scholarly journals ANALYSIS OF HEAVY METAL SEA SEDIMENT FROM MELAWAI BEACH OF BALIKPAPAN, EAST KALIMANTAN

2018 ◽  
Author(s):  
Ismail Marzuki
Keyword(s):  
Heavy Metals ◽  
Heavy Metal ◽  
Sample Preparation ◽  
Atomic Absorption ◽  
Research Method ◽  
Atomic Absorption Spectrophotometry ◽  
Metal Concentrations ◽  
Absorption Spectrophotometry ◽  
East Kalimantan

The Research has been conducted by analysis of heavy metal sea sediments concentrations of Lead (Pb), Copper (Cu), arsenic (As) and mercury (Hg) from Melawai Beach of Balikpapan, East Kalimantan. The research Method for all sample preparation is done by dry destruction, except for Hg analysis done by wet destruction then analyzed using Atomic Absorption Spectrophotometry (AAS) with specific wavelength for each metal. Concentrations were obtained from sediment of heavy metals Pb, Cu, As and Hg: Pb (λ max: 217.0 nm): 35.7504 to 41.4850 mg/kg; Cu (λ max: 253.7 nm): 16.0713 to 30.2314 mg/kg; As metal (λ max: 109.7 nm), 4.1406 to 5.3359 mg/kg; and Hg (λ max: 357.3 nm) from 0.8975 to 1.1991 mg/Kg, respectively. The analysis results of this research concluded that, the Melawai Balikpapan beach polluted with heavy metals, especially Pb, Cu, As and Hg.

scholarly journals Comparative Study of Heavy Metals in Dried and Fluid Milk in Peshawar by Atomic Absorption Spectrophotometry

2014 ◽  
Vol 2014 ◽  
pp. 1-5 ◽  
Author(s):  
Ghosia Lutfullah ◽  
Abid Ali Khan ◽  
Azra Yasmeen Amjad ◽  
Sajida Perveen
Keyword(s):  
Heavy Metals ◽  
Heavy Metal ◽  
Atomic Absorption ◽  
Atomic Absorption Spectrophotometry ◽  
Cow Milk ◽  
Toxic Heavy Metals ◽  
Metal Concentrations ◽  
Heavy Metal Concentrations ◽  
Milk Samples ◽  
Absorption Spectrophotometry

Various essential and toxic heavy metals (Ca, Mg, Cu, Zn, Fe, Mn, Pb, Cd, Cr, and Ni) contents in various types of dried (infant formulaandpowdered) and fluid (freshandprocessed) cow milk were assessed by atomic absorption spectrophotometry. The milk samples were collected from local markets of different parts of Peshawar city, Pakistan. Heavy metal concentrations varied significantly depending upon the type of milk. The heavy metal concentrations in most of the samples were within normal and permissible ranges. It was observed that the samples contained considerable amounts of calcium, while magnesium levels were well above the required levels. The results also revealed that copper levels were slightly lower than the permissible limits. The concentration of zinc in dried milk samples was greater than the values for the liquid milk types. Infant milk formulae had higher iron levels as compared to other milk samples because of the added constituents. Significant differences were observed in the mean values of manganese and cadmium in different types of milk. The toxic metals were within the acceptable limits and did not show significant levels leading to toxicity.

scholarly journals Kandungan Logam Berat Besi (Fe) Pada Air, Sedimen, Dan Kerang Hijau (Perna viridis) Di Perairan Tanjung Emas Semarang

2015 ◽  
Vol 18 (1) ◽  
Author(s):  
Endang Supriyantini ◽  
Hadi Endrawati
Keyword(s):  
Heavy Metals ◽  
Heavy Metal ◽  
Flow Velocity ◽  
Atomic Absorption ◽  
Key Words ◽  
Atomic Absorption Spectrophotometry ◽  
Pollution Level ◽  
Perna Viridis ◽  
Absorption Spectrophotometry ◽  
Living Organisms

