstruction of the geometric parameters of extended interlayer defects of special multilayer materials and coatings from the frequency dependence of the attenuation coefficient of the field of a slow surface electromagnetic wave. Unlike the methods that make use from the complex reflection coefficient we proposed to increase the accuracy of the reconstruction of the geometric parameters of extended interlayer defects taking into account the linear frequency dependence of the attenuation coefficient as well as reducing the number of fixed measurement frequencies. Moreover, the determination procedure is rather simple, since only the field strength of the surface electromagnetic wave is measured, and there is no need for phase measurements. Experimental data obtained on a multifrequency measuring complex in the range of 10 – 11 GHz were used for reconstruction of the interlayer defects in the coating under study. The developed method provided a relative error of thickness estimation below 10%. The proposed method approach can be used in studying multilayer dielectric coatings on the metal for detection of delamination in the lack of glue or poor adhesion between the layers. The developed method is also suitable for control of the defects in semiconductors, ferrite and composite materials.


1963 ◽  
Vol 41 (10) ◽  
pp. 1679-1685 ◽  
Author(s):  
V. Muralidhara Rao

An interferometric method has been developed for the measurement of ε′ and ε″ at 8.3-mm wavelength. The values obtained by the method are compared with those obtained by the standing-wave method. The agreement is fair.


1997 ◽  
Vol 503 ◽  
Author(s):  
B. K. Diefenderfer ◽  
I. L. Al-Qadi ◽  
J. J. Yoho ◽  
S. M. Riad ◽  
A. Loulizi

ABSTRACTPortland cement concrete (PCC) structures deteriorate with age and need to be maintained or replaced. Early detection of deterioration in PCC (e.g., alkali-silica reaction, freeze/thaw damage, or chloride presence) can lead to significant reductions in maintenance costs. However, it is often too late to perform low-cost preventative maintenance by the time deterioration becomes evident. By developing techniques that would enable civil engineers to evaluate PCC structures and detect deterioration at early stages (without causing further damage), optimization of life-cycle costs of the constructed facility and minimization of disturbance to the facility users can be achieved.Nondestructive evaluation (NDE) methods are potentially one of the most useful techniques ever developed for assessing constructed facilities. They are noninvasive and can be performed rapidly. Portland cement concrete can be nondestructively evaluated by electrically characterizing its complex dielectric constant. The real part of the dielectric constant depicts the velocity of electromagnetic waves in PCC. The imaginary part, termed the “loss factor,” describes the conductivity of PCC and the attenuation of electromagnetic waves.Dielectric properties of PCC have been investigated in a laboratory setting using a parallel plate capacitor operating in the frequency range of 0.1 to 40.1MIHz. This capacitor set-up consists of two horizontal-parallel plates with an adjustable separation for insertion of a dielectric specimen (PCC). While useful in research, this approach is not practical for field implementation. A new capacitor probe has been developed which consists of two plates, located within the same horizontal plane, for placement upon the specimen to be tested. Preliminary results show that this technique is feasible and results are promising; further testing and evaluation is currently underway.


2002 ◽  
Vol 716 ◽  
Author(s):  
Alok Nandini ◽  
U. Roy ◽  
A. Mallikarjunan ◽  
A. Kumar ◽  
J. Fortin ◽  
...  

AbstractThin films of low dielectric constant (κ) materials such as Xerogel (ĸ=1.76) and SilkTM (ĸ=2.65) were implanted with argon, neon, nitrogen, carbon and helium with 2 x 1015 cm -2 and 1 x 1016 cm -2 dose at energies varying from 50 to 150 keV at room temperature. In this work we discuss the improvement of hardness as well as elasticity of low ĸ dielectric materials by ion implantation. Ultrasonic Force Microscopy (UFM) [6] and Nano indentation technique [5] have been used for qualitative and quantitative measurements respectively. The hardness increased with increasing ion energy and dose of implantation. For a given energy and dose, the hardness improvement varied with ion species. Dramatic improvement of hardness is seen for multi-dose implantation. Among all the implanted ion species (Helium, Carbon, Nitrogen, Neon and Argon), Argon implantation resulted in 5x hardness increase in Xerogel films, sacrificing only a slight increase (∼ 15%) in dielectric constant.


2015 ◽  
Vol 7 (3-4) ◽  
pp. 369-377 ◽  
Author(s):  
Alex Pacini ◽  
Alessandra Costanzo ◽  
Diego Masotti

An increasing interest is arising in developing miniaturized antennas in the microwave range. However, even when the adopted antennas dimensions are small compared with the wavelength, radiation performances have to be preserved to keep the system-operating conditions. For this purpose, magneto-dielectric materials are currently exploited as promising substrates, which allows us to reduce antenna dimensions by exploiting both relative permittivity and permeability. In this paper, we address generic antennas in resonant conditions and we develop a general theoretical approach, not based on simplified equivalent models, to establish topologies most suitable for exploiting high permeability and/or high-permittivity substrates, for miniaturization purposes. A novel definition of the region pertaining to the antenna near-field and of the associated field strength is proposed. It is then showed that radiation efficiency and bandwidth can be preserved only by a selected combinations of antenna topologies and substrate characteristics. Indeed, by the proposed independent approach, we confirm that non-dispersive magneto-dielectric materials with relative permeability greater than unit, can be efficiently adopted only by antennas that are mainly represented by equivalent magnetic sources. Conversely, if equivalent electric sources are involved, the antenna performances are significantly degraded. The theoretical results are validated by full-wave numerical simulations of reference topologies.


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