scholarly journals Ca-induced Plasticity in Magnesium Alloy: EBSD Measurements and VPSC Calculations

Crystals ◽  
2020 ◽  
Vol 10 (2) ◽  
pp. 67 ◽  
Author(s):  
Umer Masood Chaudry ◽  
Kotiba Hamad ◽  
Jung-Gu Kim

In the present work, Ca-induced plasticity of AZ31 magnesium alloy was studied using electron backscattered diffraction (EBSD) measurements supported by viscoplastic self-consistent (VPSC) calculations. For this purpose, alloy samples were stretched to various strains (5%, 10%, and 15%) at room temperature and a strain rate of 10−3 s−1. The EBSD measurements showed a higher activity of non-basal slip system (prismatic slip) as compared to that of tension twins. The VPSC confirmed the EBSD results, where it was found that the critical resolved shear stress of the various slip systems and their corresponding activities changed during the stretching of the alloy samples.

1996 ◽  
Vol 460 ◽  
Author(s):  
M. Moriwaki ◽  
K. Ito ◽  
H. Inui ◽  
M. Yamaguchi

ABSTRACTThe deformation behavior of single crystals of Mo(Si,Al)2 with the C40 structure has been studied as a function of crystal orientation and Al content in the temperature range from room temperature to 1500°C in compression. Plastic flow is possible only above 1100°C for orientations where slip along <1120> on (0001) is operative and no other slip systems are observed over whole temperature range investigated. The critical resolved shear stress for basal slip decreases rapidly with increasing temperature and the Schmid law is valid. Basal slip appears to occur through a synchroshear mechanism, in which a-dislocations (b=1/3<1120>) dissociate into two synchro-partial dislocations with the identical Burgers vector(b*1/6<1120>) and each synchro-partial further dissociates into two partials on two adjacent planes.


Single-crystal test specimens of van Arkel titanium were obtained by a modification of the strain anneal technique.The modes of slip have been identified as (101̄0) [112̄0],(101̄1) [112̄0], and (0001) [112̄0]. It has been shown that not only does the interstitial impurity affect the magnitude of the critical resolved shear stress but also the relative values for the three slip systems. (101̄0) is the principal slip system and is favoured by increasing purity. A possible mechanism for the role of oxygen and nitrogen in this effect is put forward wherein it is shown that the interstitial sites occupied are such that interstitial elements render slip more difficult on two of the three slip planes in titanium.


2010 ◽  
Vol 654-656 ◽  
pp. 695-698 ◽  
Author(s):  
Tsuyoshi Mayama ◽  
Tetsuya Ohashi ◽  
Kenji Higashida

Crystal plasticity finite element analysis method considering the accumulation of geometrically necessary (GN) dislocations was applied to monotonic loading of pure magnesium bi-crystal. The deformation mechanisms considering in the present analysis method are basal slip <a>, prismatic slip <a>, 1st order pyramidal slip <a>, 2nd order pyramidal slip <a+c> and tensile twinning <a+c>. Tensile twinning is incorporated into crystal plasticity analysis assuming that twinning plane and direction of shear by twinning are equivalent to slip plane and slip direction, respectively. Critical resolved shear stresses (CRSSs) for each slip system in the literatures were used. Analysis model is designed to investigate the influence of grain boundary on the activation of slip systems. That is, one grain consisting of bi-crystal (grain A) had the crystal orientation whose Schmid factor for prismatic slip is 0.5. The crystal orientation of the other grain (grain B) was slightly deviated from that of grain A. The result of the calculation of tensile loading of the bi-crystal showed that both grains are deformed by the multiple slip of basal slip system, which resulted in the formation of GN dislocation bands.