Logam berat Fe merupakan logam berat essensial yang keberadaannya dalam jumlah tertentu sangat dibutuhkan oleh organisme hidup, namun dalam jumlah yang berlebih dapat menimbulkan efek racun.Penelitian ini bertujuan untuk menganalisis kandungan dan tingkat pencemaran logam berat Fe pada air, sedimen, dan kerang hijau (Perna viridis) di perairan Tanjung Emas Semarang. Penelitian ini dilaksanakan pada tanggal 7 November dan 7 Desember 2013 dengan metode penelitian deskriptif. Logam berat Fe dalam sampel air, sedimen dan kerang hijau dianalisis di Laboratorium Balai Besar Teknologi Pencegahan Pencemaran Industri (BTPPI) Semarang dengan menggunakan metode AAS (AtomicAbsorption Spectrophotometry). Hasil penelitian menunjukkan bahwa perairan Tanjung Emas masih dalam taraf terkontaminasi logam Fe. Sedangkan pada sedimen dan pada kerang hijau (Perna viridis) sudah terindikasi tercemar logam Fe.Meskipun demikian variasi faktor lingkungan seperti suhu, salinitas, pH, kecepatan arus dan jenis sedimen juga memberikan kontribusi yang cukup penting terhadap kandungan logam Fe.Kata Kunci: logam Fe, Air, Sedimen, Perna viridis, metode AAS Heavy metalsiron(Fe) is anessentialheavy metalswhose presencein a certain amountis neededby living organisms, but inexcessiveamountscan causetoxic effects.The aims of the research is to analyze the heavy metals coccentration and the pollution level of Fe in water, sediment, and green mussels (Perna viridis) at Tanjung Emas Semarang. This research was conducted from 7 November and 7 December 2013 using the Atomic Absorption Spectrophotometry (AAS) and research methodswithdescriptive. The results showed that the waters of the Tanjung Emas is still in the stage of heavy metals contaminated iron (Fe). Sediment and green mussels (Perna viridis)already indicated heavy metal contaminatediron. However, variations inenvironmental factorssuch astemperature, salinity, pH, flow velocity an dsediment types also providean important contributionto heavy metal contentof iron(Fe).Key Words: Fe, water, sediment, Perna viridis, metode AAS

scholarly journals Heavy Metal Concentration in Eight Fish Species from Epe Lagoon (Nigeria)

2019 ◽  
Vol 21 (1) ◽  
pp. 69-82
Author(s):  
Iyabode Olusola Taiwo ◽  
Olaniyi Alaba Olopade ◽  
Nathanael Akinsafe Bamidele
Keyword(s):  
Heavy Metals ◽  
Heavy Metal ◽  
Atomic Absorption ◽  
Metal Concentration ◽  
Fish Species ◽  
Heavy Metal Concentration ◽  
Atomic Absorption Spectrophotometry ◽  
Human Consumption ◽  
Heavy Metal Concentrations ◽  
Absorption Spectrophotometry

Abstract This research was undertaken to find out the levels of five heavy metals (Cu, Fe, Mn, Pb, and Zn) in the muscles of eight fish species from Epe Lagoon. The levels of heavy metals were determined by atomic absorption spectrophotometry after digestion of the samples using Kjldahl heating digester. The heavy metal concentrations among the fish species were statistically dissimilar (P < 0.5). The heavy metals of Pb, Fe, and Mn were above the FAO/WHO agreeable limits for human consumption.

scholarly journals Relationship Between Metal Load (Selenium, Arsenic, Molybdenum) of Soil, Plant and Serum of Buffaloes

2020 ◽  
Vol 71 (8) ◽  
pp. 80-89
Author(s):  
Zafar Iqbal Khan ◽  
Kafeel Ahmad ◽  
Naunain Mehmood ◽  
Asia Fardous ◽  
Yongjun Yang ◽  
...  
Keyword(s):  
Heavy Metals ◽  
Heavy Metal ◽  
Atomic Absorption ◽  
Negative Correlation ◽  
Metal Contamination ◽  
Atomic Absorption Spectrophotometry ◽  
Absorption Spectrophotometry ◽  
Permissible Levels ◽  
Metal Load ◽  
Metal Quantification

Presence of hazardous minerals in three major components (soil, forage and buffalo serum) was evaluated for determining extent of metal contamination in Sargodha, Pakistan. Ten soil and forage samples for each season were taken from ten randomly selected sites. 30 grazing buffaloes of �niliravi� breed (calves, non-lactating and lactating) were also sampled randomly from these sites for collection of serum. Heavy metal quantification via atomic absorption spectrophotometry was carried out for selenium, molybdenum and arsenic. Non-significant but positive correlation was found for selenium (Se) concentrations in soil, forage and serum and molybdenum (Mo) concentrations in soil and serum. Negative correlation (p]0.05) was obtained for Mo level between forage-serum and soil-forage which was indicative of molybdenum deficiency in the soil. The results suggested that the heavy metals remained below maximum permissible levels and were non-toxic for the ruminants of the study area.

