scholarly journals One-step method for obtaining potassium sulfate and processing of lye

Author(s):  
V. V. Shauchuk ◽  
Z. A. Hotto ◽  
A. S. Stromsky ◽  
A. A. Stromsky

Method of obtaining potassium sulfate with basic substance content higher 92 % shown. Process conditions: 110 % KCl (10 % excess substance from stoichiometry), mixing at temperature higher 95 °C during 30 min, mixing at temperature 0 °C for 1 hour, stirrer speed 500 rpm, sludge washing 15 % water from wet sludge weight, drying the washed sludge at 70–80 °C during 1 hour. The degree of evaporation of the solution at which the double salt of potassium and ammonium sulfate precipitated was determined. The degree is 30 % at the evaporated suspension cooled, and is 45 % at hot filtration.

2011 ◽  
Vol 117-119 ◽  
pp. 256-261 ◽  
Author(s):  
Wei Gong ◽  
Ying He ◽  
Chun Zhang ◽  
Jian Hua Zhu ◽  
Li He

The microcellular foaming PP/GF composites was made under the condition of twice-open mold by using chemical foaming injection method, according to glass fiber reinforced mechanism, the effect rule of GF on mechanics properties was studied in microcellular foam PP composites. The results showed that tensile and impact strength of Micro-foam PP/GF composites by one-step method were higher than that of micro-foam PP/GF composites by two-step method, when the content of GF is 30%, the tensile and impact strength of micro-foam PP/GF composites by one-step method can reach 55.72MPa and 7.5kJ/m2respectively,one-step method can get higher strength and higher toughness micro-foam PP/GF composites.


1993 ◽  
Vol 58 (11) ◽  
pp. 2642-2650 ◽  
Author(s):  
Zdeněk Kruliš ◽  
Ivan Fortelný ◽  
Josef Kovář

The effect of dynamic curing of PP/EPDM blends with sulfur and thiuram disulfide systems on their mechanical properties was studied. The results were interpreted using the knowledge of the formation of phase structure in the blends during their melt mixing. It was shown, that a sufficiently slow curing reaction is necessary if a high impact strength is to be obtained. Only in such case, a fine and homogeneous dispersion of elastomer can be formed, which is the necessary condition for high impact strength of the blend. Using an inhibitor of curing in the system and a one-step method of dynamic curing leads to an increase in impact strength of blends. From the comparison of shear modulus and impact strength values, it follows that, at the stiffness, the dynamically cured blends have higher impact strength than the uncured ones.


2019 ◽  
Vol 375 ◽  
pp. 122000 ◽  
Author(s):  
Yang Xuan ◽  
Xian-Lin Song ◽  
Xiao-Quan Yang ◽  
Ruo-Yun Zhang ◽  
Zi-Yu Song ◽  
...  

Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 3138
Author(s):  
Kamila Gosz ◽  
Agnieszka Tercjak ◽  
Adam Olszewski ◽  
Józef Haponiuk ◽  
Łukasz Piszczyk

The utilization of forestry waste resources in the production of polyurethane resins is a promising green alternative to the use of unsustainable resources. Liquefaction of wood-based biomass gives polyols with properties depending on the reagents used. In this article, the liquefaction of forestry wastes, including sawdust, in solvents such as glycerol and polyethylene glycol was investigated. The liquefaction process was carried out at temperatures of 120, 150, and 170 °C. The resulting bio-polyols were analyzed for process efficiency, hydroxyl number, water content, viscosity, and structural features using the Fourier transform infrared spectroscopy (FTIR). The optimum liquefaction temperature was 150 °C and the time of 6 h. Comprehensive analysis of polyol properties shows high biomass conversion and hydroxyl number in the range of 238–815 mg KOH/g. This may indicate that bio-polyols may be used as a potential substitute for petrochemical polyols. During polyurethane synthesis, materials with more than 80 wt% of bio-polyol were obtained. The materials were obtained by a one-step method by hot-pressing for 15 min at 100 °C and a pressure of 5 MPa with an NCO:OH ratio of 1:1 and 1.2:1. Dynamical-mechanical analysis (DMA) showed a high modulus of elasticity in the range of 62–839 MPa which depends on the reaction conditions.


2013 ◽  
Vol 321-324 ◽  
pp. 209-212
Author(s):  
Chun Yan Xia

nfluences on properties of the concrete highway pavement were analyzed in this paper, and the optimal formulation materials were gotten to use in the repair of used-broken cement blocks in the experiment. Polyurethane concrete material was prepared, combing the ordinary concrete technology with one-step method of the synthesis of polyurethane hard bubble, and then its mechanical properties of the relevant parameters were measured to determine the optimal preparation program. The results show that the polyurethane concrete also has sufficiently good mechanical properties while it has the characteristic of fast patching.


2002 ◽  
Vol 43 (21) ◽  
pp. 3887-3890 ◽  
Author(s):  
Michael R. Wood ◽  
June Y. Kim ◽  
Kathy M. Books

Author(s):  
JingWei Wen ◽  
XiaoCong Qiu ◽  
XiangYu Kong ◽  
XinYu Chen ◽  
Fan Yang ◽  
...  

Nanoscale ◽  
2019 ◽  
Vol 11 (6) ◽  
pp. 2871-2877 ◽  
Author(s):  
Ting Zhang ◽  
Feng Wang ◽  
Peng Zhang ◽  
Yafei Wang ◽  
Hao Chen ◽  
...  

The flexible perovskite photodetector, fabricated by a modified one-step method, showed a broadband spectrum response from blind ultraviolet to visible light, and exhibited excellent mechanical flexibility and improved environmental stability.


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