Microstructural Analysis of Failure of a Stainless Steel Bone Plate Implant

Materials ◽  
2021 ◽  
Vol 14 (23) ◽  
pp. 7110
Author(s):  
Yanbin Pei ◽  
Xuanhui Qu ◽  
Qilu Ge ◽  
Tiejun Wang

Borated stainless steel (BSS) specimens have a boron content of 1.86 wt%, and are prepared by hot isostatic pressing (HIP) conducted at different temperatures, ranging from 1000 to 1100 °C and a constant true strain rate (0.01, 0.1, 1 and 10 s−1). These tests, with observations and microstructural analysis, have achieved the hot deformation characteristics and mechanisms of BSS. In this research, the activation energy (Q) and Zener–Hollomon parameter (Z) were contrasted against the flow curves: Q = 442.35 kJ/mol. The critical conditions associated with the initiation of dynamic recrystallization (DRX) for BSS were precisely calculated based on the function between the strain hardening rate with the flow stress: at different temperatures from 1000 to 1100 °C: the critical stresses were 146.69–254.77 MPa and the critical strains were 0.022–0.044. The facts show that the boron-containing phase of BSS prevented the onset of DRX, despite the saturated boron in the austenite initiated DRX. The microstructural analysis showed that hot deformation promoted the generation of borides, which differed from the initial microstructure of HIP. The inhomogeneous distribution of elements in the boron-containing phase was caused by hot compression.


2021 ◽  
Vol 1016 ◽  
pp. 206-212
Author(s):  
Kazuyoshi Saida ◽  
Tomo Ogura ◽  
Shotaro Yamashita ◽  
Yusuke Oikawa

Computer simulation of the α/γ phase transformation in multipass weld of duplex stainless steel was made for predicting the distribution of the γ phase fraction in the weld metal (WM) and HAZ. The kinetic equations including rate constants of the dissolution behaviour as well as precipitation behaviour of γ phase were determined by isothermal heat treatment test. Based on the kinetic equations determined, the distribution of the γ phase fraction in multipass weld of duplex stainless steel was calculated applying the incremental method combined with the heat conduction analysis in welding process. The γ phase fraction was reduced in the higher temperature HAZ and WM, however, that in the reheated HAZ and WM was increased and recovered to the base metal level. Microstructural analysis revealed that the calculated results of the γ phase fraction in multipass weld were consistent with experimental ones. Based on the computer prediction, the microstructural improvement welding (“reheat bead welding”) process, with analogous concept to the temper bead welding technique, was newly proposed for recovering the γ phase fraction in weld even in the as-welded situation.


Materials ◽  
2020 ◽  
Vol 13 (19) ◽  
pp. 4377
Author(s):  
Tomas Cegan ◽  
Marek Pagac ◽  
Jan Jurica ◽  
Katerina Skotnicova ◽  
Jiri Hajnys ◽  
...  

The manufacturing route primarily determines the properties of materials prepared by additive manufacturing methods. In this work, the microstructural features and mechanical properties of 316 L stainless steel prepared by the selective laser method have been determined. Three types of samples, (i) selective laser melted (SLM), (ii) selective laser melted and hot isostatic pressed (HIP) and (iii) selective laser melted and heat treated (HT), were characterized. Microstructural analysis revealed that SLM samples were formed by melt pool boundaries with fine cellular–dendritic-type microstructure. This type of microstructure disappeared after HT or HIP and material were formed by larger grains and sharply defined grain boundaries. The SLM-prepared samples contained different levels of porosity depending on the preparation conditions. The open interconnected LOF (lack of fusion) pores were observed in the samples, which were prepared with using of scanning speed 1200 mm/s. The blowhole and keyhole type of porosity were observed in the samples prepared by lower scanning speeds. The HIP caused a significant decrease in internal closed porosity to 0.1%, and a higher pressure of 190 MPa was more effective than the usually used pressure of 140 MPa, but for samples with open porosity, HIP was not effective. The relatively high yield strength of 570 MPa, tensile strength of 650 MPa and low ductility of 30–34% were determined for SLM samples with the lower porosity content than 1.3%. The samples after HIP showed lower yield strengths than after SLM (from 290 to 325 MPa) and relatively high ductility of 47.8–48.5%, regardless of the used SLM conditions.


Coatings ◽  
2020 ◽  
Vol 10 (2) ◽  
pp. 140 ◽  
Author(s):  
W. K. Chan ◽  
C. T. Kwok ◽  
K. H. Lo

In the present study, the feasibility of laser surface melting (LSM) of AISI 430 ferritic stainless steel to minimize hydrogen embrittlement (HE) was investigated. LSM of AISI 430 steel was successfully achieved by a 2.3-kW high power diode laser (HPDL) with scanning speeds of 60 mm/s and 80 mm/s (the samples are designated as V60 and V80, respectively) at a power of 2 kW. To investigate the HE effect on the AISI 430 steel without and with LSM, hydrogen was introduced into specimens by cathodic charging in 0.1 M NaOH solution under galvanostatic conditions at a current density of 30 mA/cm2 and 25 °C. Detail microstructural analysis was performed and the correlation of microstructure with HE was evaluated. By electron backscatter diffraction (EBSD) analysis, the austenite contents for the laser-surface melted specimens V60 and V80 are found to be 0.6 and 1.9 wt%, respectively. The amount of retained austenite in LSM specimens was reduced with lower laser scanning speed. The surface microhardness of the laser-surface melted AISI 430 steel (~280 HV0.2) is found to be increased by 56% as compared with that of the substrate (~180 HV0.2) because of the presence of martensite. The degree of embrittlement caused by hydrogen for the charged and non-charged AISI 430 steel was obtained using slow-strain-rate tensile (SSRT) test in air at a strain rate of 3 × 10−5 s−1. After hydrogen pre-charging, the ductility of as-received AISI 430 steel was reduced from 0.44 to 0.25 while the laser-surface melted AISI 430 steel showed similar tensile properties as the as-received one. After LSM, the value of HE susceptibility Iδ decreases from 43.2% to 38.9% and 38.2% for V60 and V80, respectively, due to the presence of martensite.


2017 ◽  
Vol 740 ◽  
pp. 54-59
Author(s):  
Siti Khadijah Alias ◽  
Bulan Abdullah ◽  
Mahesh Talari ◽  
Muhammad Hafizuddin Jumadin ◽  
Mohd Faizul Idham ◽  
...  

The implementation of boronizing in low alloy steel had been implemented tremendously in past years as this method offers excellent surface protection that led to enhancement of hardness and wear of the material. In conjunction to that, few parameters had been recognized as the factor that promotes boron diffusion into the surface of the material which is the selection of boronizing temperature and time. This study concentrated on the effect of pack boronizing on the boride layer thickness of 304 stainless steel which contained high amount of alloying elements. The microstructural analysis and boron layer thickness was measured and observed using optical microscopy and SEM analyzer. The microhardness of the material was measured using Vickers microhardness tester. The results portrayed that boronizing successfully induced boronizing layer containing FeB and Fe2B phases with thickness of 15μm. This resulted in major improvement of the microhardness values with improvement of 5 times compared to non-boronized samples.


2017 ◽  
Vol 75 (36) ◽  
pp. 9-17 ◽  
Author(s):  
Motoaki Morita ◽  
Wataru Shinohara ◽  
Ryohei Hashimoto ◽  
Shinichi Motoda

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