scholarly journals PROMINE

PROMINE ◽  
2017 ◽  
Vol 5 (2) ◽  
pp. 15-29
Author(s):  
Eka Sari ◽  
Dyah Sandra Fiona ◽  
Nuril Hidayati ◽  
Eddy Nurtjahya
Keyword(s):  
Heavy Metals ◽  
Heavy Metal ◽  
Atomic Absorption ◽  
Secondary Forest ◽  
Atomic Absorption Spectrophotometry ◽  
Metal Contaminants ◽  
Vegetation Analysis ◽  
Absorption Spectrophotometry ◽  
Heavy Metal Contaminants ◽  
Accumulator Plant

Besides to impact on changing of landscape and biodiversity, tin mined left heavy metal contaminants,and phytoremediation (the use of plants to accumulate heavy metals) is a chosen method. This studymeasures Pb (Lead), Cu (Copper), Zn (Zinc) in soil and dominant terestrial plants in tin mined landand Fe (Iron), Al (Aluminum), As (Arsen) in root and shoot of dominant plants in ex-tin mined pond.Dominant species was determined by vegetation analysis of quadrate method. Metals analysis wasconducted using atomic absorption spectrophotometry. Pb in secondary forest (8 ppm), in revegetatedtin mined soil (10,80 ppm) and in 0 year abandoned tin mined soil) (20,70 ppm) exceed qualitystandards. There is no potential of becoming accumulator plant for Pb, Cu, Zn in tin mined land, butSchima wallichii was found potential to be Cu accumulator in secondary forest because it hastranslocation factor (TF)>1. The highest Fe > 2% in shoot and > 3% in roots. Al > 2% in shoot and >3% in root. As was not detected.Keywords: Tin mined soil, Bangka, Metal, Accumulator plants

scholarly journals Analisa Kadar Timbal (Pb) pada Lipstik di Wilayah Kota Surabaya yang Teregistrasi dan Tidak Teregistrasi Menggunakan Spektofotometri Serapan Atom (SSA)

2019 ◽  
Vol 4 (1) ◽  
pp. 41-44
Author(s):  
M.A. Hanny Ferry Fernanda ◽  
Devi Elidya ◽  
Novianti Ayu Manaheda ◽  
Nurul Qomaryah ◽  
Muhammad Khotibul Umam ◽  
...  
Keyword(s):  
Heavy Metal ◽  
Sample Preparation ◽  
Atomic Absorption ◽  
Metal Content ◽  
Atomic Absorption Spectrophotometry ◽  
Heavy Metal Content ◽  
Atomic Absorption Spectrophotometer ◽  
Aqua Regia ◽  
Absorption Spectrophotometry ◽  
A Value

ABSTRAKLipstik merupakan salah satu kosmetik yang paling banyak dan hampir setiap hari digunakan oleh wanita. Timbal adalah salah satu cemaran logam berat yang terdapat dalam lipstik. Penelitian ini bertujuan untukmengetahui kandungan logam berat timbal dalam lipstik yang teregistrasi dan tidak teregistrasi mengguanakan Spektrofotometer Serapan Atom (SSA). Preparasi sampel menggunakan destruksi basah dengan aqua regia. Sampel lipstik yang digunakan sebanyak 24 sampel lipstik yang diambil di wilayah Kota Surabaya, dimana 12 sampel memiliki nomor registrasi BPOM dan 12 sampel tidak memiliki nomor registrasi BPOM. Hasil penelitian menunjukkan adanya kandungan logam berat yang melebihi persyaratan BPOM pada semua sampel lipstikdengan rata-rata kadar 108.9517 ppm untuk lipstik yang teregistrasi dan 102.7183 ppm untuk lipstik yang tidak teregistrasi. Berdasarkan uji Mann-Whitney U diketahui bahwa tidak ada beda antara kadar Pb pada lipstik yang teregistrasi dengan lipstik yang tidak teregistrasi dengan nilai α= 0,05.Kata kunci: Timbal (Pb), Lipstik, Surabaya, Registrasi, Spektrofotometri Serapan Atom. ABSTRACTLipstick is one of the most widely used cosmetics every day by women. Lead is one of the heavy metal contaminants found in lipstick. This study aims to determine the heavy metal content of lead in registered lipstickand not registered using Atomic Absorption Spectrophotometer (AAS). Sample preparation using wet destruction with aqua regia. Lipstick samples were used as many as 24 lipstick samples taken in the Surabaya area, where 12 samples had BPOM registration numbers and 12 samples did not have BPOM registration numbers. The results showed that there was a heavy metal content that exceeded BPOM requirements for all lipstick samples with an average level of 108.9517 ppm for registered lipstick and 102.7183 ppm for unregistered lipstick. Basedon the Mann-Whitney U test it is known that there is no difference between Pb levels on lipstick registered with lipstick which was not registered with a value of α = 0.05.Keywords: Lead (Pb), Lipstick, Surabaya, Registration, Atomic Absorption Spectrophotometry..