2008 ◽  
Vol 72 (6) ◽  
pp. 1181-1199 ◽  
Author(s):  
C. D. Barrie ◽  
A. P. Boyle ◽  
S. F. Cox ◽  
D. J. Prior

AbstractA suite of experimentally deformed single-crystal pyrite samples has been investigated using electron backscatter diffraction (EBSD). Single crystals were loaded parallel to <100> or <110> and deformed at a strain rate of 10-5s-1, confining pressure of 300 MPa and temperatures of 600°C and 700°C. Although geometrically (Schmid factor) the {001}<100> slip system should not be activated in <100> loaded samples, lattice rotation and boundary trace analyses of the distorted crystals indicate this slip system is easier to justify. Determination of 75 MPa as the critical resolved shear stress (CRSS) for {001}<100> activation, in the <110> loaded crystals, suggests a crystal misalignment of ~5—15° in the <100> loaded crystals would be sufficient to activate the {001}<100> slip system. Therefore, {001}<100> is considered the dominant slip system in all of the single-crystal pyrite samples studied. Slip-system analysis of the experimentally deformed polycrystalline pyrite aggregates is consistent with the single-crystal findings, with the exception that {001}<11̄> also appears to be important, although less common than the {001}<100> slip system. The lack of crystal preferred orientation (CPO) development in the polycrystalline pyrite aggregates can be accounted for by the presence of two independent symmetrically equivalent slip systems more than satisfying the von Mises criterion.


Materials ◽  
2020 ◽  
Vol 13 (11) ◽  
pp. 2633 ◽  
Author(s):  
Umer Masood Chaudry ◽  
Kotiba Hamad ◽  
Jung-Gu Kim

Pre-stretching experiments were carried out on AZ31–0.5Ca magnesium alloy to alter the microstructure and texture for enhancing room-temperature formability. Compared to as-received alloy, the formability of a 5%-stretched sample was improved by 15%. This was attributed to enhanced strain hardening capability related to the weakening of basal texture and less homogeneous microstructure. In addition, in-grain misorientation axis analysis performed on the samples (as-received and stretched) also confirmed the higher activity of the non-basal slip systems in the 5%-stretched sample.


Author(s):  
Shadab Siddiqui ◽  
Nagaraj K. Arakere ◽  
Fereshteh Ebrahimi

A comprehensive numerical investigation of plasticity (slip) evolution near notches was conducted at 28°C and 927°C, for two crystallographic orientations of double-notched single crystal nickel base superalloys (SCNBS) specimens. The two specimens have a common loading orientation of &lt;001&gt; and have notches parallel to the &lt;010&gt; (specimen I) and &lt;110&gt; (specimen II) orientation, respectively. A three dimensional anisotropic linear elastic finite element model was employed to calculate the stress field near the notch of these samples. Resolved shear stress values were obtained near the notch for the primary octahedral slip systems ({111} &lt;110&gt;) and cube slip systems ({100} &lt;110&gt;). The effect of temperature was incorporated in the model as changes in the elastic modulus values and the critical resolved shear stress (CRSS). The results suggest that the number of dominant slip systems (slip systems with the highest resolved shear stress) and the size and the shape of the plastic zones around the notch are both functions of the orientation as well as the test temperature. A comparison between the absolute values of resolved shear stresses near the notch at 28°C and 927°C on the {111} slip planes revealed that the plastic zone size and the number of activated dominant slip systems are not significantly affected by the temperature dependency of the elastic properties of the SCNBS, but rather by the change in critical resolved shear stress of this material with temperature. The load required to initiate slip was found to be lower in specimen II than in specimen I at both temperatures. Furthermore, at 927°C the maximum resolved shear stress (RSS) on the notch surface was found to be greater on the {100} slip planes as compared with the {111} slip planes in both specimens. The results from this study will be helpful in understanding the slip evolution in SCNBS at high temperatures.


2007 ◽  
Vol 561-565 ◽  
pp. 459-462
Author(s):  
Katsushi Tanaka ◽  
Hiromitsu Ide ◽  
Yoshinori Sumi ◽  
Kyosuke Kishida ◽  
Haruyuki Inui

Compressive deformation of L10-ordered single crystals of FePd whose c/a ratio less than unity have been investigated from room temperature to 823 K. The results show that the critical resolved shear stress (CRSS) for octahedral glide of ordinary dislocations is smaller than that of super-lattice dislocations in all the temperature range investigated, that is the opposite sense to the case of Ti-56 mol% Al. The CRSS for ordinary dislocations virtually independent to the temperature. On the other hand, the CRSS for super dislocations exhibits a weak positive temperature dependence from room temperature up to 573 K and decreases in higher temperatures.


