scholarly journals Evolution of Recrystallized Grain and Texture of Cold-Drawn Pure Mg Wire and Their Effect on Mechanical Properties

Materials ◽  
2020 ◽  
Vol 13 (2) ◽  
pp. 427
Author(s):  
Jiao Meng ◽  
Liuxia Sun ◽  
Yue Zhang ◽  
Feng Xue ◽  
Chenglin Chu ◽  
...  

Static recrystallization plays a key role in the fabrication of thin Mg wires as well as the mechanical properties of the final wires. The effect of annealing parameters on the evolution of the microstructures, textures and mechanical properties of cold-drawn pure Mg wire was studied by means of optical microscopy (OM), electron backscatter diffraction (EBSD), a tensile test and a hardness test. This study shows that the mechanical properties of as-annealed pure thin Mg wire is affected not only by the average grain size, but also the uniformity of the recrystallization grains, including the uniformity of grain size and crystal orientation distribution (more random texture component). With increasing annealing temperature and time, the uniformity of recrystallization grain size first improved and then declined after obvious grain growth. At the same time, the randomness of the basal texture component declined with the development of recrystallization. Annealing at 300 °C for 30 min caused the most uniform grain size and orientation distribution in the microstructures, thus contributing to the best plasticity among all experimental wires. It is reasonable to conclude that more uniform and regular recrystallized grains and a more randomly distributed crystal orientation would be benefit for the mechanical properties of Mg wires.

2012 ◽  
Vol 217-219 ◽  
pp. 433-436
Author(s):  
Zhi Fen Wang ◽  
Rong Dong Han ◽  
Shun Bin Zhou ◽  
Hai E Huang ◽  
Li Xin Wu

Effect of phosphorus content on the mechanical properties and microstructure of IF steel sheets was investigated. Average grain size and recrystallization texture were measured by electron backscatter diffraction (EBSD). The results showed that the higher P resulted in higher tensile strength and lowered the elongation and r-value. The average grain size increased with decreasing P content. The //ND (γ-fiber) pole intensity had a lowest value for IF steel with the highest P content which in turn deteriorate r-value. The element P played an important role in recrystallization process which affected the mechanical properties and microstructure of IF steels.


2007 ◽  
Vol 558-559 ◽  
pp. 149-152
Author(s):  
H.S. Chen ◽  
Andrew Godfrey ◽  
Niels Hansen ◽  
Qing Liu

The effect of crystal orientation on the recovery and recrystallization of cold-rolled Ni (99.96% purity) has been investigated. Particular attention was paid to the annealing response of regions with either the Copper (C), Brass (B) or S rolling texture orientations. Samples with an initial average grain size of approx. 500μm were deformed to strains of up to εvM = 4.5. As a result of the large initial grain size, even after high rolling reductions it is possible to find sufficiently large regions of material with similar crystal orientation to analyze the recovery and recrystallization behaviour as a function of crystal orientation. Microstructural investigations were carried out in the scanning electron microscope using both electron channeling contrast and electron backscatter diffraction orientation mapping. Both the S and C orientation regions exhibit a heterogeneous microstructure containing bands of localized deformation. The presence of volumes surrounded by high angle boundaries in these regions strongly influences both the recovery and recrystallization behaviour of the material. Twinning was observed also to play an important role in the generation of recrystallized grains, with twin chains of up to 3 generations being observed.


2012 ◽  
Vol 535-537 ◽  
pp. 593-596
Author(s):  
Zhi Fen Wang ◽  
Rong Dong Han ◽  
Shun Bing Zhou ◽  
Zhong Hai Yao ◽  
Li Xin Wu

Effect of annealing time on the microstructure and texture of IF steel sheets was investigated. Average grain size, grain boundary character and recrystallization texture were measured by X-ray diffraction (XRD) and electron backscatter diffraction (EBSD) in order to clarify the effect of annealing time on microstructure of recrystallization process. The average grain size increased with increasing annealing time. With rising annealing time, the number of low angle boundary (0~15o) decreased due to the mergence of grain with sub-boundary. The //ND (-fiber) pole intensity had a highest value annealed at 60s. The annealing time played an important role in recrystallization process which affected the mechanical properties and microstructure of IF steels.


2011 ◽  
Vol 702-703 ◽  
pp. 165-168 ◽  
Author(s):  
Aicha Loucif ◽  
Thierry Baudin ◽  
François Brisset ◽  
Roberto B. Figueiredo ◽  
Rafik Chemam ◽  
...  

This investigation uses electron backscatter diffraction (EBSD) to study the development of microtexture with increasing deformation in an AlMgSi alloy having an initial grain size of about 150 µm subjected to high pressure torsion (HPT) up to a total of 5 turns. An homogeneous microstructure was achieved throughout the disc sample at high strains with the formation of ultra-fine grains. Observations based on orientation distribution function (ODF) calculation reveals the presence of the torsion texture components often reported in the literature for f.c.c. materials. In particular, the C {001}<110> component was found to be dominant. Furthermore, no significant change in the texture sharpness was observed by increasing the strain.


2021 ◽  
Vol 71 (03) ◽  
pp. 359-364
Author(s):  
Abir Roy ◽  
Abhishek Kumar

In the present study, AlMgSi alloy was processed through multi-axial compression (MAC) to produce ultrafine-grained microstructure at room temperature. The AlMgSi alloys are widely used in automobile industries for making cylinder heads and brake disks etc. MAC was performed up to three cycles and showed improvement in mechanical properties. The impact of different strain levels upon microstructure changes is investigated using electron backscatter diffraction (EBSD). The average grain size reduced from an initial average grain size of ~ 124 to ~ 3 μm after completion of three cycles of MAC processing. Samples were tested for mechanical properties using uniaxial tensile test, hardness measurements, and corrosion. Tensile test results show a considerable increase in yield strength from ~90 MPa to ~249 MPa after 3 cycles of MAC. The average hardness value increased from 52 VHN to 90 VHN after 3 cycles of MAC. The corrosion resistance of MAC processed samples was found to decrease in comparison to solution-treated samples.


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