Analysis of Lead Heavy Metal (Pb) Contamination on Matte Lipstick Preparations for Sale in Banda Aceh City Aceh Market

2020 ◽  
Vol 2 (1) ◽  
Author(s):  
Rizki Andalia ◽  
Mulia Aria Suzanni ◽  
Rini Rini
Keyword(s):  
Heavy Metal ◽  
Atomic Absorption ◽  
Atomic Absorption Spectrophotometry ◽  
The Body ◽  
Permissible Limit ◽  
The Sun ◽  
Absorption Spectrophotometry ◽  
Pb Contamination ◽  
Body Organ ◽  
Banda Aceh

Lipstick or lip dye is a cosmetic dose that serves to coloring, decorative the lips, as a moisturizing material and protect the lips from exposure the sun to provide optimum results. Lipstick should not contain chemicals such as lead (Pb) because the Pb is a heavy metal that is very dangerous when continuously used on the skin, because it will be absorbed into the blood and attack the body organ causing the onset of disease. According to BPOM that the lead rate on the lipstick does not exceed the permissible limit of 20 mg/kg or 20 ppm.This research aims to know the levels contained in the samples are 4 brands of matte lipstick that are sold in the Aceh market in Banda Aceh City with the method of atomic absorption spectrophotometry (AAS). The results showed that on the 4 brands of lipstick matte contain heavy metal lead (Pb) with a rate still qualified allowed by BPOM  is samples A, B, C, and D, respectively at 0.24 ppm; 0.10 ppm; 2.87 ppm and 1.32 ppm, so that the 4 brands of lipstick matte are still used.

scholarly journals Potential of Hyacinth Activated in Lowering Levels of Lead Heavy Metals by Method of Atomic Absorption Spectrophotometry

2021 ◽  
Vol 4 (2) ◽  
pp. 53-61
Author(s):  
Dita Kusuma Wardani ◽  
Tuti Alawiyah ◽  
Madschen Sia Mei Ol Siska Selvija Tambun
Keyword(s):  
Heavy Metals ◽  
Activated Carbon ◽  
Atomic Absorption ◽  
Atomic Absorption Spectrophotometry ◽  
Absorption Spectrophotometry ◽  
Metal Levels ◽  
Lead Metal ◽  
Maximum Contact ◽  
Test Result ◽  
Made In

The Barito River as the largest and longest river in South Kalimantan has been convicted as the most polluted river on an international level. Where one of the most commonly found compounds is the heavy metal lead (Pb) with a high enough levels that alternatives are needed to reduce the levels of the metal. One way to reduce the levels of such heavy metals is to use activated carbon hyacinth. So the activated carbon from hyacinth is made in accordance with SII No.0258-79 and knows the effect of variations in the administration of activated carbon hyacinth at a time of 15 minutes, 30 minutes and 45 minutes in lowering the levels of lead heavy metals (Pb). The research method used to determine the effect of variations in the administration of activated carbon hyacinth is by quantitative testing using the Atomic Absorption Spectrophotometry tool. The results showed that activated carbon hyacinth has met SII No.0258-79 with a randemen test result of 15%, water content of 3%, and absorption of iodine of 241.16 mg / gram. Significant value produced 0.742 with regression value (r) 0.999 and resulted in decreased lead metal levels in the variation of 15 minutes activated carbon administration of -0.030 mg / l with an absorption of 120%, 30 minutes of 0.073 mg / l with an absorption of 48% and 45 minutes of -0.097 mg / l with an absorption of 167%. Hyacinth activated carbon can be used to lower the levels of lead heavy metals (Pb) with a maximum contact time of 45 minutes by 167%.

scholarly journals KANDUNGAN LOGAM BERAT (Cu, Pb, Zn, Cd, dan Cr) DALAM AIR DAN SEDIMEN DI PERAIRAN TELUK JAKARTA

2016 ◽  
Vol 11 (1) ◽  
pp. 9 ◽  
Author(s):  
Yani Permanawati ◽  
Rina Zuraida ◽  
Andrian Ibrahim
Keyword(s):  
Heavy Metals ◽  
Heavy Metal ◽  
Metal Content ◽  
Sea Water ◽  
Sediment Quality ◽  
Atomic Absorption Spectrophotometry ◽  
Quality Score ◽  
Subsurface Sediment ◽  
Absorption Spectrophotometry ◽  
Seawater Quality