Solid Earth ◽  
2017 ◽  
Vol 8 (5) ◽  
pp. 883-898 ◽  
Author(s):  
Ilka Weikusat ◽  
Ernst-Jan N. Kuiper ◽  
Gill M. Pennock ◽  
Sepp Kipfstuhl ◽  
Martyn R. Drury

Abstract. Ice has a very high plastic anisotropy with easy dislocation glide on basal planes, while glide on non-basal planes is much harder. Basal glide involves dislocations with the Burgers vector b = 〈a〉, while glide on non-basal planes can involve dislocations with b = 〈a〉, b = [c], and b = 〈c + a〉. During the natural ductile flow of polar ice sheets, most of the deformation is expected to occur by basal slip accommodated by other processes, including non-basal slip and grain boundary processes. However, the importance of different accommodating processes is controversial. The recent application of micro-diffraction analysis methods to ice, such as X-ray Laue diffraction and electron backscattered diffraction (EBSD), has demonstrated that subgrain boundaries indicative of non-basal slip are present in naturally deformed ice, although so far the available data sets are limited. In this study we present an analysis of a large number of subgrain boundaries in ice core samples from one depth level from two deep ice cores from Antarctica (EPICA-DML deep ice core at 656 m of depth) and Greenland (NEEM deep ice core at 719 m of depth). EBSD provides information for the characterization of subgrain boundary types and on the dislocations that are likely to be present along the boundary. EBSD analyses, in combination with light microscopy measurements, are presented and interpreted in terms of the dislocation slip systems. The most common subgrain boundaries are indicative of basal 〈a〉 slip with an almost equal occurrence of subgrain boundaries indicative of prism [c] or 〈c + a〉 slip on prism and/or pyramidal planes. A few subgrain boundaries are indicative of prism 〈a〉 slip or slip of 〈a〉 screw dislocations on the basal plane. In addition to these classical polygonization processes that involve the recovery of dislocations into boundaries, alternative mechanisms are discussed for the formation of subgrain boundaries that are not related to the crystallography of the host grain.The finding that subgrain boundaries indicative of non-basal slip are as frequent as those indicating basal slip is surprising. Our evidence of frequent non-basal slip in naturally deformed polar ice core samples has important implications for discussions on ice about plasticity descriptions, rate-controlling processes which accommodate basal glide, and anisotropic ice flow descriptions of large ice masses with the wider perspective of sea level evolution.


1990 ◽  
Vol 213 ◽  
Author(s):  
R.D. Field ◽  
D.F. Lahrman ◽  
R. Darolia

ABSTRACTA detailed study of deformation of NiAl single crystals in two soft orientations, <110> and <111>, has been conducted. The Schmid factor favors {100} slip in the former and {110} slip in the latter. Detailed dislocation analysis, critical resolved shear stress measurements, and slip trace analysis have been performed to determine the nature of dislocation motion and interactions in this material. Particular attention is given to prismatic loops formed during deformation, since the shapes of these loops reveal the active slip planes. Similar loop morphologies observed in elevated temperature [001] oriented tensile specimens are also discussed.


1990 ◽  
Vol 186 ◽  
Author(s):  
F.D. Tichelaar ◽  
F.W. Schapink

AbstractThe glide behaviour of superdislocations at a coherent twin boundary in ordered Cu3Au was examined in a transmission electron microscope for the case when the superdislocations are sessile in the boundary. Possible schemes for dissociation of a superdislocation in the boundary were analysed geometrically. The leading superpartial of each superdislocation dissociated into a superpartial in the matrix and a residual Shockley partial in the boundary of glissile type. The trailing superpartial remained undissociated in the boundary. The superpartial in the matrix glided on a cube plane, and a ribbon of APB connected to the boundary was left in its trail. The cube slip occurs as a result of (i) a maximal resolved shear stress for the observed slip system and (ii) the geometric criteria for slip applied to all possible slip systems in the matrix. The Schmid factors for the slip systems in the matrix could be calculated by assuming a uniform tensile axis in the foil. The tensile axis was deduced from the observed slip systems in the twin.


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