Penelitian Lingkungan dan Kebencanaan Geologi Kelautan Perairan Teluk Jakarta (Tanjung Kait – Muara Gembong) dilakukan pada bulan Oktober - November 2010. Uji logam berat (Cu, Pb, Zn, Cd, dan Cr) dilakukan terhadap 28 contoh air laut dan 28 contoh sedimen dasar laut menggunakan metoda Atomic Absorption Spectrophotometry (AAS). Tujuan penelitian ini adalah untuk mendapatkan data dan informasi kondisi lingkungan terkini dari kandungan logam berat dalam air laut dan sedimen dasar laut. Kandungan logam berat (air laut dalam mg/l : sedimen dasar laut dalam ppm) terukur sebagai berikut : Cu ( <0.005 : 15.000-169.500 ); Pb (0.005-0.011 : 14.000-58.100); Zn (0.005-0.007 : 95.800-333.000); Cd (0.006-0.015 : 0.012-0.750); Cr (<0.001 : 45.320-139.180). Berdasarkan Metode Storet dapat dilihat nilai status mutu air laut perairan ini adalah -12, berarti bahwa kualitas air laut di perairan termasuk kelas C (tercemar sedang). Sedangkan status mutu sedimen di perairan menunjukkan skor nilai status mutu sedimen adalah 0, yang berarti bahwa kualitas sedimen termasuk kelas A (tidak tercemar/memenuhi baku mutu). Jelas terlihat bahwa nilai ambang batas (NAB) logam berat dalam sedimen jauh lebih tinggi dari NAB logam berat dalam air. Kata kunci: logam berat, sedimen dasar laut, air laut, nilai status mutu Marine Environmental and Geological Hazard Survey In Jakarta Bay Waters (Tanjung Kait - Muara Gembong) conducted in October-November 2010. Testing of heavy metals (Cu, Pb, Zn, Cd, and Cr) performed on 28 samples of sea water and 28 subsurface sediment samples using the method of Atomic Absorption Spectrophotometry (AAS). The purpose of this study was to obtain data and information on current environmental conditions of heavy metal content in seawater and subsurface sediment. Heavy metal content (sea water in mg/l: subsurface sediment in ppm) measured as follows: Cu ( <0.005 : 15.000-169.500 ); Pb (0.005-0.011 : 14.000-58.100); Zn (0.005-0.007 : 95.800-333.000); Cd (0.006-0.015 : 0.012-0.750); Cr (<0.001 : 45.320-139.180). Based on the Storet method shows the value of water quality status of sea waters is -12, which means that the seawater quality in these waters belong to a class C (medium contaminated). While the status of sediment quality in these waters indicate subsurface sediment quality score status value is 0, which means that subsurface sediment quality belongs to the class A (not polluted/correspond to the quality standards). It is clearly seen that the threshold value (NAV) of heavy metals in sediments is much higher than the NAV of heavy metals in water. Keywords: heavy metal, subsurface sediment, seawater, quality score status

Analysis for lead in undiluted whole blood by tantalum ribbon atomic absorption spectrophotometry.

1978 ◽  
Vol 24 (7) ◽  
pp. 1182-1185 ◽  
Author(s):  
B L Therrell ◽  
J M Drosche ◽  
T W Dziuk
Keyword(s):  
Sample Preparation ◽  
Atomic Absorption ◽  
Whole Blood ◽  
Extended Period ◽  
Atomic Absorption Spectrophotometry ◽  
Single Beam ◽  
Absorption Spectrophotometry ◽  
Primary Screening ◽  
Beam System ◽  
No Sample Preparation

Abstract We describe a modified tantalum ribbon atomic absorption procedure for determining lead in undiluted whole blood. An instrumentation Laboratory (I.L.) Model 151 atomic absorption spectrophotometer equipped with an I.L. Model 355 Flameless Sampler was used. The Flameless Sampler was slightly modified to include three-cycle operation instead of the normal two cycles. This modified single-beam system, equipped with background correction, allows 5-microliter specimens of whole blood to be quickly and accurately analyzed. No sample preparation other than vortex mixing is involved and method reliability has been demonstrated during an extended period of successful participation in proficiency testing studies conducted by the Center for Disease Control. This tantalum ribbon methodology has further been demonstrated to be effective both as a primary screening procedure and as a confirmatory procedure, when coupled with erythrocyte protoporphyrin determinations, in screening over 300 000 clients during a three-year period of use in the Early and Periodic Screening, Diagnosis and Treatment (EPSDT) Program in Texas.

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